16 June 2015 Work Order: 1506024 Price: $1,610.00 Paul J. Knoerr

MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
16 June 2015
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Work Order: 1506024
Price: $1,610.00
Paul J. Knoerr
MDEQ-RRD-GRAND RAPIDS
350 Ottawa Ave. NW, Unit 10
Grand Rapids, MI 49503-2341
RE: FORMER BELDING PRODUCTS
I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods
approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .
Sincerely,
George Krisztian
Laboratory Director
Lab Work Order # 1506024
Page
1 of1 31
Page
of 32
Michigan Department of Environmental Quality Analytical Testing Report
Work Order:
1506024
6/16/2015 10:58
Report Date:
MDEQ-RRD-GRAND RAPIDS
Client:
Paul J. Knoerr
Attention:
Project Name:
FORMER BELDING PRODUCTS
34000083
Project Number:
Sample Number
Sample ID
Sample Depth
Date Collected
Date Received
Analyte
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofluorobenzene
Bromoform
Bromomethane
Target Detection Drinking Water
Limit (TDL)
Criteria (DWC)
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Method
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
1
1
1
1
1
1
NA
1
NA
5
1
NA
0
1
1
1
1
1
1
25
50
5
50
50
2
1
1
NA
1
NA
1
5
77
200
9
5
880
7
NA
42
NA
70
63
NA
0
600
5
5
72
7
75
13,000
1,000
260
730
1,800
3
5
18
NA
80
NA
80
10
Groundwater
Surface Water
Interface
Criteria (GSIC)
Groundwater
Volatilization to
Indoor Air
Inhalation
Criteria (GVIIC)
Organics-Volatiles
ID
15,000
89
660,000
78
12,000
330
17,000
740
1,000,000
130
200
NA
NA
NA
8,300
NA
NA
99
300,000
17
56,000
NA
NA
6
2,400
13
160,000
360
9,600
230
16,000
45
61,000
28
18,000
17
16,000
2,200
240,000,000
ID
4,200,000
19
25,000
1,700
1,000,000,000
ID
20,000,000
2
34,000
200
5,600
NA
180,000
NA
NA
ID
4,800
NA
NA
ID
470,000
35
4,000
1506024-01
MW1
1506024-02
MW2
1506024-03
MW2D
1506024-04
MW3
1506024-05
MW4S
1506024-06
MW4D
Rule 57 Final
Acute Value
(FAV)
6/2/2015
6/3/2015
6/2/2015
6/3/2015
6/2/2015
6/3/2015
6/2/2015
6/3/2015
6/2/2015
6/3/2015
6/2/2015
6/3/2015
ID
1,600
1,800
6,400
13,000
2,300
NA
NA
NA
850
310
NA
280
240
16,000
4,000
810
200
210
40,000
ID
340
30,000
ID
1,200
1,900
NA
NA
ID
NA
ID
640
<1.0
<1.0
<1.0
<1.0
3
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
49
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
48.8
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
49.9
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
1.3
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
48.5
<1.0
<5.0
<1.0
6.1
<1.0
<1.0
9.3
2.3
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
48
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
48.2
<1.0
<5.0
Sample Number
Sample ID
Sample Depth
Date Collected
Date Received
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
Toluene-d8
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
Target Detection Drinking Water
Limit (TDL)
Criteria (DWC)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
5
1
1
5
1
5
1
NA
NA
5
5
5
10
5
1
5
5
5
NA
NA
5
5
5
1
1
NA
NA
1
1
1
50
5
1
90
1
NA
1
NA
NA
1
1
1
800
5
100
430
80
260
70
NA
NA
80
80
1,700
10
30
74
49
7
800
NA
NA
5
40
520
80
80
NA
NA
80
100
80
3,900
190
5
95
790
NA
100
NA
NA
5
2,600
2
Groundwater
Surface Water
Interface
Criteria (GSIC)
Groundwater
Volatilization to
Indoor Air
Inhalation
Criteria (GVIIC)
Rule 57 Final
Acute Value
(FAV)
ID
45
25
1,100
350
ID
620
NA
NA
ID
NA
ID
ID
ID
18
ID
7
28
NA
NA
1,500
7,100
11
ID
ID
NA
NA
ID
80
ID
NA
NA
60
11,000
270
NA
1,500
NA
NA
200
NA
13
250,000
370
210,000
5,700,000
28,000
8,600
93,000
NA
NA
14,000
ID
220,000
61,000,000
8,000
110,000
2,900,000
27,000
56,000
NA
NA
220,000
47,000,000
31,000
ID
ID
NA
NA
ID
170,000
ID
1,000,000,000
260,000
25,000
6,900,000
530,000
NA
85,000
NA
NA
2,200
1,100,000
1,100
ID
1,400
450
20,000
11,000
ID
11,000
NA
NA
ID
NA
ID
ID
ID
320
ID
210
500
NA
NA
17,000
420,000
200
ID
ID
NA
NA
ID
2,900
ID
NA
NA
2,900
150,000
2,600
NA
28,000
NA
NA
3,500
NA
17,000
1506024-01
MW1
1506024-02
MW2
1506024-03
MW2D
1506024-04
MW3
1506024-05
MW4S
1506024-06
MW4D
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
15
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
50
<1.0
<1.0
<5.0
<1.0
<1.0
110
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
8
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
49.6
<1.0
<1.0
<5.0
<1.0
<1.0
15
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
49.8
<1.0
<1.0
<5.0
<1.0
<1.0
<1.0
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
46
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
50
<1.0
<1.0
<5.0
<1.0
<1.0
2.2
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
130
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
50.1
<1.0
<1.0
<5.0
<1.0
<1.0
260
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
50.4
<1.0
<1.0
<5.0
<1.0
<1.0
<1.0
Sample Number
Sample ID
Sample Depth
Date Collected
Date Received
Dibromofluoromethane
Target Detection Drinking Water
Limit (TDL)
Criteria (DWC)
ug/L
8260
NA
NA
Grey indicates contaminant was detected.
Yellow indicates contaminant exceeds DWC.
Blue indicates contaminant exceeds GSIC.
Green indicates contaminant exceeds both DWC and GSIC.
Orange indicates contaminant exceeds one or more criteria; GVIIC and/or FAV.
“ID” means insufficient data to develop criterion.
“NA” means a criterion or value is not available or, in the case of background, not applicable.
“NLV” means hazardous substance is not likely to volatilize under most conditions.
Letters in criteria columns refer to Footnotes of the Criteria/RBSLs tables.
