CLOVER RESEARCH CENTRE TECHNICAL IN-FORMATION

‘.i ,
0
l
CLOVER RESEARCH CENTRE
TECHNICAL
e
IN-FORMATION
CHROMATOGRAMS
TUNA FISH OIL
PRODUCT CODE: 7005
Please note:
GC calibrated against standards on a daily
basis.
l
l
l
0
r;-
cm0
10 161
13235
13.956
it-4014727
:1 15.6%
. IL
%i
‘-,5:0
l
.c1s 1 16.066
-172
16.744
-41
. ‘I
24.270.
b .$’
f&F7
.25.653
0
0
Data
File
Name
Operator
Instrument
Sample
Name
Run Time
Bar Code:
Acquired
on
Report
Created
on:
Last
Recalib
on
Multiplier
Sample
Info
:
:
:
:
C:\HPCHEM\l\DATA\URGENT\EPOO2715.D
OB
5890-FID
TO.PRODUCTION
: 17 Mar
17 Mar
: 17 NOV
: 1
: Signal
250~1.
99
99
93
11:25
12:10
08:32
Noise-19.
AM
PM
AM
Tuna
Fish
Page Number
: 1
Vial
Number
:6
Injection
Number
:
Sequence
Line
Instrument
Method:
GEORGEl.MT
Analysis
Method
: GEORGEl.MT
Sample
Amount
: 1
ISTD Amount
Oil.Hi-DHA
25N3.7003.B.No.EClOl
@
.
‘)
Data File
Name
:
Operator
:
Instrument
:
:
Sample Name
Run Time Bar Code:
Acquired
on
:
Report
Created
on:
:
Last Recalib
on
:l
Multiplier
Not
all
time
C:\HPCHEM\l\DATA\URGENT\EPOO2715.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
TO.PRODUCTION
Sequence Line
Instrument
Method:
11:25 AM
17 Mar 99
Analysis
Method
12:lO
PM
17 Mar 99
Sample Amount
17 NOV 93 08:32 AM
ISTD Amount
reference
peaks
were
Area
0
l
a
Data File
Name
:
Operator
:
Instrument
Sample Name
F.
Time Bar Code:
A+uired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
Sample Info
Sig.
:5
:6
:
GEORGE1.M'
: GEORGE~.M
: 1
found
Percent
Report
C:\HPCHEM\l\DATA\URGENT\EPOO2715.D
1
OB
Page Number
: 1
5890-FID
Vial
Number
:6
TO.PRODUCTION
Injection
Number :
Sequence Line
17 Mar 99
11:25 AM
Instrument
Method:
GEORGEl.M?
17 Mar 99 12:lO
PM
Analysis
Method
: GEORGEl.M'I
17 NOV 93 08:32 AM
Sample Amount
:l
1
ISTD Amount
Signal
Noise-19.
Tuna Fish Oil.Hi-DHA
25N3.7003.B.No.EClOl
1 in C:\HPCHEM\l\DATA\URGENT\EPOO2715.D
Pk#
Ret Time
Area
Height
Tn?e
++------ --I ,---------^---1 --------------I----I-------1
10.181
1244
423 'W
2
12.002
0
42
Fsho
3
12.058
1733
PV
264
4
13.235
1662
PV
333
5
13.956
1044
BV
183
6
14.227
112517
W
36044
7
14.937
0
Rsho
213
8
15.121
1616
VV
139
9
15.458
1413
w
188
10
15.696
7290
VV
1072
11
16.086
2165
W
365
12
16.269
1016
W
128
13
16.744
32004
w
7377
14
17.048
0
45 Rsho
15
17.991
0
Fsho
174
16
18.066
3850
PV
470
17
19.579
0
Fsho
71998
18
19.621
640648
w
95439
19
20.147
19898
W
2865
20
20.382
1344
w
220
Width
0.045
0.000
0.088
0.071
0.079
0.048
0.000
0.150
0.105
0.105
0.086
0.109
0.066
0.000
0.000
0.115
0.000
0.098
0.103
0.092
Area %
I--------- 1
0.0368
0.0000
0.0513
0.0492
0.0309
3.3286
0.0000
0.0478
0.0418
0.2157
0.0641
0.0300
0 -9468
0.0000
0.0000
0.1139
0.0000
18.9526
0.5887
0.0398
: C:\HPCHEM\l\DATA\URGENT\EPOO27lS.D
Page Number
OB
Mm. Instrument
Vial
Number
5890-FID
Injection
Number
TO.PRODUCTION
Sample Name
\
Sequence
Line
Run Time Bar Code:
Instrument
Method:
17 Mar 99 11:25 AM
Acquired
on
Analysis
Method
12:lO
PM
17
Mar
99
Report
Created
on:
Sample Amount
Last Recalib
on
: 17 NOV 93 08:32 AM
ISTD Amount
1
Multiplier
Data
File
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
0
l
,.:,* -~,
l
_ .:
l
l
l
49
50
51
52
53
54
55
56
57
58
59
60
61
Name
20.569
20.898
21.235
21.364
22.029
22.069
22.196
22.585
22.783
23.121
23.519
23.737
24.162
24.270
24.727
24.858
25.166
25.853
26.287
26.565
26.740
26.952
27.157
27.355
27.567
27.625
27.751
28.211
28.249
28.655
28.903
29.226
29.603
29.755
29.932
30.355
30.421
31.047
31.155
31.302
31.656
10789
130261
0
21903
0
4035
0
29124
0
35312
6931
2334
0
21890
6114
3236
1751
2453
163393
0
6878
7580
388129
78943
0
2148
5397
0
2244
54155
7771
10002
7860
4216
0
0
27526
0
9453
38776
0
1620
22324
420
1881
278
375
95
2732
610
5886
978
221
176
3364
894
442
152
333
33053
170
740
1669
79025
17026
448
445
658
169
227
12472
1440
1483
1284
428
122
1192
4943
45
1874
9468
2338
W
W
Fsho
W
Fsho
w
Rsho
W
Rsho
W
W
w
Fsho
W
W
W
W
PV
PV
Rsho
w
W
W
W
Rsho
w
W
Fsho
W
VV
w
w
W
W
Rsho
Fsho
w
Fsho
Pv
W
Fsho
0.102
0.090
0.000
0.172
0 * 000
0.150
0.000
0.146
0.000
0.091
0.104
0.141
0.000
0.096
0.100
0.102
0.157
0.105
0.077
0.000
0.129
0.069
0.077
0.070
0.000
0.071
0.113
0.000
0.137
0.066
0.082
0.097
0.089
0.133
0.000
0.000
0.079
0.000
0.074
0.062
0.000
:6
:6
:
:
GEORGE~.MT
: GEORGEl.MT
:l
0.3192
3.8536
0.0000
0.6480
0.0000
0.1194
0.0000
0.8616
0.0000
1.0447
0.2051
0.0690
0.0000
0.6476
0.1809
0.0957
0.0518
0.0726
4.8337
0.0000
0.2035
0.2242
11.4822
2.3354
0.0000
0.0636
0.1597
0.0000
0.0664
1.6021
0.2299
0.2959
0.2325
0.1247
0.0000
0.0000
0.8143
0.0000
0.2797
1.1471
0.0000
'
*
:
l
-z
1
m
l
0
0
l
m
.,
‘*
.,
Data File
Name
:
Gperator
Instrument
Gample Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
62
63
64
65
66
67
68
69
70
71
72
73
74
75
'76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
100
101
31.676
31.790
32.033
32.718
33.046
33.170
33.679
33.785
33.876
34.065
34.237
34.477
34.952
35.179
35.396
35.539
35.665
36.034
36.311
36.619
36.854
36.891
37.172
37.521
37.773
37.798
38.J.27
38.356
38.471
38.559
38.690
38.840
38.901
39.020
39.273
39.438
39.640
39.739
40.217
40.229
C:\HPCHEM\l\DATA\URGENT\EPOO2715.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
TO.PRODUCTION
Sequence Line
Instrument
Method:
11:25 A M
17 Mar 99
Analysis
Method
PM
17 Mar 99 12:lO
Sample Amount
17 NOV 93 08:32 A M
ISTD Amount
1
14065
34919
4789
2457
6581
4675
0
8931
0
0
56067
5364
6966
14877
21145
4582
247657
1123
1388
4424
0
1153
3304
9445
0
9226
55286
0
4054
0
18200
1461
1473
36445
0
874224
2511
2078
0
1343
3157
8161
614
313
1411
724
200
935
311
36
15549
1029
1902
3379
4077
1175
73202
136
142
688
132
139
342
1993
1010
1542
14935
250
479
201
5550
517
518
10650
185
206643
405
313
154
158
w
w
W
PV
w
W
Fsho
w
Rsho
Rsho
PV
w
PV
w
w
w
W
W
W
w
Fsho
w
W
w
Fsho
W
PV
Rsho
w
Rsho
w
w
w
W
Fsho
W
w
w
Fsho
PV
0.066
0.064
0.111
0.112
0.069
0.091
0.000
0.132
0.000
0.000
0.055
0.076
0.056
0.066
0.077
0.059
0.053
0.118
0.127
0.094
0.000
0.114
0.127
0.069
0.000
0.086
0.056
0.000
0.122
0.000
0.051
0.043
0.044
0.054
0.000
0.060
0.083
0.093
0.000
0.142
:7
:6
:
GEORGEI.~
: GEORGE1.b
: 1
0.4161
1.0330
0.1417
0.0727
0.1947
0.1383
0.0000
0.2642
0.0000
0.0000
1.6587
0.1587
0.2061
0.4401
0.6255
0.1356
7.3266
0.0332
0.0411
0.1309
0.0000
0.0341
0.0978
0.2794
0.0000
0.2729
1.6356
0.0000
0.1199
0.0000
0.5384
0.0432
0.0436
1.0782
0.0000
25.8626
0.0743
0.0615
0.0000
0.0397
!
