THRIFTY OIL CO. 0-15

(562)921-3581
90670 CA Springs, Fe Santa Highway, Imperial 13116
closure.
before Chevron by conducted were activities remediation No 2009. July in granted was closure
until RP remained Chevron years. six for facility the operated had ARCO after 2003, September
in activities upgrade piping and dispenser ARCO's during contamination soil of discovery
the following 1-00626A), (Case 2003 October in RP primary named again was Chevron
1996. September
in LARWQCB the by granted was closure until RP remained Chevron 1970s. mid the since
facility the operated had Chevron 1-00626); (Case 1986 February in gasoline of gallons 2,600 of
release reported the following 1987 April in LARWQCB the by RP primary named was Chevron
below: presented reasons the for decision, arbitrary and unfair
an is RPs three the of one as Thrifty name to decision the that believe We A). (Attachment
2015 15, August by Plan) (Work Plan Work Installation Well Monitoring Groundwater
a of submittal requiring are and property, above-referenced the at characterization site
perform to RPs as (ARCO) Company Richfield Atlantic and (Chevron), Company Management
Environmental Chevron Thrifty, named LARWQCB the Thrifty, to letter 2015 24, June their In
California. Malibu,
in Road Heathercliff 29145 at located #213 Station Service Thrifty former the at characterization
site perform to (RP) party responsible a as Thrifty of (LARWQCB) Board Control Quality Water
Regional Angeles Los the by designation the regarding (SWRCB), Board Control Resources
Water State California the by reviewed be to petition this submitting is (Thrifty) Co. Oil Thrifty
Crowl, Ms. Dear
Characterization Site Perform to Party Responsible as Co. Oil Thrifty
Designating Regarding Board Control Resources Water State the to Petition Subject:
T10000004593 ID. Global
I-00626B No. Case LARWQCB
4850 5855 0003 3500 7011
Mail Certified
90265 California Malibu,
Road Heathercliff 29145
#213 Station Co. Oil Thrifty Former
Re:
95812-0100 California Sacramento,
100 Box P.O.
Counsel Chief of Office
Board Control Resources Water State
Crowl M. Adrianna Ms.
2239 0-15
2015 15, July
CO. OIL THRIFTY
.)(-1!0
2
that soil in (TPHd) diesel as hydrocarbons petroleum total detected Any
rebuttal: following the presents Thrifty statement, this to response In (RPs). parties
responsible the as to referred be will and requirements Board Regional with comply
jointlymust above listed addressees all made, is determination a Until requirements.
Board Regional with comply to responsibility bears also Thrifty property, referenced
the of owner the As plume.commingled a formedreleases Those groundwater.
and soil in detected was TPHd and operations their during fuel diesel dispensed
and stored ARCO and Thrifty 1990. in Chevron from Site the purchasing after 1991
in property the on UST diesel a installed Thrifty site: the at RP a as Thrifty naming
justify to statement following the makes LARWQCB the letter, 2015 24, June their In
improper: or inappropriate was inaction or action the reasons the of statement A 4.
2015. 24, June dated letter
their in issued were directives LARWQCB the above, 2 no. bullet in described As
act: to requested was or act, to refused or acted, Board Water Regional the date The 3.
A). (Attachment 2015 15, August by Plan) (Work Plan Work
Installation Well Monitoring Groundwater a of submittal requiring are and property,
above-referenced the at characterization site perform to RPs as ARCO and Chevron
with along Thrifty, designated LARWQCB the Thrifty, to letter 2015 24, June their In
available: if act, to refusal any or challenged being action the
of copy a including petitioned, being Board Water Regional the of inaction or action The 2.
[email protected] Address: E-Mail
921-3581 (562) Number: Phone
90670 CA Springs, Fe Santa
Hwy. Imperial 13116
Berkett Barry Mr. Attn:
Co. Oil Thrifty
petitioner: the of address e-mail and number, telephone address, Name,
1.
2015). 1, June (Updated Petitions
Quality Water Filing for Instructions SWRCB's the in published format the follows appeal This
RPs. three the of
one of instead RP Secondary as named be to possible, not is that if or RP,
additional an as named
be not should Thrifty that demonstrate to serve which below presented is evidence Additional
RP. third a as Thrifty implicate would which documented been have releases unauthorized other
No Chevron. from contamination pre-existing verified and/or ARCO by release new a either
to attributable be to have would and responsibility, Thrifty's be cannot facility) the operated last
Thrifty (when 1997 year after releases Any instances. both in contamination the for responsible
was Chevron that aware well obviously was LARWQCB
the RP, as Chevron naming twice In
with comply to required being is it that unfair is it believes Thrifty Lastly,
diesel. of release the to contribute
not did Thrifty operation, of period short its during diesel stored and 1991,
in tank diesel a installed Thrifty that facts the notwithstanding Therefore,
2012. through 1997 from operations ARCO's during concentrations
diesel in increase significant a represent which ug/l), (770 2012 and (ug/l))
liter per micrograms (0.85 1998 in were 2 Table in presented groundwater
in TPHd of detections reported only The 1996. to 1990 from site the at
operations Thrifty's during groundwater in TPHd linking evidence no is there
Therefore, letter. LARWQCB 2015 24, June the of 2 Table in summarized
as 1996, and years1993 conducted in activities assessment in nor assessment,
baselining 1997 the in TPHd for analyzed not were samples Groundwater
assessment. that of time the at available criteria screening
the using levels, actionable at present not therefore was TPHd The 1996.