Groundwater
Surface Water
Interface
Criteria (GSIC)
Groundwater
Volatilization to
Indoor Air
Inhalation
Criteria (GVIIC)
Rule 57 Final
Acute Value
(FAV)
NA
NA
NA
1506024-01
MW1
1506024-02
MW2
1506024-03
MW2D
1506024-04
MW3
1506024-05
MW4S
1506024-06
MW4D
6/2/2015
6/3/2015
48
6/2/2015
6/3/2015
45.8
6/2/2015
6/3/2015
47.1
6/2/2015
6/3/2015
46.7
6/2/2015
6/3/2015
47
6/2/2015
6/3/2015
46.6
Michigan Department of Environmental Quality Analytical Testing Report
Work Order:
1506024
6/16/2015 10:58
Report Date:
MDEQ-RRD-GRAND RAPIDS
Client:
Paul J. Knoerr
Attention:
Project Name:
FORMER BELDING PRODUCTS
34000083
Project Number:
Sample Number
Sample ID
Sample Depth
Date Collected
Date Received
Analyte
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofluorobenzene
Bromoform
Bromomethane
Target Detection Drinking Water
Limit (TDL)
Criteria (DWC)
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Method
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
1
1
1
1
1
1
NA
1
NA
5
1
NA
0
1
1
1
1
1
1
25
50
5
50
50
2
1
1
NA
1
NA
1
5
77
200
9
5
880
7
NA
42
NA
70
63
NA
0
600
5
5
72
7
75
13,000
1,000
260
730
1,800
3
5
18
NA
80
NA
80
10
Groundwater
Surface Water
Interface
Criteria (GSIC)
Groundwater
Volatilization to
Indoor Air
Inhalation
Criteria (GVIIC)
Organics-Volatiles
ID
15,000
89
660,000
78
12,000
330
17,000
740
1,000,000
130
200
NA
NA
NA
8,300
NA
NA
99
300,000
17
56,000
NA
NA
6
2,400
13
160,000
360
9,600
230
16,000
45
61,000
28
18,000
17
16,000
2,200
240,000,000
ID
4,200,000
19
25,000
1,700
1,000,000,000
ID
20,000,000
2
34,000
200
5,600
NA
180,000
NA
NA
ID
4,800
NA
NA
ID
470,000
35
4,000
1506024-07
MW6
1506024-08
MW7
1506024-09
MW8
1506024-10
MW9
1506024-11
MW10
1506024-12
MW11
Rule 57 Final
Acute Value
(FAV)
6/2/2015
6/3/2015
6/2/2015
6/3/2015
6/2/2015
6/3/2015
6/2/2015
6/3/2015
6/2/2015
6/3/2015
6/2/2015
6/3/2015
ID
1,600
1,800
6,400
13,000
2,300
NA
NA
NA
850
310
NA
280
240
16,000
4,000
810
200
210
40,000
ID
340
30,000
ID
1,200
1,900
NA
NA
ID
NA
ID
640
<1.0
7.4
<1.0
<1.0
<1.0
1.6
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
48.9
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
47.9
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
43
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
48.8
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
0.97
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
49.1
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
48.1
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
47.8
<1.0
<5.0
Sample Number
Sample ID
Sample Depth
Date Collected
Date Received
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
Toluene-d8
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
Target Detection Drinking Water
Limit (TDL)
Criteria (DWC)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
5
1
1
5
1
5
1
NA
NA
5
5
5
10
5
1
5
5
5
NA
NA
5
5
5
1
1
NA
NA
1
1
1
50
5
1
90
1
NA
1
NA
NA
1
1
1
800
5
100
430
80
260
70
NA
NA
80
80
1,700
10
30
74
49
7
800
NA
NA
5
40
520
80
80
NA
NA
80
100
80
3,900
190
5
95
790
NA
100
NA
NA
5
2,600
2
Groundwater
Surface Water
Interface
Criteria (GSIC)
Groundwater
Volatilization to
Indoor Air
Inhalation
Criteria (GVIIC)
Rule 57 Final
Acute Value
(FAV)
ID
45
25
1,100
350
ID
620
NA
NA
ID
NA
ID
ID
ID
18
ID
7
28
NA
NA
1,500
7,100
11
ID
ID
NA
NA
ID
80
ID
NA
NA
60
11,000
270
NA
1,500
NA
NA
200
NA
13
250,000
370
210,000
5,700,000
28,000
8,600
93,000
NA
NA
14,000
ID
220,000
61,000,000
8,000
110,000
2,900,000
27,000
56,000
NA
NA
220,000
47,000,000
31,000
ID
ID
NA
NA
ID
170,000
ID
1,000,000,000
260,000
25,000
6,900,000
530,000
NA
85,000
NA
NA
2,200
1,100,000
1,100
ID
1,400
450
20,000
11,000
ID
11,000
NA
NA
ID
NA
ID
ID
ID
320
ID
210
500
NA
NA
17,000
420,000
200
ID
ID
NA
NA
ID
2,900
ID
NA
NA
2,900
150,000
2,600
NA
28,000
NA
NA
3,500
NA
17,000
1506024-07
MW6
1506024-08
MW7
1506024-09
MW8
1506024-10
MW9
1506024-11
MW10
1506024-12
MW11
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
140
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
13
<5.0
<1.0
50.5
<1.0
<1.0
<5.0
2900
<1.0
1.4
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
50.6
<1.0
<1.0
<5.0
<1.0
<1.0
<1.0
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
5.1
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
50.1
1.5
<1.0
<5.0
1.1
<1.0
13
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
49.4
<1.0
<1.0
<5.0
<1.0
<1.0
<1.0
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
51.1
<1.0
<1.0
<5.0
<1.0
<1.0
1.5
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
49.6
<1.0
<1.0
<5.0
<1.0
<1.0
<1.0
Sample Number
Sample ID
Sample Depth
Date Collected
Date Received
Dibromofluoromethane
Target Detection Drinking Water
Limit (TDL)
Criteria (DWC)
ug/L
8260
NA
NA
Grey indicates contaminant was detected.
Yellow indicates contaminant exceeds DWC.
Blue indicates contaminant exceeds GSIC.
Green indicates contaminant exceeds both DWC and GSIC.
Orange indicates contaminant exceeds one or more criteria; GVIIC and/or FAV.
“ID” means insufficient data to develop criterion.
“NA” means a criterion or value is not available or, in the case of background, not applicable.
“NLV” means hazardous substance is not likely to volatilize under most conditions.
Letters in criteria columns refer to Footnotes of the Criteria/RBSLs tables.