‘3
a
-\
Data File
Name
:
Operator
Instrument
Sample Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
Total
a
l
l
a
amount
C:\HPCHEM\l\DATA\URGENT\EPO82715.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
TO.PRODUCTION,
Sequence
Line
17 Mar 99 11:25 AM
Instrument
Method:
17 Mar 99 12:lO
Analysis
Method
PM
17 NOV 93 08:32 AM
Sample Amount
ISTD Amount
1
= 3.38026E+006
:8
:6
:
GEORGE~.MT
: GEORGEl.MT
: 1
CLOVER RESEARCH CENTRE
TECHNICAL
-.
s
INFORMATION
CHROMATOGRAMS
TUNA FISH OIL
l
.
PRODUCT CODE: 9004
Please note:
GC calibrated against standards on a daily
basis.
\i’
)
a
I-
N
::
m
Iz
.l
0
!I
4
.--.
-.- --___
__
_..’70
i
-7.504
8s
d
l
:0 8.590
I%%%7
LCl3:O 10.890
t11.483
'ii'-.
5%%
SW--. .-..,.--A. .-----:I 12.886 *l-L
r .
;
*- ,. . . -- -c15:0
13.733
2
s-m .- -- ---
r1.$&q-
.109
. $L
~4#?8
a
K
---16:lw7
0
-----X18:022.699
Cl8:3w3
26.945
17.122
'3. 8 f
4.7,
*
-2
.
0
Data
File
Operator
Instrument
Name
Sample
Name
Run Time
Bar
Acquired
on
Report
Created
Last
Recalib
Multiplier
Sample
Info
: C:\HPCHEM\l\DATA\URGENT\EPOOl874.D
: OB
5890-FID
: PRODUCTION
Code:
on:
on
: 01
01
:
17
Jul
98
Jul
98
NOV 93
: 1
: Signal-16.Hi-DHA
02:38
03:21
08:32
PM
PM
AM
Tuna
oil.
Page Number
:
Vial
Number
:
Injection
Number
:
Sequence
Line
Instrument
Method:
Analysis
Method
:
Sample
Amount
:
ISTD Amount
B.N.
DF161.
4OOu1/2ml.
1
11
GEORGEl.MTH
GEORGEL.MTE
1
'.
\
Data File
Name
:
Operator
Instrument
Sample Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
C:\HPCHEM\l\DATA\URGENT\EPOOl874.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
PRODUCTION
Sequence Line
Instrument
Method:
01 Jul 98 02:38 PM
Analysis
Method
01 Jul 98 03:21 PM
Sample Amount
17 NOV 93 08:32 AM
ISTD Amount
1
Area
Data File
Name
:
Operator
Instrument
Sample Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
I
t Recalib
on
:
b.-,tiplier
Sample Info
l
Percent
:5
: 11
:
GEGRGE1.M:
: GEORGE~.M:
: 1
Report
C:\HPCHEM\l\DATA\URGENT\EPOOl874.D
Page Number
:l
OB
Vial
Number
: 11
5890-FID
Injection
Number :
PRODUCTION
Sequence Line
:
Instrument
Method:
GEORGE1.M:
01 Jul 98 02:38 PM
01 Jul 98 03:21 PM
Analysis
Method
: GEORGEl.Mlj
Sample Amount
17 NOV 93 08:32 AM
:l
1
ISTD Amount
Signal-16.Hi-DHA
Tuna oil.
B.N. DF161. 400u1/2ml.
l
Sig.
l
0
l
l
1 in C:\HPCHEM\l\DATA\URGENT\EPOOl874.D
Pk#
Ret Time
Area
Height
l---l----------l
------ ------l--------------l----l----1
7.504
2069
430
2
8.112
1624
104
3
8.504
1272
133
4
8.590
2694
1207
5
8.700
1298
295
6
8.852
1074
141
7
9.477
1566
114
8
9.762
1522
102
9
9.344
0
448
10
9.957
2827
733
11
10.890
2372
580
12
11.483
2044
339
13
12.109
99057
37959
14
12.216
2363
521
15
12.650
1716
358
16
12.886
7648
2006
17
13.195
1776
426
18
13.733
28241
8219
19
14.406
1422
218
20
14.794
0
492
21
14.818
4241
685
22
16.118
572445
82990
23
16.490
18030
3583
Tme
W
W
W
v-v
W
w
W
W
Fsho
W
W
W
W
W
W
W
W
W
W
Fsho
W
W
W
Width
---0.088
0.190
0.121
0.037
0.059
0.096
0.169
0.248
0.000
0.065
0.057
0.081
0.041
0.065
0.068
0.057
0.062
0.054
0.093
0.000
0.088
0.093
0.077
Area %
I-- --------I
0.0602
0.0472
0.0370
0.0784
0.0378
0.0313
0.0456
0.0443
0.0000
0.0822
0.0690
0.0594
2.8813
0.0687
0.0499
0.2224
0.0517
0.8214
0.0414
0.0000
0.1234
16.6507
0.5244
-
?I
l
_--
7
l
a
l
a
l
Data File
Name
:
Operator
Instrument
Sample Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
24
25
26
27
28
29
30
31
32
33
34
35
36
37
.38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
16.671
16.822
17.122
17.399
17.498
17.930
18.097
18.575
18.675
18.982
19.144
19.468
19.746
20.250
20.393
20.953
21.060
21.283
21.310
21.931
22.662
22.699
22.837
23.093
23.194
23.334
23.365
23.206
23.635
23.820
23.997
24.181
24.665
24.979
25.002
25.142
25.437
25.703
26.091
26.289
26.645
C:\RPCBEM\l\DATA\URGENT\EPOOI874.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
PRODUCTION
Sequence
Line
Instrument
Method:
02:3a
PM
01 Jul 98
03:21
PM
Analysis
Method
01 Jul 98
Sample Amount
17 NOV 93 oa:32 AM
ISTD Amount
1
1177
10389
133264
0
19958
1203
2925
29675
0
1798
34293
6715
1579
0
25893
8053
0
0
1553
1323
0
161957
3178
5788
0
0
9091
0
431683
74644
3858
6558
2359
0
1498
45869
8858
11691
8238
4338
0
218
1845
25656
493
3102
166
453
3520
1290
293
5485
963
183
129
4007
994
290
108
119
201
19134
25653
507
597
401
1010
1134
53133
63085
16234
555
1225
442
207
233
10244
1770
2138
1547
856
92
w
w
W
Fsho
W
w
w
W
Rsho
w
w
W
w
Fsho
w
w
Rsho
Fsho
w
w
Fsho
W
w
v-v
Rsho
Fsho
w
Fsho
W
W
w
w
W
Fsho
W
W
w
W
w
w
Fsho
0.079
0.086
0.082
0.000
0.095
0.107
0.100
0.121
0.000
0.091
0.097
0.106
0.125
0.000
0.101
0.117
0.000
0.000
0.171
0.098
0.000
0.094
0.105
0.133
0.000
0.000
0.112
0.000
0.096
0.071
0.103
0.080
0.080
0.000
0.089
0.070
0.076
0.082
0.081
0.076
0.000
:6
: 11
:
:
GEORGEI.K
: GEORGEI.M
:l
0.0342
0.3022
3.8763
0.0000
0.5805
0.0350
0.0851,
0.8631
0.0000
0.0523
0.9975
0.1953
0.0459
0.0000
0.7532
0.2342
0.0000
0.0000
0.0452
0.0385
0.0000
4.7108
0.0924
0.1684
0.0000
0.0000
0.2644
0.0000
12.5563
2.1712
0.1122
0.1907
0.0686
0.0000
0.0436
1.3342
0.2576
0.3400
0.2396
0.1262
0.0000
-
Data File
Name
:
Operator*
Instrument
Sample Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
l
--,
0
65
66
67
68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
100
101
102
103
l
a
',C<
1.
0
l
l
.-
Total
C:\HPCHEM\l\DATA\URGENT\EPOOl874.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
PRODUCTION
Sequence Line
Instrument
Method:
02:38 PM
01 Jul 98
Analysis
Method
01 Jul 98 03:21 PM
Sample Amount
17 NOV 93 08:32 AM
ISTD Amount
1
26.679
26.945
27.827
28.359
28.491
28.690
28.988
29.337
29.731
29.895
30.142
30.168
30.330
30.456
30.926
31.159
31.764
31.863
32.181
32.202
32.357
32.498
32.782
33.336
33.423
33.795
33.98*4
34.145
34.231
34.556
34.891
35.015
35.208
35.378
35.580
35.782
36.181
36.212
36.326
amount
= 3.43797E+006
1036
20392
36158
44934
56798
5397
1501
3005
11266
2992
0
1212
2611
5168
65509
9433
6275
17293
0
51479
234858
3672
1305
0
4416
1018
1740
1930
7304
8270
57093
4868
1579
1384
21471
46213
0
881681
0
126
4794
8858
9544
14637
1233
344
636
2925
701
148
181
619
1206
17970
2516
1778
4633
8584
11529
59974
724
277
203
746
150
344
558
2081
2240
16367
1147
432
263
5849
11346
127895
165491
98
W
w
w
w
W
W
w
W
w
w
Fsho
W
W
W
PV
W
W
W
Fsho
w
w
W
W
Fsho
PV
w
w
W
W
W
W
w
PV
W
W
W
Fsho
PV
Rsho
0.114
0.066
0.064
0.071
0.061
0.067
0.067
0.073
0.060
0.066
0.000
0.095
0.065
0.066
0.058
0.058
0.055
0.057
0.000
0.066
0.061
0.073
0.071
0.000
0.083
0.098
0.072
0.052
0.055
0.057
0.055
0.065
0.057
0.075
0.056
0.064
0.000
0.077
0.000
: 7
: 11
:
GEORGE~.MTI
: GEORGE~. MTI
:l
0.0301
0.5931
1.0517
1.3070
1.6521
0.1570
0.0437
0.0874
0.3277
0.0870
0.0000
0.0352
0.0759
0.1503
1.9054
0.2744
0.1825
0.5030
0.0000
1.4974
6.8313
0.1068
0.0379
0 .oooo
0.1284
0.0296
0.0506
0.0561
0.2125
0.2406
1.6607
0.1416
0.0459
0.0403
0.6245
1.3442
0.0000
25.6454
0.0000
:
l
CLOVER RESEARCH CENTRE
e
7.
TECHNICAL
INFORMATION
l
0
CHROMATOGRAMS
TtiA
FISH OIL
.
PRODUCT CODE: 8505
l
,
Please note:
GC calibrated against standards on a daily
basis.
.
*
10.
I
s-
a
17 0
73%
p I
07
1
,768
11.525
l
Cl2578
tl3209
l
g:
l
l
Data File
Name
Operator
Instrument
Sample Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
Sample Info
Lb-)', 7,
C:\HPCHEM\l\DATA\URGENT\EPOO3095.D
OB
Page Number
: 1
\...7j 'I
5890-FID
Vial Number
: 3 c
aL tirrProd.Tuna
Oil
Injection
Number
:
SrrD.
Sequence
Line
07 Jul 99
11:Sl
AM
Instrument
Method:
GEORGEl.MT
07 Jul 99 12:36
PM
Analysis
Method
: GEORGEl.MT
17 NOV 93 08:32 AM
Sample Amount
: 1
1
ISTD Amount
Signal
Noise
33.Tuna
Fish Oil Hi-DHA 2585
Prod.ID
8505
Batch No. EC181
l
.
j
Could
0
C:\HPCHEM\l\DATA\URGENT\EPOO3095.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
Prod.Tuna
Oil
Sequence
Line
07 Jul 99
11:51 AM
Instrument
Method:
07 Jul 99 12:36 PM
Analysis
Method
Sample Amount
17 NOV 93 08:32 AM
ISTD Amount
1
Data File
Name
:
Operator
Instrument
Sample Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
Not
not find
time
reference
peak:
No peak of Number 30's description
all
time reference
peaks were found
Area
0
l
Data File
Name
:
(..,.
Operator
_,.x
T trument
z .ple Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
Sample Info
Sig.
0
1)
l
e
l
at
Percent
30.813
+ 0.124
- 0.063
:5
:3
:
GEORGE1.M:
: GEORGE1.M:
: 1
min.
Report
C:\HPCHEM\l\DATA\URGENT\EPOO3095.D
Page Number
: 1
OB
Vial
Number
S890-FID
:3
Injection
Number :
Prod.Tuna
Oil
Sequence
Line
07 Jul 99 11:Sl
AM
Instrument
Method:
GEORGEl.M?
07 Jul 99 12:36 PM
Analysis
Method
: GEORGEl.M'I
17 NOV 93 08:32 AM
Sample Amount
:l
1
ISTD Amount
Signal
Noise 33.Tuna
Fish Oil‘Hi-DHA
2585
Prod.ID
8505
Batch No. EC181
1 in C:\HPCHEM\l\DATA\URGENT\EPOO3095.D
Ret Time
Area
Pk#
Height
Tme
I---I
---------- ---_-_I-----1 --------------I----I-35 Fsho
0
6.864
1
2472
7.386
43 BV
2
1301
9 .7,68
3
330
BV
Fsho
104
0
11.493
4
2029
11.525
5
185
PV
11.845
6
29 Rsho
0
2153
12.578
7
232
PV
12.796
8
46 Rsho
0
13.209
9
151
w
1292
13.774
10
16 -Fsho
0
13.875
11
125011
42030
PV
14.232
12
143 w
1541
14.551
13
183 VV
1349
14.742
14
8135
1055
w
1925
327
w
15.090
15
15.250
16
128 W
1043
15.630
17
4490
Fsho
0
.,:-< -1
I
Width
-----0.000
0.695
0.083
0.000
0.148
0.000
0.124
0.000
0.115
0.000
0.093
0.141
0.117
0.118
0.087
0.112
0.000
Area %
I---------0.0000
0.0595
0.0313
0.0000
0.0489
0.0000
0.0519
0.0000
0.0311
0.0000
3.0109
0.0371
0.0325
0.1959
0.0464
0.0251
0.0000
1
l
'\
l
Data
File
Name
: C:\HPCHEM\l\DATA\DRGENT\EPOO3095.D
OB
Operator
5890-FID
Instrument
Prod.Tuna
Oil
Sample
Name
Run Time
Bar Code:
11:51
AM
Acquired
on
07 Jul
99
12:36
PM
Report
Created
on:
07 Jul
99
Last
Recalib
on
: 17 NOV 93 08:32
AM
Multiplier
1
l
e
.
l
l
0
0
e
l
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
15.656
16.042
16.792
16.823
18.171
18.645
18.847
19.014
19.299
19.653
19.707
20.357
20.721
20.870
21.065
21.442
21.918
22.184
22.609
22.737
23.251
23.413
23.749
24.515
24.738
24.939
25.317
25.442
25.660
25.882
26.087
26.405
26.525
27.054
27.173
27.293
27.464
27.745
27.947
28.087
28.469
36198
0
0
4167
721909
23500
1483
13039
159988
0
26356
4594
0
37037
0
40730
8612
2381
0
28848
7270
3500
2023
2431
0
191405
1545
8397
9290
508252
93942
2376
7485
3891
0
1351
62959
10764
0
13590
10288
8281
37
353
471
111488
3600
295
2218
29283
1491
2316
426
102
3089
913
5536
980
209
184
3663
829
405
138
265
13
33562
253
852
1909
87216
17482
455
670
360
115
261
12622
1614
144
1639
1451
Page Number
Vial
Number
Injection
Number
Sequence
Line
Instrument
Method:
Analysis
Method
Sample
Amount
ISTD Amount
V-V
Rsho
Fsho
PV
VV
V-V
w
VV
VV
Fsho
VV
IN
Fsho
V-V
Rsho
VV
V-V
v-v
Fsho
VV
VU
vv
VV
PV
Rsho
PV
VV
V-V
v-v
VV
V-V
vv
VV
VV
Rsho
VV
VV
VV
Rsho
VV
VV
0.067
0.000
0.000
0.124
0.103
0.098
0.084
0.091
0.085
0.000
0.166
0.163
0.000
0.165
0.000
0.111
0.130
0.172
0.000
0.115
0.127
0.144
0.203
0.129
0.000
0.089
0.102
0.156
0.074
0.091
0.082
0.076
0.154
0.157
0.000
0.078
0.076
0.100
0.000
0.122
0.102
:6
:3
:
:
GEORGE~.M,
: GEORGE~.M,
:l
0.8718
0.0000
0.0000
0.1004
17.3873
0.5660
0.0357
0.3140
3.8533
0.0000
0.6348
0.1107
0.0000
0.8920
0.0000
0.9810
0.2074
0.0573
0.0000
0.6948
0.1751
0.0843
0.0487
0.0586
0.0000
4.6100
0.0372
0.2022
0.2238
12.2413
2.2626
0.0572
0.1803
0.0937
0.0000
0.0325
1.5164
0.2593
0.0000
0.3273
0.2478
)
-
;j
l
'-J
l
Data File
Name
:
Operator
Instrument
Saiple
Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
59
0
l
0
l
l
l
60
61
62
63
64
65
66
67
68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
28.636
28.789
29.294
29,.321
30.074
30.108
30.236
30.620
30.741
31.011
31.372
31.729
31.935
32.043
32.201
32.763
32.800
33.246
33.509
33.756
34.004
34.215
34.441
34.702
34.971
35.423
35.720
36.042
36.064
36.321
36.460
36.593
36.871
37.197
37.573
37.685
37.785
37.984
38.101
38.526
38.712
C:\HPCHEM\l\DATA\URGENT\EP003095.D
OB
5890-FID
Prod.Tuna
Oil
AM
07 Jul 99 11:Sl
PM
07 Jul 99 12:36
17 NOV 93 08:32 AM
1
5001
0
0
31490
0
8769
42680
22630
49007
6254
1281
4873
0
9209
4780
0
8419
76551
9943
0
7941
18123
29675
305262
0
2838
4001
0
1870
3873
0
9120
8183
74675
2709
0
20224
4485
49043
1121439
0
470
169
3442
4978
1011
1759
9332
4744
10356
575
147
500
46
1566
693
682
1036
19380
1270
145
2114
3760
5247
83320
197
178
665
138
142
411
64
2096
1737
18597
430
74
5673
872
12904
228315
464
Page Number
Vial
Number
Injection
Number
Sequence Line
Instrument
Method:
Analysis
Method
Sample Amount
ISTD Amount
w
Rsho
Fsho
W
Fsho
PV
w
w
W
w
w
w
Rsho
W
W
,Fsho
W
W
W
Rsho
W
PV
W
W
Rsho
W
W
Fsho
W
w
Rsho
PV
w
PV
w
Rsho
W
W
w
W
Rsho
0.149
0.000
0.000
0.091
0.000
0.076
0.071
0.071
0.072
0.148
0.124
0.144
0.000
0.086
0.098
0.000
0.116
0.062
0.108
0.000
0 IO59
0.074
0.085
0.058
0.000
0.209
0.093
0.000
0.173
0.129
0.000
0.067
0.073
0.062
0.094
0.000
0.057
0.072
0.060
0.072
0.000
: 7
:3
:
:
GEORGE~.M'
: GEORGE~.M'
: 1
0.1204
0.0000
0.0000
0.7584
0.0000
0.2112
1.0280 1
0.5450
1.1803
0.1506
0.0308
0.1174
0.0000
0.2218
0.1151
0.0000
0.2028
1.8437
0.2395
0.0000
0.1913
0.4365
0.7147
7.3523
0.0000
0.0684
0.0964
0.0000
0.0450
0.0933
0.0000
0.2196
0.1971
1.7986
0.0653
0.0000
0.4871
0.1080
1.1812
27.0100
0.0000
l
‘.