Groundwater
Surface Water
Interface
Criteria (GSIC)
Groundwater
Volatilization to
Indoor Air
Inhalation
Criteria (GVIIC)
Rule 57 Final
Acute Value
(FAV)
NA
NA
NA
1506024-07
MW6
1506024-08
MW7
1506024-09
MW8
1506024-10
MW9
1506024-11
MW10
1506024-12
MW11
6/2/2015
6/3/2015
47.5
6/2/2015
6/3/2015
46
6/2/2015
6/3/2015
46.7
6/2/2015
6/3/2015
47.2
6/2/2015
6/3/2015
46.3
6/2/2015
6/3/2015
45.9
Michigan Department of Environmental Quality Analytical Testing Report
Work Order:
1506024
6/16/2015 10:58
Report Date:
MDEQ-RRD-GRAND RAPIDS
Client:
Paul J. Knoerr
Attention:
Project Name:
FORMER BELDING PRODUCTS
34000083
Project Number:
Sample Number
Sample ID
Sample Depth
Date Collected
Date Received
Analyte
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromofluorobenzene
Bromoform
Bromomethane
Target Detection Drinking Water
Limit (TDL)
Criteria (DWC)
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Method
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
1
1
1
1
1
1
NA
1
NA
5
1
NA
0
1
1
1
1
1
1
25
50
5
50
50
2
1
1
NA
1
NA
1
5
77
200
9
5
880
7
NA
42
NA
70
63
NA
0
600
5
5
72
7
75
13,000
1,000
260
730
1,800
3
5
18
NA
80
NA
80
10
Groundwater
Surface Water
Interface
Criteria (GSIC)
Groundwater
Volatilization to
Indoor Air
Inhalation
Criteria (GVIIC)
Organics-Volatiles
ID
15,000
89
660,000
78
12,000
330
17,000
740
1,000,000
130
200
NA
NA
NA
8,300
NA
NA
99
300,000
17
56,000
NA
NA
6
2,400
13
160,000
360
9,600
230
16,000
45
61,000
28
18,000
17
16,000
2,200
240,000,000
ID
4,200,000
19
25,000
1,700
1,000,000,000
ID
20,000,000
2
34,000
200
5,600
NA
180,000
NA
NA
ID
4,800
NA
NA
ID
470,000
35
4,000
1506024-13
MW12
1506024-14
MW13
Rule 57 Final
Acute Value
(FAV)
6/2/2015
6/3/2015
6/2/2015
6/3/2015
ID
1,600
1,800
6,400
13,000
2,300
NA
NA
NA
850
310
NA
280
240
16,000
4,000
810
200
210
40,000
ID
340
30,000
ID
1,200
1,900
NA
NA
ID
NA
ID
640
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
49.1
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<1.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<5.0
<5.0
<5.0
<20
<5.0
<5.0
<1.0
<1.0
<1.0
<1.0
49.9
<1.0
<5.0
Sample Number
Sample ID
Sample Depth
Date Collected
Date Received
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
Toluene-d8
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
Target Detection Drinking Water
Limit (TDL)
Criteria (DWC)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
8260
5
1
1
5
1
5
1
NA
NA
5
5
5
10
5
1
5
5
5
NA
NA
5
5
5
1
1
NA
NA
1
1
1
50
5
1
90
1
NA
1
NA
NA
1
1
1
800
5
100
430
80
260
70
NA
NA
80
80
1,700
10
30
74
49
7
800
NA
NA
5
40
520
80
80
NA
NA
80
100
80
3,900
190
5
95
790
NA
100
NA
NA
5
2,600
2
Groundwater
Surface Water
Interface
Criteria (GSIC)
Groundwater
Volatilization to
Indoor Air
Inhalation
Criteria (GVIIC)
Rule 57 Final
Acute Value
(FAV)
ID
45
25
1,100
350
ID
620
NA
NA
ID
NA
ID
ID
ID
18
ID
7
28
NA
NA
1,500
7,100
11
ID
ID
NA
NA
ID
80
ID
NA
NA
60
11,000
270
NA
1,500
NA
NA
200
NA
13
250,000
370
210,000
5,700,000
28,000
8,600
93,000
NA
NA
14,000
ID
220,000
61,000,000
8,000
110,000
2,900,000
27,000
56,000
NA
NA
220,000
47,000,000
31,000
ID
ID
NA
NA
ID
170,000
ID
1,000,000,000
260,000
25,000
6,900,000
530,000
NA
85,000
NA
NA
2,200
1,100,000
1,100
ID
1,400
450
20,000
11,000
ID
11,000
NA
NA
ID
NA
ID
ID
ID
320
ID
210
500
NA
NA
17,000
420,000
200
ID
ID
NA
NA
ID
2,900
ID
NA
NA
2,900
150,000
2,600
NA
28,000
NA
NA
3,500
NA
17,000
1506024-13
MW12
1506024-14
MW13
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
1
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
49.3
<1.0
<1.0
<5.0
15
<1.0
<1.0
6/2/2015
6/3/2015
<1.0
<1.0
<1.0
<5.0
<1.0
<5.0
70
<1.0
<5.0
<1.0
<1.0
<5.0
<5.0
<5.0
<1.0
<5.0
<5.0
<1.0
<2.0
<1.0
<5.0
<1.0
<5.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<1.0
<50
<5.0
<1.0
<5.0
<1.0
49.6
2.9
<1.0
<5.0
9.7
<1.0
9.2
Sample Number
Sample ID
Sample Depth
Date Collected
Date Received
Dibromofluoromethane
Target Detection Drinking Water
Limit (TDL)
Criteria (DWC)
ug/L
8260
NA
NA
Grey indicates contaminant was detected.
Yellow indicates contaminant exceeds DWC.
Blue indicates contaminant exceeds GSIC.
Green indicates contaminant exceeds both DWC and GSIC.
Orange indicates contaminant exceeds one or more criteria; GVIIC and/or FAV.
“ID” means insufficient data to develop criterion.
“NA” means a criterion or value is not available or, in the case of background, not applicable.
“NLV” means hazardous substance is not likely to volatilize under most conditions.
Letters in criteria columns refer to Footnotes of the Criteria/RBSLs tables.
Groundwater
Surface Water
Interface
Criteria (GSIC)
Groundwater
Volatilization to
Indoor Air
Inhalation
Criteria (GVIIC)
Rule 57 Final
Acute Value
(FAV)
NA
NA
NA
1506024-13
MW12
1506024-14
MW13
6/2/2015
6/3/2015
47.9
6/2/2015
6/3/2015
48.2
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
MDEQ-RRD-GRAND RAPIDS
350 Ottawa Ave. NW, Unit 10
Grand Rapids MI, 49503-2341
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Project: FORMER BELDING PRODUCTS
Site Code: 34000083
Project Manager: Paul J. Knoerr
Reported:
06/16/2015
Analytical Report for Samples
Sample ID
Laboratory ID
Matrix
Date Sampled
Date Received
MW1
1506024-01
Water
06/02/2015
06/03/2015
MW2
1506024-02
Water
06/02/2015
06/03/2015
MW2D
1506024-03
Water
06/02/2015
06/03/2015
MW3
1506024-04
Water
06/02/2015
06/03/2015
MW4S
1506024-05
Water
06/02/2015
06/03/2015
MW4D
1506024-06
Water
06/02/2015
06/03/2015
MW6
1506024-07
Water
06/02/2015
06/03/2015
MW7
1506024-08
Water
06/02/2015
06/03/2015
MW8
1506024-09
Water
06/02/2015
06/03/2015
MW9
1506024-10
Water
06/02/2015
06/03/2015
MW10
1506024-11
Water
06/02/2015
06/03/2015
MW11
1506024-12
Water
06/02/2015
06/03/2015
MW12
1506024-13
Water
06/02/2015
06/03/2015
MW13
1506024-14
Water
06/02/2015
06/03/2015
Qualifier
Notes and Definitions
X
Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene
have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.