\
a
Data File
Name
:
Operator
Instrument
Sample Name
Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
100
101
102
103
104
0
Total
l
amount
C:\!.-IPCHEM\l\DATA\DRGENT\EPOO309S.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
Prod.Tuna
Oil
Sequence Line
Instrument
Method:
07 JuI 99 11:51 AM
Analysis
Method
PM
12:36
07 Jul 99
Sample Amount
17 NOV 93 08:32 AM
ISTD Amount
1
38.831
39.034
39.207
39.577
39.602
= 4.151933+006
5150
2654
0
0
1928
610
223
83
142
162
V-V
VV
Rsho
Fsho
PV
0.120
0.162
0.000
0.000
0.155
: 8
:3
:
GEORGE~.MT
: GEORGE~.MT
: 1
0.1240
0.0639
0.0000
0.0000
0.0464
1
CLOVER RESEARCH CENTRE
TECHNICAL
IN-FORMATION
CHROMATOGRAMS
TtiA
FISH OIL
PRODUCT CODE: 8501
l
,
Please note:
GC calibrated against standards on a daily
basis.
3
1
0
425
e
e
16 7:
16:lw720795
e
~7124.173
I IL.
.7-j
0
0
.--....1131724
l
l
Data
File
Name
: C:\HPCHEM\l\DATA\URGENT\EPOO2953.D
Operator
OB
Instrument
5890-FID
Sample
Name
ProductionTO
Run Time
Bar Code:
Acquired
on
25 May 99
11:28
AM
Report
Created
oni
25 May 99
12:15
PM
Last
Recalib
on
: 17 NOV 93 08:32
AM
Multiplier
1
Sample
Info
Signal
Noise
28.TO.Product:
\.L\
L-t
Page Number
: 1
tbD7d
Vial
Number
: 10
Injection
Number
:
Sequence
Line
:
Instrument
Method:
GEORGE1.M':
: GEORGE1.M';
Analysis
Method
Sample
Amount
: 1
ISTD Amount
8501.Batch:
EE191.250ul.
f
hta File Name
: C:\HPCHEM\l\DATA\URGENT\EPOO2953.D
-Operator
OB
-nstrument
5890-FID
ProductionTO
Lample Name
1 Run Time Bar Code:
25 May 99 11:28 AM
cquired
on
PM
Report
Created
on: 25 May 99 12:15
17
NOV
93
08:32
AM
'.ast Recalib
on
:
1
ultiplier
0
0
;ig.
0
.; -,v-.
r;,
.s
.
,.*
1 in C:\HPCHEM\l\DATA\URGENT\EPOO2953.D
Pk#
Ret Time
Area
Height
--.+-.-----1
--------------I-----------I
1
6.888
0
2
3
4
5
6
7
8
9
10
11
-2
13
7.425
10.170
12.033
12.057
12.212
13.224
14.685
15.084
15.250
15.427
15.648
16.040
16.682
17.045
17.917
17.991
19.519
20.051
20.287
20.471
20.795
21.121
21.252
21.454
21.964
1530
1206
0
1509
0
1271
104274
1242
0
1034
6807
1391
29720
0
0
3602
621508
19025
1296
10860
133298
0
19103
0
3515
17
18
19
20
21
22
23
24
25
26
5
10
GEORGEl.MTH
GEORGE~.MTH
I.
C:\HPCHEM\l\DATA\URGENT\EPOO2953.D
Page Number
:l
OB
Vial
Number
: 10
5890-FID
Injection
Number :
ProductionTO
Sequence
Line
Instrument
Method:
GEORGEl.MTH
25 May 99 11:28 AM
Analysis
Method
PM
: GEORGEl.MTH
25 May 99 12:15
Sample Amount
: 1
17 NOV 93 08:32 AM
ISTD Amount
1
Signal
Noise
28.TO.Product:
8501.Batch:
EE191.250ul.
,Jata File
Name
Operator
nstrument
3ample Name
un Time Bar Code:
xquired
on
L<eport Created
on:
&;ast
Recalib
on
:
A*
lultiplier
'Imp
. Info
a
Page Number
:
Vial
Number
:
Injection
Number :
Sequence Line
-.:
Instrument
Method:
Analysis
Method
:
Sample Amount
:
ISTD Amount
,
Area %
Width
'W-w
-I---1 ---------I----------I
87
Fsho
0.000
0.0000
PV
38
0.478
0.0413
BV
369
0.048
0.0325
Fsho
100
0.000
0.0000
-.
BV
0.0407
172
0.114
40
Rsho
0.000
0.0000
PV
143
0.118
0.0343
W
33530
0.048
2.8143
W
104
0.155
0.0335
46
Rsho
0.000
0.0000
W
139
0.105
0.0279
W
850
0.112
0.1837
W
224
0.091
0.0375
6572
W
0.068
0.8021
Rsho
50
0.000
0.0000
164
Fsho
0.000
0.0000
W
398
0.126
0.0972
W
94276
0.094
16.7740
W
2683
0.105
0.5135
W
215
0.090
0.0350
W
1680
0.100
0.2931
W
23140
3.5976
0.089
410
Fsho
0.000
0 .oooo
1467
W
0.189
0.5156
207
Rsho
0.000
0.0000
W
341
0.148
0.0949
Data File
Operator
l
Name
Instrument
.
0
:
0
l
0
*
22.475
22.666
23.012
23.206
23.436
23.659
24.035
24.139
24.173
24.449
24.632
24.784
24.895
25.089
25.810
25.970
26.199
26.452
26.657
26.875
27.083
27.276
27.570
27.675
28.149
28.186
28.336
28.418
28.586
28.828
29.166
29.517
29.544
29.681
30.303
30.368
30.744
31.089
31.257
31.603
31.724
ISTD
31563
0
36733
0
6247
1792
0
0
27899
0
8783
0
0
1378
1253
0
178533
1895
7228
9392
473730
79284
2513
6578
0
2917
0
1162
55457
8713
13521
0
9458
5673
0
26346
1106
10746
24920
34180
59762
Number
:6
: 10
:
Line
Instrument
Method:
GEORGEi.MT:
Analysis
Method
: GEORGEl.My
Sample Amount
:l
:l
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
60
61
62
63
64
65
66
67
Number
Number
Vial
Injection
Sequence
5890-FID
Sample Name
: ProductionTO
Run Time Bar Code:
Acquired
on
: 25 May 99 11:28 AM
PM
Report
Created
on: 25 May 99 12:15
:
17
NOV
93
08:32
AM
Last Recalib
on
Multiplier
a
: C:\HPCHEM\l\DATA\URGENT\EPO~2953.D
Page
: OB
3470
663
6030
147
836
170
142
2586
4277
51
878
274
97
108
136
Amount
w
Rsho
W
Rsho
W
w
Fsho
Fsho
W
Rsho
W
Rsho
Rsho
W
BV
29
35932
Rsho
PV
307
762
2083
90466
16691
492
747
210
275
71
270
12410
1552
1911
1016
1342
591
1559
3799
107
1777
6088
7973
14739
w
W
W
W
W
w
w
Fsho
W
Rsho
W
W
W
w
Fsho
W
w
Fsho
w
w
w
w
w
w
0.127
0.000
0.092
0.000
0.109
0.136
0.000
0.000
0.095
0.000
0.137
0.000
0.000
0.161
0.124
0.000
0.077
0.093
0.153
0.069
0.077
0.073
0.074
0.123
0.000
0.153
0.000
0.067
0.069
0.088
0.103
0.000
0.100
0.132
0.000
0.096
0.142
0.088
0.064
0.065
0.063
0.8519
0.0000
0.9914
0.0000
0.1686
0.0484
0.0000
0.0000
0.7530
0.0000
0.2370
0.0000
0.0000
0.0372
0.0338
0.0000
4.8184
0.0511
0.1951
0.2535
12.7855
2.1398
0.0678
0.1775
0.0000
0.0787
0.0000
0.0314
1.4967
0.2352
0.3649
0.0000
0.2553
0.1531
0.0000
0.7111
0 -0299
0.2900
0.6726
0.9225
1.6129
-
R
Data File
Name
:
:
Operator
Instrument
Sample Name
'1
j Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
0
.