T
Reported value is less than the reporting limit (RL). Result is estimated.
A05
Result and reporting limit are estimated due to low continuing calibration standard criteria failure.
A03
Result(s) and reporting limit(s) are estimated due to low matrix spike recovery.
ND
Indicates compound analyzed for but not detected
RL
Reporting Limit
NA
Not Applicable
Lab Work Order # 1506024
Page
2 of2 31
Page
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW1
Lab ID: 1506024-01
CAS #
Analyte
Result
RL
Units
1.0
ug/L
Dilution
Analyzed
Date
QC Batch
Method
06/06/15
B5F0515
8260
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
ND
ND
ND
ND
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2.9
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.0
ug/L
156-59-2
10061-01-5
110-82-7
124-48-1
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
15
ND
1.0
ug/L
1.0
ug/L
1
06/06/15
B5F0515
8260
Cyclohexane
Dibromochloromethane
ND
ND
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
X
A05
Lab Work Order # 1506024
Page
3 of3 31
Page
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW1
Lab ID: 1506024-01
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
75-01-4
Vinyl chloride
110
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
98.6 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
96.1 %
82.7-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
99.5 %
85-115
06/06/15
B5F0515
8260
X
Lab Work Order # 1506024
Page
4 of4 31
Page
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW2
Lab ID: 1506024-02
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
156-59-2
10061-01-5
110-82-7
124-48-1
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
8.0
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
X
A05
Lab Work Order # 1506024
Page
5 of5 31
Page
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW2
Lab ID: 1506024-02
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
75-01-4
Vinyl chloride
15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
97.7 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
91.6 %
82.7-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
99.2 %
85-115
06/06/15
B5F0515
8260
X
Lab Work Order # 1506024
Page
6 of6 31
Page
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW2D
Lab ID: 1506024-03
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
110-82-7
124-48-1
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
1.0
ug/L
X
A05
Lab Work Order # 1506024
Page
7 of7 31
Page
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW2D
Lab ID: 1506024-03
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
75-01-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
99.9 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
94.2 %
82.7-115
06/06/15
B5F0515
8260
99.7 %
85-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
X
Lab Work Order # 1506024
Page
8 of8 31
Page
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW3
Lab ID: 1506024-04
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
ND
ND
ND
ND
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
1,1-Dichloroethane
1,1-Dichloroethylene
1.3
ND
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Chloroethane
Chloroform
46
ND
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
ND
ND
ND
ND
ND
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
110-82-7
124-48-1
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
X
A05
Lab Work Order # 1506024
Page
9 of9 31
Page
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW3
Lab ID: 1506024-04
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
75-01-4
Vinyl chloride
2.2
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
97.0 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
93.5 %
82.7-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
100 %
85-115
06/06/15
B5F0515
8260
X
Lab Work Order # 1506024
Page
of 31
Page1010
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW4S
Lab ID: 1506024-05
CAS #
Analyte
Result
Analyzed
Date
QC Batch
Method
06/06/15
B5F0515
8260
RL
Units
ND
1.0
ug/L
6.1
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Dilution
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1
75-34-3
1,1-Dichloroethane
9.3
1.0
ug/L
1
06/06/15
B5F0515
8260
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
2.3
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
156-59-2
10061-01-5
110-82-7
124-48-1
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
8260
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
130
ND
1.0
ug/L
1
06/06/15
B5F0515
1.0
ug/L
1
06/06/15
B5F0515
8260
Cyclohexane
Dibromochloromethane
ND
ND
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
X
A05
Lab Work Order # 1506024
Page
of 31
Page1111
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW4S
Lab ID: 1506024-05
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
75-01-4
Vinyl chloride
260
5.0
ug/L
5
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
96.0 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
94.0 %
82.7-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
100 %
85-115
06/06/15
B5F0515
8260
X
Lab Work Order # 1506024
Page
of 31
Page1212
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW4D
Lab ID: 1506024-06
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
110-82-7
124-48-1
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
1.0
ug/L
X
A05
Lab Work Order # 1506024
Page
of 31
Page1313
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW4D
Lab ID: 1506024-06
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
75-01-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
96.4 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
93.2 %
82.7-115
06/06/15
B5F0515
8260
101 %
85-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
X
Lab Work Order # 1506024
Page
of 31
Page1414
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW6
Lab ID: 1506024-07
CAS #
Analyte
Result
Analyzed
Date
QC Batch
Method
06/06/15
B5F0515
8260
RL
Units
ND
1.0
ug/L
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Dilution
Qualifier
Organics-Volatiles
630-20-6
1,1,1,2-Tetrachloroethane
1
71-55-6
79-34-5
79-00-5
75-34-3
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
7.4
ND
ND
ND
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1.6
ND
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.0
ug/L
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
140
ND
1.0
ug/L
1.0
ug/L
1
06/06/15
B5F0515
8260
Cyclohexane
Dibromochloromethane
ND
ND
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
156-59-2
10061-01-5
110-82-7
124-48-1
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
X
A05
Lab Work Order # 1506024
Page
of 31
Page1515
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW6
Lab ID: 1506024-07
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
Tetrachloroethylene
Tetrahydrofuran
13
ND
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
ND
ND
ND
ND
79-01-6
75-69-4
Trichloroethylene
Trichlorofluoromethane
2900
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
75-01-4
Vinyl chloride
1.4
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
50
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
97.7 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
95.0 %
82.7-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
101 %
85-115
06/06/15
B5F0515
8260
X
Lab Work Order # 1506024
Page
of 31
Page1616
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW7
Lab ID: 1506024-08
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
110-82-7
124-48-1
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
1.0
ug/L
X
A05
Lab Work Order # 1506024
Page
of 31
Page1717
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW7
Lab ID: 1506024-08
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
75-01-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
95.8 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
92.1 %
82.7-115
06/06/15
B5F0515
8260
101 %
85-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
X
Lab Work Order # 1506024
Page
of 31
Page1818
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW8
Lab ID: 1506024-09
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
ND
ND
ND
ND
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
1,1-Dichloroethane
1,1-Dichloroethylene
156-59-2
10061-01-5
110-82-7
124-48-1
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
43
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
5.1
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Cyclohexane
Dibromochloromethane
ND
ND
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
ug/L
X
A05
Lab Work Order # 1506024
Page
of 31
Page1919
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW8
Lab ID: 1506024-09
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
156-60-5
10061-02-6
110-57-6
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
1.5
ND
trans-1,4-Dichloro-2-butene
ND
5.0
ug/L
1
06/06/15
B5F0515
8260
79-01-6
75-69-4
Trichloroethylene
Trichlorofluoromethane
1.1
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
75-01-4
Vinyl chloride
13
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
97.5 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
93.5 %
82.7-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
100 %
85-115
06/06/15
B5F0515
8260
X
Lab Work Order # 1506024
Page
of 31
Page2020
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW9
Lab ID: 1506024-10
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
ND
ND
ND
ND
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
110-82-7
124-48-1
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
0.97
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
5.0
ug/L
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
T
X
A05
Lab Work Order # 1506024
Page
of 31
Page2121
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW9
Lab ID: 1506024-10
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
75-01-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
98.2 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
94.4 %
82.7-115
06/06/15
B5F0515
8260
98.9 %
85-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
X
Lab Work Order # 1506024
Page
of 31
Page2222
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW10
Lab ID: 1506024-11
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
110-82-7
124-48-1
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
1.0
ug/L
X
A05
Lab Work Order # 1506024
Page
of 31
Page2323
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW10
Lab ID: 1506024-11
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
75-01-4
Vinyl chloride
1.5
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
96.2 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
92.6 %
82.7-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
102 %
85-115
06/06/15
B5F0515
8260
X
Lab Work Order # 1506024
Page
of 31
Page2424
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW11
Lab ID: 1506024-12
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
156-59-2
10061-01-5
110-82-7
124-48-1
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1
06/06/15
B5F0515
8260
1.0
ug/L
X
A05
Lab Work Order # 1506024
Page
of 31
Page2525
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW11
Lab ID: 1506024-12
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
79-01-6
75-69-4
75-01-4
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
95.6 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
91.9 %
82.7-115
06/06/15
B5F0515
8260
99.1 %
85-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
X
Lab Work Order # 1506024
Page
of 31
Page2626
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW12
Lab ID: 1506024-13
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
156-59-2
10061-01-5
110-82-7
124-48-1
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
Cyclohexane
Dibromochloromethane
1.0
ND
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
X
A05
Lab Work Order # 1506024
Page
of 31
Page2727
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW12
Lab ID: 1506024-13
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
156-60-5
10061-02-6
110-57-6
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
trans-1,4-Dichloro-2-butene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
79-01-6
75-69-4
75-01-4
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
15
ND
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
98.3 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
95.8 %
82.7-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
98.6 %
85-115
06/06/15
B5F0515
8260
X
Lab Work Order # 1506024
Page
of 31
Page2828
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW13
Lab ID: 1506024-14
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
630-20-6
71-55-6
79-34-5
79-00-5
75-34-3
75-35-4
87-61-6
96-18-4
526-73-8
120-82-1
95-63-6
96-12-8
106-93-4
95-50-1
107-06-2
78-87-5
108-67-8
541-73-1
106-46-7
78-93-3
591-78-6
91-57-6
67-64-1
108-10-1
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,3-Trimethylbenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
2-Butanone (MEK)
2-Hexanone
2-Methylnaphthalene
2-Propanone (acetone)
4-Methyl-2-pentanone (MIBK)
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
156-59-2
10061-01-5
110-82-7
124-48-1
cis-1,2-Dichloroethylene
cis-1,3-Dichloropropylene
70
ND
ND
ND
Cyclohexane
Dibromochloromethane
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
20
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
5.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
A03, X
A05
Lab Work Order # 1506024
Page
of 31
Page2929
of 32
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
Client ID: MW13
Lab ID: 1506024-14
CAS #
Analyte
Result
RL
Units
Dilution
Analyzed
Date
QC Batch
Method
Qualifier
Organics-Volatiles
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
74-95-3
75-71-8
60-29-7
108-20-3
100-41-4
637-92-3
67-72-1
98-82-8
1330-20-7
74-88-4
75-09-2
1634-04-4
91-20-3
104-51-8
103-65-1
95-47-6
99-87-6
135-98-8
100-42-5
98-06-6
75-65-0
994-05-8
127-18-4
109-99-9
108-88-3
Dibromomethane
Dichlorodifluoromethane
Diethyl ether
Diisopropyl Ether
Ethylbenzene
Ethyltertiarybutylether
Hexachloroethane
Isopropylbenzene
m & p - Xylene
Methyl iodide
Methylene chloride
Methyltertiarybutylether
Naphthalene
n-Butylbenzene
n-Propylbenzene
o-Xylene
p-Isopropyl toluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
tertiary Butyl Alcohol
tertiaryAmylmethylether
Tetrachloroethylene
Tetrahydrofuran
Toluene
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
156-60-5
10061-02-6
110-57-6
trans-1,2-Dichloroethylene
trans-1,3-Dichloropropylene
2.9
ND
trans-1,4-Dichloro-2-butene
ND
5.0
ug/L
1
06/06/15
B5F0515
8260
79-01-6
75-69-4
Trichloroethylene
Trichlorofluoromethane
9.7
ND
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
75-01-4
Vinyl chloride
9.2
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
B5F0515
8260
B5F0515
8260
2.0
ug/L
1
06/06/15
1.0
ug/L
1
06/06/15
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
50
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
5.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
1.0
ug/L
1
06/06/15
B5F0515
8260
Surrogate: Bromofluorobenzene
99.8 %
85-115
06/06/15
B5F0515
8260
Surrogate: Dibromofluoromethane
96.3 %
82.7-115
06/06/15
B5F0515
8260
Surrogate: Toluene-d8
99.2 %
85-115
06/06/15
B5F0515
8260
X
Lab Work Order # 1506024
Page
of 31
Page3030
of 32
DEu=
Michigan Department of Environmental Quality
Laboratory Services Section
,~b\Yo~~=~ ~~,
Analvsis Reauest Sheet
II.__
Pro-!«t_
N•m_·_
_
_
AY
1
~L~-~-·o_"_~o_;a_·n_"~-rct_R_a_p_rd_s_
_ _
F_o_rm_e_r_B_e_ld_i_n_g_P_r_o_d_u_c_
t s_ _ _ _
_
___,l
CCEmoill
Sam le Col~ectot
jjodonnelld@mlchrgan .gov
2015
Irc
___jl ('dex44910
I
II
I
IPCA 30740
Paul J. Knoerr
Em•ii2
11.____
_
_..jl l(616) 356-0624
ctem..l3
( onltactflrm
II
Actept An;atysls
Overflow lab Choke I
Contnct firm P11ma
hold timecodes
la b Use
only
oo
Collectio n
Dole
Field Sample ldenllncallon
,.