l
a
0
1
0
0
c
68
69
70
71
72
73
74
75
76
77
8
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
34
95
96
97
98
99
100
101
102
103
104
105
106
107
108
31.974
32.313
32.675
32.985
33.116
33.447
33.707
33.737
34.188
34.420
34.609
34.749
34.891
35.131
35.329
35.475
35.619
35.821
35.994
36.265
36.501
36.562
36.928
37.130
37.189
37.479
37.745
38.OdO
38.335
38.433
38.539
38.631
38.838
38.857
38.975
39.226
39.395
39.588
39.693
39.887
40.065
C:\HPCHEM\l\DATA\URGENT\EPOO2953.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
ProductionTO
Sequence Line
Instrument
Method:
AM
25 May 99 ii:28
Analysis
Method
PM
25 May 99 12:lS
Sample Amount
17 NOV 93 08:32 AM
ISTD Amount
1
5024
1048
3717
10060
4719
1564
0
9761
73979
11773
0
0
7121
18191
38023
7746
247196
1294
2772
2407
0
6831
1165
0
4134
10678
10169
70708
0
4926
0
20047
0
3136
47319
0
975335
3012
4326
3231
2826
611
135
423
2200
673
245
750
1143
20550
1889
202
75
1860
4226
7325
1688
73145
221
257
210
345
730
167
264
396
1928
2270
19631
282
676
205
5938
418
666
13467
249
218201
491
541
335
291
W
w
W
PV
W
W
Fsho
w
W
w
Rsho
Rsho
w
W
W
w
w
w
W
w
Fsho
w
W
Fsho
W
W
W
PV
Rsho
W
Rsho
W
Fsho
w
W
Fsho
W
w
w
w
w-
0.115
0.118
0.132
0.069
0.117
0.094
0.000
0.117
0.057
0.088
0.000
0.000
0.060
0.066
0.076
0.070
0.054
0.097
0.147
0.154
0.000
0.133
0.099
0.000
0.137
0.080
0.068
0.056
0.000
0.105
0.000
0.054
0.000
0.067
0.056
0.000
0.070
0.091
0.111
0.136
0.130
:7
: 10
:
:
GEORGEl.MTF
: GEORGE~.MTE
: 1
0.1356
0.0283
0.1003
0.2715
0.1274
0.0422
0.0000
0.2634
1.9966
0.3177
0.0000
0.0000
0.1922
0.4910
1.0262
0.2091
6.6716
0.0349
0.0748
0.0650
0.0000
0.1844
0.0315
0.0000
0.1116
0.2882
0.2744
1.9083
0.0000
0.1330
0.0000
0.5410
0.0000
0.0846
1.2771
0.0000
26.3234
0.0813
0.1168
0.0872
0.0763
*3
Data
File
Name
:
. Operator
Instrument
Sample Name
\ Run Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
Total
amount
C:\HPCHEM\l\DATA\URGENT\EPO~2953.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
ProductionTO
Sequence
Line
25 May 99
11:28 AM
Instrument
Method:
Analysis
Method
25 May 99
12:15
PM
Sample
Amount
08:32
AM
17 NOV 93
ISTD Amount
1
= 3.70519E+006
-.
: 8
: 10
:
GEORGE~.MTE
: GEORGE~.MTE
:l
l
CLOVER
RESEARCH
TECHNICAL
l
CENTRE
INFORMATION
TUNA OIL STANDARDS
0 REFERENCE LABORATORIES
l
Please, note:
GC.,calibrated against standards on a daily
basis..
Comparison
of G.C. Fatty Acid Composition
Determined
bv Clover and 2 Benchmark
Laboratories
Fatty Acid %
DHA
EPA
Erucic
l
,
l
l
Acid
Clover Standard
25.6
5.8
0.3
Leatherhead
Food R.A.
Mylnefield Research
Services
26.4
5.8
0.4
25.3
5.8
0.1
0.l
0
P
0
!tl
P
3
(D
?
0
rc
h
i.-----
--._____----
-___.--._____..
- ..- _-
-__- -. _. -. .._ _._
l
----c14.013796
162~420.059
l
4
n.
0
l
Data
File
&me
:
Operator
:
Instrument
:
Sample
Name
:
Run Time
Bar Code:
Acquired
on
:
Report
Created
on:
Last
Recalib
on
:
Multiplier
:
Sample
Info
:
k,
9.466
9.910
.421
C:\HPCEEM\l\DATA\URGENT\EPOO3585.D
OB
5890-FID
Standards2000
01 Feb 00
01 Feb 00
17 NOV 93
1
Signal-38.199
12:21
01:06
08:32
PM
PM
AM
Roche
#l
Page Number
Vial
Number
Injection
Number
Sequence
Line
Instrument
Method:
Analysis
Method
Sample
Amount
ISTD Amount
- Standard
:l
: 13
:
GEORGEl.M'I
: GEORGEl.M'I
:l
:
.
-I
l
Data File
Name
:
Operator
Instrument
Sample-Name
Run
Time Bar Code:
Acquired
on
Report
Created
on:
Last Recalib
on
:
Multiplier
Not
all
time
C:\HPCHEM\l\DATA\URGENT\EPOO3585.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
standards2000
Sequence Line
Instrument
Method:
12:21 PM
01 Feb 00
Analysis
Method
01:06 PM
01 Feb 00
Sample Amount
17 NOV 93 08:32 AM
ISTD Amount
1
reference
peaks
were
Area
Data File
Name
:
:
Operator
:
Instrument
Sample Name
:
7
Time Bar Code:
A,+ired
on
:
Report
Created
on:
Last Recalib
on
:
Multiplier
:
Sample Info
:
l
l
Sig.
0
e
l
l
e
:5
: 13
:
:
GEORGEi.
: GEORGE1.b
:l
found
Percent
Report
C:\HPC!HEM\l\DATA\URGENT\EPOO3585.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
Standards2000
Sequence Line
01 Feb 00
12:21 PM
Instrument
Method:
01 Feb 00
01:06 PM
Analysis
Method
17 NOV 93 08:32 AM
Sample Amount
1
ISTD Amount
Signal-38.199
Roche #l - Standard
1 in C:\HPCHEM\l\DATA\URGENT\EPOO3585.D
Pk#
Ret Time
Area
Height
I---I----------I----_________ 1--------------I---I-------.
7.391
1
2273
67
2
7.925
0
94
3
7.928
2660
95
4
8.369
1889
87
5
8.559
1013
155
6
8.805
1462
101
7
9.183
1430
92
8
9.628
0
91
9
9.680
1943
114
10
11.425
1402
642
11
12.476
1643
666
12
13.120
1149
353
13
13.798
97073
34330
14
13.906
0
418
15
14.022
0
95
16
14.421
1260
374
17
14.628
5771
1251
18
14.956
1305
345
19
15.526
30161
8227
20
16.581
0
213
21
16.651
4085
630
22
17.982
545869
86882
i;
Tee
Width
w
0.410
0.000
0.342
0.275
0.087
0.190
0.190
0.000
0.211
0.034
0.038
0.049
0.044
0.000
0.000
0.052
0.066
0.059
0.057
0.000
0.092
0 f 095
Fsho
W
W
W
W
W
Fsho
W
BV
PV
W
PV
Rsho
Rsho
W
W
W
W
Fsho
W
W
: 1
: 13
:
GEORGE1.M
: GEORGE1.M
:l
Area %
I---------0.0761
0.0000
0.0890
0.0632
0.0339
0.0489
0.0479
0.0000
0.0650
0.0469
0.0550
0.0385
3.2486
0.0000
0.0000
0.0422
0.1931
0.0437
1.0094
0.0000
0.1367
18.2679
1
.