1 : ~\
2 !I) d.
3
D)
.
Cont:a1M t
<ouot
\~C\o
3
MW2
6/2/ 2014
l ·.\~ p
'2.
MW2D
6/2/2014
l ~ L\o
~ -
6/2/ 2014
I ~C>~I'l
2.
"'''~
:,
os
MW4S
6
6l:.'
MW4D
7
en
MW6:
.., .
..
m
Mws'
10
( b
MW9
.
RGANIC CHEMISTRY
@
VOA ·Yolotile orsanlc Ad dle
Vola lllu-fu iiUst
~ 0
6TEX/M16E/TMBonly
2 3 4 S 6 7 8 9 10
Ch lorinated only
1 23 4 56789 10
GRO
I 2 3 4 5 6 7 8 9 10
1,4 Olo.,ne
1 2 3 4 s 6 7 8 9 10
'MfrH • Moth ane, Ethane, Eth ene
Methane-, Et hane, Ethene 1234 567 8 9 10
ON · Pesticides, PCBS
Pesticides & PC8s
I 23 45 6 7 8 9 10
Penlcldes o nfy
1 2 3 4 56789 10
PCB> only
1 2 3 4 5 6 7 8 9 10
loxaphtne
I 2 3 4 5 6 7 8 9 10
Chlordane
I 2 3 4 5 6 7 8 9 10
-aNA· Base Neutral Acids
BNA>
I 2 3 4 5 6 7 8 9 10
Bt nzld fnes
1 234567 8 9 10
PNA>only
1 234 56789 10
8Nsooly
I 2 3 4 5 6 7 8 9 10
Acids only
12 3 4 56 7 8 9 10
o rgan I< Specialty Rtqut sU
Ubrary search· Volatiles 1 2 34 56 7 8 9 10
libra ry searc h - St:! miVo ls 12 3 4 56 7 89 10
flnger Prin1
12 3 4 56 78 9 10
ORO/ORO
1 234567 8 9 10
METALS CHEMISTRY PACKAGES
OpMtmo1 · Total
OpMemo2 - Olnoh-ed
I23456789 10
12 34 56789 10
(ib,AJ,b,~.C'd_.C~.~u.Co.F~.Pb.Mn,Hg.Mo,tli,St.Ac,Tl,V,Zn)
Mk hl&•niO · Total
Mkh!g.l niO· Dissolved
.
.
t!:S . MW7
9
6/2/2014
I 2 3 4 5· 6 7 8 9 10
1 2 3 4 S 6 7 8 9 10
IAs.8a.Cd.tr.C~.P b.H• .Se.Al! .lnl
·6/i/2014
u ~~,-,
'6/2/2014
\f'. \fo
.,
6/2/ 2014
lO ~~'
2
6/2/ 2014
ll H\ o..
t
6/2/2014
11,(0 p
l
1
1
I
I
I
I
1
1
1
I
Ob s · Aluminu m· AI
Oiss.- Antnk • A1
Ofss - Boron • 8
Olss ·Ba rium· Sa
Diss · BerylliUm · 8e
Olss ·Cadmium· Cd
Dlss ·Cob> it · Co
Dlss · Ch romium · Cr
Olss - Cop pt r • Cu
Dlss- Iron· Fe
Diu • Merrury • Hg
Ols• · lit Mum · ll
1
OJ~s- Molybdtnum
• Mo 1
I
1
f>tn - Ma nganese· Mn 1
Dlss ·lllckel· Nl
Olss · l ead • Pb
Diss- Antimony .. Sb
Ol\s • Sefenlum • Se
Olss • StronHu m .. Sr
1
1
1
I
1
Dfss. litil niLJ m. n
I
Oiu · Thallium · Tl
1
Oiss • Ura n!um • U
1
Ofss. - Va nadium. V
1
or.ss- Zinc. Zn
I
Oiss • Calciom • ca
1
Oiss- Potassium · K
I
oJss - MaenesfrJm ·Me I
DJss - Sodium· N1
I
·mss .·Hard lles.s - Ca,Mg 1
Mo·=Meiiil oJnoiV.iii···
2 3 4 5 6 7 8 9 10
2345 6 789 IO
23 4 5 6 789 10
2 3 4 S 6 7 8 9 10
2 3 4 5 6 7 8 9 10
2 3 456 7 89 10
2 345 678 9 10
2 3 4 5 6789 10
23 456789 10
2345 6 7 89 10
2 3 4 5 6 7 8 9 IO
2 3 4 5 6 7 8 9 IO
2345 6 789 10
2345 67 89 10
23 4 5 6 789 10
2 3 4 5 6 7 8 9 ID
2 3 4 5 6 7 8 9 10
2 3 4 5 6 7 8 9 IO
2 3 4 5 6 7 8 9 10
2 3 4 5 6 7 8 9 10
2 3 4 5 6 7 8 9 10
2 3 4 s 6 7 8 9 10
2345 67 89 10
2 3 4 s 6 7 8 9 10
2 34 56 7 8910
2 3 4 5 6 7 8 9 10
2 3 4 s 6 7 8 9 10
2 3 4 s 6 7 8 9 10
2 3 4 s 6 7 8 9 10
234 5 67 8 9 10
12345 6 78 9 10
Whfiltr"t1on
~
..
.
..
.
MA · TOTAL MET~U
MAD · OI)SOLVtu METALS
Olss ~ Silver ~ Aa
Commen t s
..
6/2/ 2014
4 6"- \ MW3
8
Collection
Time
MW1
5
Contact
one
ovtiliow lib ChOice 2
1
WATER
r •trlx
Silvtr · AI
Aluminum· AI
Arunk - A!