71
-“I
l
0
0
l
.Data
File
Name
:
:
Operator
:
Instrument
:
Sample -Name
Run
Time Bar Code:
:
Acquired
on
Report
Created
on:
:
Last Recalib
on
:
Multiplier
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
so
51
52
53
54
55
56
57
58
59
60
61
62
63
18.229
18.446
18.632
18.811
19.117
19.334
19.447
19.560
20.018
20.059
20.576
20.618
20.879
21.150
21.695
22.452
22.490
22.683
22.971
23.120
23.249
24.333
24.716
24.876
25.051
25.163
25.283
25.482
25.682
25.896
26.067
26.256
27.085
27.306
27.495
27.883
27.957
28.201
28.316
28.388
29.176
C:\HPCHEM\l\DATA\DRGENT\EPOO358S.D
Page Number
OB
Vial
Number
S890-FID
Injection
Number
standards2000
Sequence
Line
Instrument
Method:
01 Feb 00 12:21 PM
Analysis
Method
01 Feb 00 01:06 PM
Sample Amount
17 NOV 93 08:32 AM
ISTD Amount
1
0
17930
1798
8221
129681
1892
11390
0
0
4287
0
30091
6705
36531
10233
0
22675
0
6675
0
2271
1341
163767
0
4416
2265
3864
0
329199
70889
2926
5502
1124
37385
9773
0
16209
2090
4692
3458
18553
251
3161
295
1284
23760
434
963
528
301
415
2585
431s
852
5337
1196
2129
3350
101
765
153
357
238
27006
556
746
431
539
537
55579
13440
612
783
159
8154
2041
947
2421
462
1002
795
3498
Rsho
W
w
W
W
w
W
Rsho
Fsho
w
Fsho
w
W
w
W
Fsho
w
Rsho
W
Rsho
w
PV
W
Rsho
W
w
w
Fsho
w
w
W
W
w
W
W
Fsho
W
W
w
w
Vi
0.000
0.085
0.089
0.095
0.085
0.073
0.157
0.000
0.000
0.144
0.000
0.106
0.120
0.105
0.122
0.000
0.101
0.000
0.126
0.000
0.099
0.085
0.093
0.000
0.089
0.076
0.102
0.000
0.086
0.080
0.080
0.108
0.101
0.071
0.074
0.000
0.095
0.069
0.069
0.073
0.081
:6
: 13
:
GEORGEl.M,
: GEORGE~.M
:l
0.0000
0.6000
0.0602
0.2751
4.3399
0.0633
0.3812
0.0000
0.0000
0.1435
0.0000
1.0070
0.2244
1.2225
0.3425
0.0000
0.7588
0.0000
0.2234
0.0000
0.0760
0.0449
5.4806
0.0000
0.1478
0.0758
0.1293
0.0000
11.0169
2.3724
0.0979
0.1841
0.0376
1.2511
0.3271
0.0000
0.5425
0.0699
0.1570
0.1157
0.6209
,
-
\
0
0
l
a
0
0
Data
File
Name
Operator
Instrument
Sample-Name
Run
Time
Bar
Code:
Acquired
on
Report
Created
on:
Last
Recalib
on
Multiplier
64
65
66
67
68
69
70
71
72
73
74
75
76
77
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
93
94
95
96
97
98
99
100
101
102
103
104
29.861
29.888
30.129
30.437
30.575
30.785
31.086
31.416
31.449
31.556
31.872
31.973
32.318
32.645
32.733
33.156
33.351
33.546
33.720
33.845
34.105
34.296
34.420
34.629
34.821
35.193
35.226
35.525
35.752
35.884
36.066
36.091
36.207
36.502
36.735
36.759
37.126
37.415
37.673
37.812
37.904
:
:
:
:
C:\BPCHEM\l\DATA\TJRGENT\EPOO3585.D
OB
5890-FID
Standards2000
: 01 Feb 00
01 Feb 00
: 17 NOV 93
1
12:21
01:06
08:32
0
13024
23968
6609
21982
4358
1717
0
1021
6428
6830
5186
1155
6152
0
57601
5324
2940
0
9090
12792
8054
3798
173720
2190
0
1912
9107
1798
1053
0
1880
4511
6852
0
9187
69472
2070
14984
1372
2416
PM
PM
AM
1777
2959
5765
921
5324
914
270
124
186
1557
1761
1230
229
1276
200
15436
1226
559
38
2262
3330
1764
986
46843
475
126
354
2083
218
165
234
328
1054
1848
1306
2085
19549
364
4227
445
725
Page Number
Vial
Number
Injection
Number
Sequence
Line
Instrument
Method:
Analysis
Method
Sample
Amount
ISTD Amount
Fsho
PV
VV
V-v
VV
vv
VV
Fsho
PV
w
VV
V-V
w
UV
Rsho
‘PV
VV
w
Rsho
W
vv
VV
W
W
vv
Fsho
PV
W
V-V
V-V
Fsho
V-V
w
PV
Fsho
V-V
PV
VII
PV
v-u
W
0.000
0.068
0.065
0.098
0.064
0.072
0.096
0.000
0.081
0.065
0.060
0.064
0.076
0.071
0.000
0.058
0.065
0.077
0.000
0.062
0.060
0.068
O.G59
0.058
0.071
0.000
0.077
0.066
0.117
0.086
0.000
0.081
0.064
0.057
0.000
0.066
0.056
0.080
0.056
0.049
0.052
: 7
: 13
:
GEORGEl.f<T.
: GEORGE~.~JT~
:l
0.0000
0.4359
0.8021
0.2212
0.7357
0.1458
0.0574
0.0000
0.0342
0.2151
0.2286
0.1735
0.0387
0.2059
0.0000
1.9277
0.1782
0.0984
0.0000
0.3042
0.4281
0.2695
0.1271
5.8137
0.0733
0.0000
0.0640
0.3048
0.0602
0.0352
0.0000
0.0629
0.1510
0.2293
0.0000
0.3075
2.3249
0.0693
0.5015
0.0459
0.0806
-#fh
;FEcl
_
.
File
Name
:
Operator
:
Instrument
:
:
Sample'Name
Run Time Bar Code:
Acquired
on
:
Report
Created
on:
Last Recalib
on
:
Multiplier
:
Data
105
106
107
108
109
110
111
112
113
114
l
..
Total
l
C:\HPCHEM\l\DATA\DRGENT\EP0035eS.D
Page Number
OB
Vial
Number
5890-FID
Injection
Number
Standards2000
Sequence Line
Instrument
Method:
01 Feb 00 12:21 PM
Analysis
Method
01 Feb 00
01:06 PM
Sample Amount
17 NOV 93 08:32 AM
ISTD Amount
1
38.027
38.292
38.464
38.561
38.705
39.409
39.488
39.910
40.000
40.421
amount
= 2.988123+006
36081
0
762568
6063
7040
0
1215
3095
0
1282
9706
417
168540
1596
1488
67
191
375
96
524
W
Fsho
W
W
W
Fsho
PV
w
Rsho
PBA
0.059
0.000
0.065
0.063
0.070
0.000
0.089
0.112
0.000
0.042
:8
: 13
:
GEORGE~.MTF
: GEORGE~.MTF
: 1
1.2075
0.0000
25.5200~D~~
0.2029
0.2356
0.0000
0.0407
0.1036
0.0000
0.0429
LeatherhTXd
Scicncc, Technology
and Information
for the
Food Industry Worldwide
e
Our Ref: MJD/040624/FRA
l
Structure
REPORT
Received
.
Reference:
F
e
.,
Date analysis
Method
started:
of analysis:
0
Results:
and Function
Test Report
ON
Ortwin Bode
Clover Corporation
Clover Research Centre
PO. Box 192
Caringbah
NSW 2229
AUSTRALIA
from:
l
Sample
E\REPORT/ll551
1-Mar-O0
115 5 l-99 F l-5
,
Fl =
F2 =
F3 =
F4 =
F5 =
On 14.02.2000
Borage oil #99125Al
Tuna oil #ROl
10.02;2000
Borage oil #RO3 10.02.2000
Evening primrose oil #rO2
10.02.2000
Evening primrose oil # E9912 16 10.02.2000
17.02.2000
Fatty acid profile by BS684 2.34/35 (WAS FC:4)
including internal standard and TBHQ antioxidant.
Fatty acid profile (% methyl esters, capillary column GC,
CP SIL 58 stationary phase on-column injection)
A. Calculated as % m/m without internal standard.
c14:o
C14:l
C14:UlS:O br
c15:o
-,
C15:l
Ci6:O
Cl6.1
C16:2/17:0 br
c17:o
Fl
tr
nd
nd
nd
nd
10.5
0.2
nd
nd
xF2
3.3
0.1
0.1
1.0
0.1
19.7
5.4
1.3
1.2
F3
tr
nd
nd
nd
nd
10.1
0.2
nd
nd
Page1 of 3
F4
tr
nd
nd
nd
nd
6.4
0.1
nd
nd
F5
tr
nd
nd
nd
nd
6.0
tr
nd
nd
i
l
m?
I
I
0
.
C17:l
lr
Cli3:O
C18:l
C18:2 : ::
C 18:3(n-6) (GLA)
4.3
17.5
36.8
20.9
0.3
21.4
nd
0.2
4.4
0.1
C I 8:3(n-3) (ALA)
C: 18:3 total
Cl 8:4
c2o:o
c20: 1
c20:2
C20:3
C20:4
% C20:5,N-3 (EPA)
c22:o
*
C22:l
c22:2
C22:3
C22:4
c22:s
& C22:6,n-3 (DHA)
C24:O
C24: 1
l
l
l
unknowns
I .o
5.7
14.3
2.4
0.1
0.5
0.7
0.7
0.4
I .o
3.4
15.6
38.0
24.4
0.1
0.1
1.9
9.5
70.6
10.4
0.2
10.6
nd
0.3
0.3
tr
nd
nd
nd
0.1
0.1
nd
nd
nd
nd
nd
tr
tr
0.0
tr
nd
nd
nd
0.2
2.9
nd
nd
nd
nd
nd
0.1
1.6
tr
0.4
2.0
5.8
0.3
0.4
tr
0.3
0.2
2.2
26.4
1.4
0.6
24.7
nd
0.2
4.0
tlnd
nd
nd
0.1
2.4
nd
nd
nd
nd
nd
tr
1.4
0.0
1.4
0.0
tr
1.9
7.3
74.1
9.9
0.1
10.1
nd
0.3
0.2
tr
nd
nd
nd
0.1
tr
nd
nd
nd
nd
nd
nd
tr
0.1
B. Calculated as % m/m using methyl heptadecanoate internal standard.
0
c14:o :::
C16:O
C16:l
C18:O
C18:l
C18:2 *
C18:3,n-6 (GLA)
Cl 8:3,N-3(ALA)
c2o:o
c20: 1
c20:2
c22:o
c22: 1
C24:O
C24:l
Total eluted material
l
l
tr
tr
9.7
0.2
3.9
16.1
33.8
19.2
0.2
0.2
4.0
0.1
0.2
2.6
0.1
1.5
9.8
0.2
3.3
15.2
37.1
23.8
0.1
0.2
3.9
tr
0.1
2.3
tr
1.4
tr
6.1
0.1
1.8
9.06
67.3
9.9
0.2
0.3
0.2
tr
0.1
0.1
tr
tr
tr
5.6
tr
1.7
6.7
68.3
9.1
0.1
0.3
0.1
tr
0.1
nd
nd
tr
92.0
97.5
95.3
92.3
nd = not detected
Page2 of 3
tr = trace (less than O.OS%)
NB. I have been unable to add an internal standard to the fish oil due to the complexity
of the chromatogram.
CommLats:
Samples will be disposed of one month after report date unless we are instructed
otherwise.
0
M.J. d ownes
Structure and Function
l
0
0
. -.
0
,
l
0
Page3 al 3
.t
i
to do
- -.
I
..
l
r
.-
_ _.-.-.
e Version:
4.l<iF<2iName
: 11551-2
.e Number: 1
rator
Time
Study
Channel
: NL:(lTON
:
: o/o
nstrument
AutoSampler
, Rack/Vial
---..-
Interface
Serial
# : 8037252605
: 0.00
m in.
Time
:
80.00
m in.
End Time
: 1.0000
Sampling Rate
pts/sec
-_
: 25/02/00
:
-_-
__
14:39
A/D mV Range : 1000
: A
Data Acquisition
-
Time:
24/02/00
05:45
Delay
0
Raw Data File
Result
File
Inst Method
. Proc Method
Calib Method
Set ?nce File
l
:
:
:
:
:
:
: 1.0000
: 1.0000
Sample Volume
Sample Amount
l
C:\TC4\NEWTON\F23020OM.RAW
C:\DOS\-RST2F47.RST
C:\TC$\METH SEQ\FAME from C:\DOS\-RST2F47.RST
C:\TC4\METH-SEQ\FAME.MTH
C:\TC4\METH SEQ\FAME.MTH
C:\TC4\METHISEQ\FAME.SEQ
Ul
Area Reject
Dilution
Factor
FATTY ACID METHYL ESTERS
-.
===============================================--------~-====--------========---
Fame Report
===================------------------========--------=------------------===----
l
.-
a
Area
Tim
ACea
Amount
Norm Area
SL
Component
[ainl
IuV~sl
[Norm.
II
Nama
1'1
111
----------------------------------------------------------------------------------------------------------------------------~----9.6
11.8
14.7
16.<
18.1
18 s
18.7
12.:
19.5
20.0
20.5
21.1
21-J
22 1
22.7
23 e
25 9
25
q
O.Gl
0.@3
0.03
0 02
3.25
0.01
0.02
?Ial171
:Il:ln
I9
0 Oi
O.iO
0.0:
0.01
O.YP
O.Gl
0.01
0 01
11
I
,;’
I, . I
26
’
; !‘:;
21
;‘i
”
i ! ‘, , : ]
4
::
I
14Q41
‘I
L i
27
28.:
i
Il:rG
0
.I
28 3
ir
c
79 7
29 c
30 0
3” c
l
1404
4427
5206
2aotl
530520
1279
3?49
>:,;
4917
16179
3107
2054
158014
1289
1403
11371
I320
G4 1s
3059
‘01844
IY2491!
33924
9 1I 3
0 01
0.04
0 02
1 24
1.1s
0 71
0 a‘,
0.01
0.03
0.03
0.0:
3.29
0.01
0.02
>.’
0.03
0.10
0.0:
0.01
0.98
0.01
0.01
0 07
19.73
0.06
0 “B
1.45
0 0,
0 :3
0.01
0 04
0.0:
1.2Y
I 19
a ?I
0 (1,
: 0.000000
: 1.00
BB
80 c12:o
BB
El8
BV
vv Cl4:O
VB
---
----
e
25454
11.6
4679
12.2
12.4
2551
33 8 923735
27:33
14-l
14 d 19OJ653
152729
35 0
1'94.3
15 4
2625
15.7
107s
35 9
209555
16.5
102132
37.1
J1649
17.5
18.2
lPO40
1%. 4
15219
75067
18.6
iI
19.4
1059
19.8
65564
40.4
41.0
21147
120550
41.2
41.4
14611
41.0
2041
1821
47 '
4
28750
42.7
41215
i--J911
41.5
14612
41.6
44.1
31703%
15811
44.9
46.0
61701
46.8
914590
41835
41.1
1427
47.9
15608
40.2
16272
40.5
49.0
11221
168%
49.6
116%
50.9
52.1
48440
4164
51.4
54.3
IT-J18
55.3
IS1866
56.7
1525
58.7
226110
60.5 425842%
60.9
91511
61.7
6264
62.2
lo515
62.8
15359
c 5
1970
. 2
2112
74.0
511%
70.4
6R%:
l
0
l
l
0
l
0.16
0 01
0.0)
5.13
0 11
11 RI
2.19
0.11
0.0:
0.02
1.10
0 66
0.44
0.11
0.09
0.41
0.71
0.01
0.41
0.17
0.75
0.09
0.01
0.01
0.1%
0.26
0.11
0.09
1.97
0.10
0.18
5.80
0.2J
0.02
0.22
0.10
0.07
0.01
0.02
0.10
0.01
0.23
2.1%
0.02
1.41
26.41
0.57
0.04
0.07
0.10
0.02
0.01
0.01
0.04
-0 I !
‘I I)1
,) . .
.I ,*
n 03
;, d .;
5 13
;I I7
II
++>
2.19
@ I!
0 0:
0.0:
1. \u
t,. !*‘i
0.44
0.11
0.09
0.47
0.73
0.01
0.4;
0.17
.0.75
so9
0.01
0.01
0.18
0.26
0.17
0.09
1.97
0.10
0.1%
5.80
0.21
0.02
0.22
0.10
0.07
0.01
0.02
0.10
0.01
0.21
2.18
0.02
1.41
26.41
0.57
0.04
0.07
0.10
0.02
2:::
0.04
“II
urr
‘IV
e r.
0v
vB
MC
LY
Yt
“V
‘It
EV
vi3
RP
R”
VU
EV
YV
1 / I
I
“18
(I
C!%
I
i In.?
(1441
ciLMee+
VB Cl%:lln-11
BB W
B@
BE C2O:O
BV
vv
va C2O:l
ss BEi
ov C2O:L
V% IS.,
BV
ii
5
K ctoBB C22:O
BV
vv
vv
VB C22:l
Be
BB M
BB 11.1
BV
VB c2:u
SB~1~c: i
ss
88 C24:O
-BE C22:6
EV C24:l
'IV
va
RR
en
OB
88
\;:f;
/
;:;; i/
:;#Q
VV
0.03
0.01
O.Gl
0.1R
0.10
0.18
5.80
/
;;;;
,,-;/
0.1
d
0.
0.
0.02
0.10
0.01
0.:1
2.1% s
0.02
1.41 J
26.41v
0.51
c.c4
O.OJ
0.10
0.0:
0.01
0.01
O.tJ4
ti
4
J
_--_---------__-________________________---------------------------------------------------------------------------------------2e407
l
100.00
1llll
3OO.OG
0
Chromatogram
l
-i
IP
i
l
I
l
.
Cl8:3
Cl 8:4
l
“I 5
c20:
c22:
4
c22:1
i-r---.-__.
-.- ___ -z.c------_--.
--.
eL-?L
I!3
t
.. 34
32
36
37
38
Mylnefield
Research
services Ltd.
The Lipid Analysis Unit,
Mylneficld, Invergowrk, Dundce DD2
MRSLUW00\197
SDA, Scotland
(Continued)
l
0
Concentration
Concentration
Concentration
of AA as Free Fatty Acid
of EPA as Free Fatty Acid
of DHA as Free Fatty Acid
15 mg/g Oil
43 mg/g Oil
185 mg/g Oil
y=Jm-
OuncarrAdarn
Laboratory Technician
C. Reid C.Chem MRSC
Senior Analytkal
Chemist
I
.
The Lipid Analysis Unit,
,Mylnefieid, Invergo wm, Dundce
Designation
Submitted
a
of sample -
SDA, Scotland
DD2
Marine Oil
Batch No. R01
Clover Corporation
by -
Our number -
MRS LU/2000/197
Your Order number -
3105
f al& acid profile (%)
0
0
l
l
14:o
150
16:O
16:l
1622
1810
l&l
l8:2
183
78:3
18:4(n-3)
20:o
2O:l
20:2(n-6)
20:3(n-6)
20:3(n-3)
20:4(n-8)
20:4(n-3)
20:5(n-3)
22:o
22:l
22:5(n-3)
22:5(n-3)
24:0
2411
myristic
pentadecanoic
palmitic
hexadecenoic
hexadecadienoic
steafic
oleic
linoleic
y-linolenic
u-linolenic
octadecatetraenoic
icosanoic
icosenoic
icosadienoic
dihomo-y-linoienic
ioosatrienoic
arachidonkz
icosatetraenoic
icosaperitaenoic
dooosanoic
docosenoic
docosapentaenoic
docosahexaenoic
tetracosanoic
tetracosenoic
minor components
Analysis carried out on a capillary column
‘\
3.3
1.1
18.9
5.2
0.3
5.6
13.9
1.3
0.4
0.5
0.8
0.4
1.1
0.2
0.1
0.1
2.0
0.4
5.8
0.3
O.-l
1.2
25.3
0.2
0.5
11.0
Material
product
Name: Hi-DHA
Not Classified as Hazardous
COMPANY
Safety Data Sheet
0 il
Issued Date. 17’” November
according to criteria of Worksafe
1999
Australia
1
DETAILS
Company Name
Address
Emergency Tel.
Tel/Fax
Clover Corporation
LimItedI
Nu-Mega Lipids Pry Ltd
31 Pinnacle Road, Altona North Vtctona 3025
Australia
PO Box 11 11, Altona Gate Victoria 3025
Australia
0418 994744
Fax: 61 3 9369 8900
Ph: 61 3 9369 4774
IDENTIFICATION
a
Tuna Oil with a high content of Long Chain
Polyunsaturated Fatty Acids (LCPs or LCPUFAs)
including DHA ( DocosaHexaenoic Acid )
Edible Oil refined from selected species of the tuna fish
family. Product Codes 700 1 to 9099
Hazardous Ingredients
None
Product Use
Nutritional supplement or functional food ingredient
UN Number
None allocated
HAZCHEM Number
Not applicable
Dangerous Goods Class/Subsidiary Risk
Not applicable
Poison Schedule Number
Not applicable
CAS Number
None allocated
Product Name
0
Physical Data
Appearance
Vapour Pressure
Specific Gravity
Flamm. Limit LELKJEL
Flash point *
Solubility
HEALTH
HAZARD
A pale yellow liquid with faint fish odour
Not applicable
0.92 - 0.94
Not applicable
approx.260”C
Not soluble in water, soluble in acetone/hexane
INFORMATION
1
I
Health Effects
The product might be an irritant to the eyes and may be absorbed through the skin.