Boron- 8
Sa ritJm · Ba
Beryllium · Be
Cadmfum · Cd
Cobolt - Co
Chromlum - Cr
Copp<r · cu
fron · Fe
Me rcury ·lig
llthlum - U
1
I
I
I
1
1
I
1
1
1
I
1
I
Mang~nese- - Mn
I
Motybdenum- Mo
1
Nkkei ·NI
l ..d · Pb
Antfmonv · Sb
Sel~n!um . se
1
I
I
Strontlu m • Sr
nta nlum - Tl
Th•llium· TI
Uranlum-U
Vanadium - V
lin< - Zn
C.lclum-ca
Potustum - K
Magnesium - Mg
Sodiu m · Na
H>rdness · C., Mg
I
I
1
I
I
I
1
I
1
I
I
I
--UIG · l ow level Metcury
P/tl('.;fV LC"wl•W;! - Jofl
GENERAL lHt MI) TRY
23 4 56789
23 4 56 78 9
2 3 4 56789
23 4 56789
2 3456789
2 3 4S6789
2 3 4 5678 9
234 56789
2 3 4 56 7 8 9
2 3 4 s 6 7 8 9
2 3 4 5 6 7 8 9
2 3 4 5 6 7 8 9
2 3 4 5 6 7 8 9
2345678 9
2 3456789
2 3 4 5 6 7 8 9
2 3 4 5 6 7 8 9
2 3 4 s 6 7 8 9
2 3 4 s 6 7 8 9
2 3 4 5 6 7 8 9
2 3 4 s 6 7 8 9
2 34 5 6 789
2 3 4 s 6 7 8 9
2 3 4 s 6 7 8 9
2 3 4 S 6 7 8 9
23 4 56789
2 3 4 5 6 7 8 9
2 3 4 s 6 7 8 9
2 3 4 5 6 7 8 9
2 3 4 s 6 7 8 9
10
10
10
10
10
10
10
10
10
IO
10
10
10
10
10
10
IO
10
10
10
10
10
10
IO
10
10
10
10
IO
10
·- -- - -
GB TotoI Cy1n!dt • CN
GB Amenable Cyonl<lo • CN
GCH AviUJb!e C'yJnfde • CN
CA Chlorophyll
GN Ortho Phosphote • OP
GN Nit..-i 1e- NOt
1
1
1
1
1
I
1
1
I
1
1
I
I
2 3456 789
2345 6 7 8 9
234 5 67 89
23 456 789
2 3 4567 89
2 3 4 S 6 7 8 9
23 4567 89
2 3 4 5 6 7 8 9
2 3 4 5 6 7 8 9
2 3 4 5 6 7 8 9
2 3 4 5 6 789
2 3 4 56 78 9
2345 678 9
GN Nitrato · NO, (C.k.)
GN SUspended Solid s · SS
GN Dissolved SOII<Is · l OS
MN Ol.s SOlid> · 1D5 JCak.)
GN TUib ldity
MN Total Alkolrnity
MN B!carb/C'Ib Alkollnity
(in<ludu Total Alkalinity)
MN Chlorl<le ·Cl
I 23 4567 89
MN f hJOikfll • f
I 2 3 45 67 8 9
MN Sulfate ·SO-l
1 234 567 89
MN Chromium 6-6.,6
I 23 4 56 7 8 9
MN Conductivity
I 23456789
MN pH
1 2 34 56 78 9
GA Chem Oxy& Otm ·COD
12 3 4 5 678 9
GA DlssOrg C. rbon- OOC (FF) 1 2 3 4 S 6 7 8 9
(FJeld ·Filleted & Preserved)
GN DI» OrgC.rbon·OOC (lf) I 2 3 4 5 6 7 8 9
(lab· Filtered & Prese rved)
GA To la1 01& Cubon • TOC
1 234 5 6 78 9
GA Ammonia • NH3
1 234 5 678 9
GA Nitrot"N~rite • NOl>N02 1 2 3 4 S 6 7 8 9
GA ~Jeldohl Nnrogon · Ktl
1 2 3 4 5 6 7 8 9
GA Total Phosphona • TP
1 234567 89
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
IO
10
10
I 2 3 4 56789 10
Relinquished by
Print Name 'D
,
t,,
~ ~lGM.~~b~
0
-·~·~
t:
:s
u
-
~0. ~
..
'
~~ ~ .
0
c:
'iO
.c
u
Print Na
~0~~·-----------------------------­
Sig n ature:
DEQ Laboratory Services Section
PhOne: 5 17-335-9800
Page 1 ot 2
Page 31 of 32
I
DE€\.
Michigan Department of Environmental Qua !fly
Laboratory Services Section
Analvsis Reauest Sheet
hbW.ork:01der Number
,:.P.:.;IO:L)<:..:<:.:.t:..:N;:;am.:,:<:..__ _ _ _ _ _ _ _ _ __ __ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _,
I \ 'S;l~, l.o c) ';j"-\ Ij
r~"-'1a:.o;l1'-'i>,__ _ _ _ _ _ _ _ _ _--,
II
Former Belding Products
Site Code}Pro!ed Number
WATER
Sampte Col!ector
2015
134000083
jRRD Grand Rapids
j Paul J. Knoerr
[email protected]
~~4=4=9=10=~~
Oept~O;v~s,o n~Dfstnct
Samp!e Collector Phone
(CEmarl2
CCEmai13
Contact
IL9'"v""elfl=o:::wTla"'b'"'C"'ho=Tc::-e•1-------- - - - - - - - - - ' ' (old time codes
O.ertiOw lab Cti<llce 2
Lab Use
Only
Field Sample ldentlliuUon
1
Collection
Date
Collection
Cootalnu
Tlme
Count
6/2/2014
2
II)
MW11
6/2/2014
3
\1
\q
MW12
6/2/2014
f f~-~~,,. . t.
MW13
6/2/2014
1\id~
4
Comments
U~\C5n 1
lth .,.;j ·J
t\
MW10
..
~
s
,
6
7
\
..
..
8
9
.
I
io
0 RGANIC CHEMISTRY
VOA- Volatile 01gan1c Addle
6 7 8 9
VolatHes- Full Ust
BTEX/MTBE/TMB only
I 2
4 S 6 7 8 9
Ch1ofrnated only
1234567 8 9
GRO
I 2 3 4 5 6 7 8 9
1/1 Ofoxane
1 2 3 4 s 6 7 8 9
MErn ·Methane~ £thane~ Ethene
Methane, Ethan~, Elhtne 1 2 3 4 5 6 7 8 9
-(>N • Pestfddel, PCB!
Peslkides & PCBS
1 23456789
Pe1Ucides onfv
1 2 3 4 5 6 7 8 9
PCB> only
1 23456789
To:-:aphene
1 23456789
Chlo1dan.>
I 23456789
BNA- Bolt Neutral Acids
SNAs
1 2 3 4 s 6 7 8 9
Benddrnes
1 2 3 4 5 6 7 8 9
PNAsonty
I 2 3 4 5 6 7 8 9
SN>only
1 2 3 4 5 6 7 8 9
Adds on~
I 2 3 4 5 6 7 8 9
"(llganlc Spedalty Requests
Ubra.ry ~ea rdt - Volati!eii 1 2 3 4 5 6 7 8 9
library se-arch- SemNob 1 23456789
Finger Pfint
1 23456789
ORO/ORO
123456789
<if!!:!!i!5
MAO· DISSOLVED METALS
Dl.s.~ • SfN~r' •
10
10
10
10
10
10
10
10
10
10
10
---·----10
10
10
10
10
10
10
10
10
METALS CHEMISTRY PACKAGES
OpMemo2 -lotal
OpMemo2 - Ol!sotved
10
123456789 10
1234~6789
(Sb,A.s,83.~,Cd,Cr,Cu,Co,re,Pb,Mn.,tfg.Mo.fiisS!',Az.TI,V,Zn)
Mlthlg•nlo- Total
1 2 3 4 5 6 7 8 9 10
I 2 3 4 5 6 7 8 9 10
Mkh!gan10 • OJ.ssoNed
lAs 8> CdC< Co Pb Hg,S<!