Threshold Limit Value
Not applicable
Toxicity
Food Grade
First Aid
Skin
Eyes
Ingestion
inhalation
Wash with soap and water
Flush with Water
Edible, Food Grade
Minimise risks through ventllatlon (otls/fats at high
temperatures may produce gaseous products of acroleln
variety)
a
Material
Nme:Hi-DHA
a
oil
Issued Date: 171hNovember
Product
Not Classified as Hazardous according to criteria of Worksafe Australia
Other Health Hazard
PRECAUTIONS
0
Safety Data Sheet
Information
1999
!
I
FOR USE
Hazardous Reactions
Pol_ymerisationnot likely to occur under normal conditions
Engineering Controls
On prolonged exposure to air and if in contact with
absorbent combustible material, the product may self-ignite
Conditions to Avoid
Prolonged exposure to air/oxygen
High temperatures near flash point
Incompatability
(Materials to avoid)
Strong oxidising agents
Hazardous Decomposition
Products
Secondary oxidation decomposition products
eg. acrolein
Personal Protection
0
I
In presenceof fish oil mists, use respiratory mask
For hot oil, use neoprene gloves
Use goggles for hot oil
Rubber boots and apron for hot oils
Respiratory Protection
Skin Protection
Eye Protection
Others
1 SAFE HANDLI-NG
INFORMATION
Storage and Transport
0
Precautions to be taken in
Handling aqd Storing
0
Other precautions
0
Store cool, dry and away from products with a strong or
foreign odour. If stored in tanks the use of nitrogen
blanketing is advised; incorporation and contact with iron
should be avoided. We recommend storing in sealed
containers ideally plastic or epon coated drums.
Store below ambient temperature. Protect from direct
sunlight. Keep away from heat, sparks and fire.
At times oil-soaked materials may spontaneously cornbust.
Do not allow absorbent material to accumulate in closed
conditions when exposed to air.
Spills and Disposal
Minor
0
Major
Wipe or mop up spilled oil. Contain rags and dispose of in
tire-proof bins to prevent self-ignition.
Absorb or contain with clay or sand. Destroy by
incineration with off-gas scrubbers. Contaminated
absorbent may be landfilled.
Material
Safety Data Sheet
Issued Date. I 71hNovember \ 999
Product ~me: Hi-DHA
oil
Not Classified as Hazardous according to criteria of Worksafe Australia
a
Since the density of oil is less than water, it will float on
the surface. The oil can then be taken off and disposed
according to regulattons.
Disposal of this material should be undertaken by a
registered chemical disposal company.
Spillage on Water
Disposal
0
Fire/Explosion
Hazard
Extinguishing
Media
Extinguishing
Media to Avoid
Special Exposure Hazards
0
Foams, Carbon Dioxide, Inert Powder
Water
Fine oil mists may be hazardous on prolonged heating at
high temperature. Gaseous decomposition components of
1
I
1
acrolein variety may occur.
l
Protection
Against
Fire
OTHER
INFORMATION
Standard, the oil floats and spreads on the surface of water
i
Environ. Protection
Packaging
Avoid contaminating waterways. Fully biodegradable.
As required by the National Code of Practice for the
Labeling of Workplace Substances.
As required by the Standard for the Uniform Scheduling of
Drugs and Poisons
Contact
Business Hours: Mr. Robert Anderson, Tel: 61 3 9369 8899
After Hours: Tel: 61 3 9809 0075
IMPORTANT
ADVICE:
This MSDS summarises our best knowledge of the health and safety hazard information of the
product and how to safely handle and use the product in the workplace. Each user should read
this MSDS and consider the information in the context of how the product will be handled and
used in the workblace including its use in conjunction with other products. If clarification or
further information is needed to ensure that an appropriate risk assessment can be made, the user
should contact Clover Corporation Limited. Our responsibility for products sold are subject to
our standard terms and conditions, a copy of which is available on request.
l
The information has been obtained from sources believed to be reliable and accurate but has not
no representation
been independently verified by Clover Corporation Limited. Accordingly,
or warranty,
express or implied,
with respect to merchantability
and fitness
particular
purpose is made with respect to the information contained herein.
End of Report
l
for
a
Material
Driphorm
Product Name
Safety Data Sheet
Hi-DH,4
Bake
Issued Date. 17”’ No\ ernbcr 90
DlOl
Product code:
Not Classified as Hazardous according to criteria of Worksafe Australia
0
COMPANY
DETAILS
Company Name
Address
a
Emergency Tel.
Tel/Fax
Clover Corporation Limrted
3 1 Pinnacle Road, Altona North Victoria
3075
Australia
PO Box 1111, Altona Gate Victoria
3025
Australia
0418994744
Fas: 61 3 9369 8900
Ph: 61 3 9369 8899
1
I
IDENTIFICATION
Product Name
l
Driphotm Hi-DHA Bake Product Code- D 10 1
Spray dried powder containing 25% Hi-DHA Tuna Oil.
microencapsulated
in a matrix of Sodium Casetnate
Modified Starch and natural food grade antioxidants.
None
Hazardous Ingredients
Nutritional
Product Use
UN Number
HAZCHEM Number
Dangerous Goods Class/Subsidiary Risk
Poison Schedule Number
CAS Number
l
supplement, Functional
None allocated
Not applicable
Not applicable
Not applicable
None allocated
Food ingredient
/
Physiical Data
Appearance
l
Vapour Pressure
Specific Gravity
Flamm. Limit LELKJEL
Flash point
-..:
l
:,i.-:
and
Free flowing light tan coloured powder with bland odour and
flavour.
Not applicable
Not applicable
Not applicable
Not applicable
r
HEALTH
HAZARD
i
I
1
INFORMATION
Health Effects
The product might be an irritant to the eyes and may be absorbed through the skin.
Not applicable
Threshold Limit Value
Food Grade
Toxicity
First Aid
Skin
Eyes
Ingestion
Inhalation
Wash with soap and water
Flush with Water-particulates may scratch eye surfaces
Edible, Food Grade
Minimise risks through ventilation , may cause lmtatlon.
there are breathing dtfficulties, seek medical advice
If
t
Material
ProductName: Driphorm
Safety Data Sheet
Hi-DHA
Bake
Issued Date
1 7’h Vovcmber 99
DlOl
Product code:
Not Classified as Hazardous accordmg to criteria of Worksafe Australia
l
1 Other Health Hazard Information
1 PRECAUTIONS
l
Hazardous
l
FOR USE
Powder and dust clouds are susceptible
explosion in confined spaces.
Reactions
Engineering Controls
Ventilation/
Conditions to Avoid
High temperatures , sources of
maximise shelf life avoid prolonged
Incompatability
Not applicable
(Materials
dust extra&on
ignition and water To
exposure to air/oxygen
to avoid)
Hazardous Decomposition
Products
l
to fire and possible
Not applicable
I
I
1 Personal Protection
Respiratory Protection
If ventilation is inadequate or powdered
for long periods, use dust mask
Skin Protection
Not applicable
Eye Protection
Safety glasses if product handling
0
! SAFE HANDLING
l
I Storage
causes dusting.
I
INFORMATION
apd Transport
Precautions to be taken in
Handling and Storing
l
product is handled
Other precautions
Store cool, dry and away from products with a strong or
foreign odour. We recommend storing in sealed containers
Avoid contact with moisture.
Store below ambient temperature. Protect from direct
sunlight. Keep away from heat, sparks and fire.
l
Spills and Disposal
l
l
Spills
Vacuum or scoop into suitable container, then sweep area
and wash with water. Recovered product IS not suitable for
human consumption.
Disposal
Comply
with appllcablc
waste disposal regulations.
0
Material
product
l
Name:
Driphorm
Safety Data Sheet
Hi-DHL4 Bake
Issued Date: 17’hNovember 99
Product code: DlOl
Not Classified as Hazardous according to criteria of Worksafe Australia
Fire/Explosion
Extinguishing
Protection
1 OTHER
Hazard
Media
Against
Fire
Water, Foams, Carbon Dioxide, Dry chemical
Typical combustion products are carbon droxide and carbon
monoxide
INFORMATION
Environ. Protection
Avoid contaminating waterways. Fully biodegradable.
Packaging
As required by the National Code of Practice for the
Labeling of Workplace Substances.
As required by the Standard for the Uniform Scheduling of
Drugs and Poisons
Contact
Business Hours: Mr. Robert Anderson, Tel: 61 3 9369 SS99
After Hours: Tel: 61 3 9809 0075
IMPORTANT
ADVICE:
This MSDS summarises our best knowledge of the health and safety hazard information of the
product and how to safely handle and use the product in the workplace. Each user should read this
MSDS and consider the information in the context of how the product will be handled and used in
the workplace including its use in conjunction with other products. If clarification or further
information is needed to ensure that an appropriate risk assessment can be made, the user should
contact Clover Corporation Limited. Our responsibility for products sold are subject to our
standard terms and conditions, a copy of which is available on request.
The information has been obtained from sources believed to be reliable and accurate but has not
been indepepdently verified by Clover Corporation Limited. Accordingly,
no representation
or
warranty,
express or implied, with respect to merchantability
and fitness for a particular
purpose is made with respect to the information
contained herein.
. . End of Report.