Relln
ul5hed
~.Znl
Ag
1
1
1
1
1
I
2 3 4 5 6 7 8 9
O~s.s • A~IJ m!num ·AI
23456789
mss • ArsenTc ·As
23456789
ms-s- Boron- 9
2 3 4 s 6 7 8 9
mss-S.;trhi rn-Ba
2 3 4 s 6 7 8 9
otss ·Beryllium- Be
23456789
Olss- Udmlum- Cd
I 23456789
Diu- Cobalt- Co
1 23456789
Olss.- Chromium- Cr
1 2 3 4 5 6 7 8 9
Dts.s ·Copper .. Cu
I 2 3 4 5 6 7 8 9
Olss- Iron- fe
1 2 3 4 5 6 7 8 9
Ol.ss- Mercury- Hg
1 2 3 4 5 6 7 8 9
Dlss ·lithium· U
t ~ 3 4 s 6 7 8 9
Diu- Ma-nga ~ese • Mn 1 2 3 4 5 6 7 8 9
mss- Motybd~ru.un • Mo 1 2 3 4 5 6 7 8 9
Dlss- Nk~el- Nl
1 23456789
Dlss- Lead - Pb
1 23456789
otss- An limo ray- Sb
1 2 3 4 5 6 7 8 9
DJss- .$('fenlum - se
1 2 3 4 s 6 7 8 9
orss- Strontium • Sr
1 ~ 3 4 5 6 7 8 9
orss- litanium- n
1 2 3 4 5 6 7 8 9
mss- Thalfrurn- 11
I 2 3 4 5 6 7 8 9
Ols.s- Uranrum- U
123456789
orss- Va-nadium .. v
123456789
Olu-nnc-m
1 2 3 4 5 6 7 8 9
Olss -cak1vm-ca
1 2 3 4 5 6 7 8 9
Dlss • Potass!um · K
I 2 3 4 5 6 7 8 9
Olss- Magraes!um- Mg I 2 3 4 s 6 7 8 9
Dl.ss- SOdium- Na
I 2 3 4 5 6 7 8 9
Dis.s · Hardness - Ca, Mg 1 2 3 4 5 6 7 8 9
MD· Mel•ls OIS<olved
lab Flll1<1tlon
I z 3 4 ~ 6 7 8 9
MA ·TOTAL METALS
10
10
10
10
10
10
10
10
10
10
10
10
10
IO
10
10
10
IO
10
10
10
10
10
10
10
10
10
10
10
10
S!~er
-Ag
Al-uminum ·AJ
Arsen!c-.ru
Bot on- 8
Barium-8<)
Berytlrum ·Be
Cadmfum·Cd
Cabalt-Co
Chromfum -Cr
Copper·Cu
!ron- Fe
Mercvry- Hg
Utt1ium-U
Manganese - Mn
Molybdenum- Mo
Nlclei -Ni
Lead- Pb
Antrmony- Sb
$e1'('n!urn- Se
Strontium· Sr
Titanium- Tl
ThaHi"tJm-11
Uranium- U
Vilnadium • V
nnc-Ztl
Wkium-C.r;~
:Potassfu m • K
Magnesfum • Mg
Smtfurn- Na
Hardness- Ca, Mg
I 2 3 4 5 6 7 8 9
1 2 3456789
I 2 3 4 5 6 7 8 9
1 2 3 4 5 6 7 8 9
1 2 3 4 5 6 7 8 9
1 2 3 4 5 6 7 8 9
I 2 3 4 s 6 1 8 9
I 2 3 4 5 6 7 8 9
1 2 3 4 s 6 7 8 9
I 2 3 4 s 6 7 8 9
1 2 3 4 s 6 7 8 9
I 2 3456789
I 2 3456789
1 2 3456789
I 2 3 4 5 6 7 8 9
1 2 3 4 5 6 7 8 9
1 23456789
I 2 3 4 5 6 7 8 9
1 2 3 4 5 6 7 8 9
I 2 3 4 5 6 7 8 9
1 234567 8 9
I 2 3 4 5 6 7 8 9
1 2 3 4 5 6 7 8 9
I 2 3 4 5 6 7 8 9
1 2 3 4 5 6 7 8 9
1 2 3 4 5 6 7 8 9
I 2 3 4 ~ 6 7 8 9
I 2 3 4 s 6 7 8 9
! 2 3 4 5 6 7 8 9
1 2 3 4 _s ~ 7. 8 9
GENERAL CHEMISTRY
10
10
10
10
10
10
10
10
10
10
IO
10
10
10
10
10
10
10
10
10
10
IO
10
10
10
10
10
10
I!)
10
(iB
TotaiCy~n!de·CN
I
1
1
I
1
I
1
1
1
1
1
I
1
G8 Amenab!eCVanfde ·CN
GCN Avai,ab!e Cyanide· CN
CA Chlo1ophyll
GN OrthoPhosphate- OP
GN Mtrite • H0 2
GN Nit1ate - N0 1 (Calc. I
GN suspended Solid>- ss
GN Dissolved Solid> -lDS
Mt>r Ois.s Solids- TOS (Cal~.)
GN Turbidity
MN Tot>!Ailal;nity
MN B!mb/Ca1b Allallnity
(Includes Total Alkalinity)
MN Chlo1lde - Cl
1
MN ffuo1ide- F
1
MN Sulfate - 504
1
MN Chromium 6 ~ Crf6
1
MN Conductivity
1
MN pH
1
GA Chem Oxyg Oem ·COD
I
GA OJ« 01g Ca1bon- DOC (Ff}1
(Field - Filte1ed & P10ser.·ed}
Gt>r O!ss 01g Ca1bon- DOC (IF) 1
(Lab- filte1ed & P1eserved)
GA Total org carbon- me
I
GA Ammonia.- NH3
I
GA NitratetNitrfte ~N03'fN02
GA Kfeldahl Nitrcgen- XN
GA Toto! Phosphoros • TP
2
2
2
2
2
2
2
2
2
2
2
2
2
10
10
10
10
10
3 4 5 6 7 8 9
3456789
3 4 s 6 7 8 9
3 4 5 6 7 8 9
3 4 5 6 7 8 9
3 4 5 6 7 8 9
3 4 5 6 7 8 9
3 4 5 6 7 8 9
3 4 5 6 1 8 9
3 4 5 6 7 8 9
3 4 5 6 7 8 9
3 4 5 6 7 8 9
3 4 s 6 7 8 9
2 3 4 5 6 7 8
2 3 4 s 6 7 8
2 3 4 5 6 7 8
2345678
2 3 4 5 6 7 8
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