May dated Guidebook Cleanup and Assessment Site Interim LARWQCB's
the of 4.1 Table in specified grade) below feet 150 to 20 from ranging depth
groundwater for mg/kg; (1,000 TPHd for levels screening soil the below
far is assessment 1997 the in mg/kg) (81 TPHd of concentration maximum
the diesel, of be to assumed were 1997 in detections TPHd alleged the if Even
dispensers. diesel the to borings soil the from distance
significant the and chain, hydrocarbon the in overlap the given TPHg, be
likely very may detections TPHd reported the Therefore, starts. range analysis
TPHd the where range C8-C12 the in be to components gasoline the of more
causing disappears, chain carbon lighter/lesser the gasoline, of weathering
of effect typical the As C6-C12. of chain hydrocarbon a have typically which
(TPHg), gasoline as hydrocarbons petroleum total of portions include would
which C8-C32, was analysis TPHd the in specified type chain hydrocarbon
the that indicate Report Baselining the in included results analytical
laboratory the of review a Furthermore, area. dispenser western the in located
dispensers diesel the from distant is which area, dispenser the of portions
southern and eastern the in located all were TDD-3 and TDD-2, TDD-1,
borings However, mg/kg). 46 to (up TDD-3 and mg/kg) (5.7 TDD-1 borings
in detected also were TPHd of concentratrations Low TDD-2. boring in
detected (mg/kg), kilogram per milligrams 81 was soil in concentration TPHd
maximum the letter, LARWQCB 2015 24, June the in cited As site. the at
operation Thrifty's during release a have not did tank diesel the that indicate
would which UST, diesel the to adjacent immediately drilled TDD-6, boring
from collected samples soil in detected was TPHd No B). (Attachment 1997
22, December dated Report) (Baselining Report Investigation Subsurface
Baselining a in included are investigation this of results The ARCO.
to lease the of inception the at conducted 1997, July and June in ARCO
by site the at activities assessment baselining the of results the in included be
would 1997) to 1990 (from site the at operation Thrifty's of result a be would
4
MTBE
TBA
Results 1997
150
81
1.5
1.9
NA
Results 2012
2,700
1,600
22
12
3.7
Benzene
TPHd
TPHg
mg/kg) (in Results Sample Soil
follows: as facility, the of operation
Thrifty's of end the at conducted investigation baseline 1997 the to compared when
investigation, baseline 2012 the in groundwater and soil in significantly increased TBA
and MTBE, benzene, TPHd, TPHg, of concentrations maximum letter, LARWQCB 2015
24, June the in summarized As lease. Tesoro's of inception the at and lease ARCO's of
end the at conducted was investigation subsurface baseline a 2012, November and July In
closure). 1996 Chevron's to (prior concentrations
pre-closure the than lower much fact in were operations Thrifty's of
end the at assessment baselining 1997 the in groundwater and soil in xylenes total
and toluene, benzene, TPHg, of concentrations maximum the letter, LARWQCB
2015 24, June attached the of 2 and 1 Tables in shown As 1997. through 1990
from facility the operated Thrifty when period the includes which 2009, through
1986 from period entire this during site the at documented were releases other No
closure. site to prior Chevron by conducted were
activities remediation No LARWQCB. the by 2009 November in closed was
site the before years 6 over for site the at RP remained Chevron RP. as Chevron
named again and site, the for case the reopened LARWQCB the 2003, October
In TBA. mg/kg 2.2 and MTBE, mg/kg 0.0021 xylenes, total mg/kg 0.0037 TPHd,
mg/kg 530 TPHg, mg/kg 0.49 of concentrations hydrocarbon maximum indicated
results analytical soil 2003, in activities upgrade piping and dispenser During
LARWQCB.
the by 1996 September in closed was site the before years 9 over for site the at
RP remained Chevron RP. the as Chevron named and site the for 1-00626 number
case opened LARWQCB the 1987, April In xylenes. total mg/kg 2,100 and
ethylbenzene, mg/kg 430 toluene, mg/kg 350 benzene, mg/kg 110 TPHg, mg/kg
2,200 were samples soil in concentrations hydrocarbon maximum 1987, and 1986
years in IT by conducted activities assessment site subsequent In 1985. October
in ended that time of period unknown an over islands dispenser two the between
located piping from lost were gasoline unleaded of gallons 2,600 approximately
reported that report incident leak a submitted (IT) Corporation Technology,
International site, the of operation Chevron's during 1986 February In
follows: as site,
the at RP as Chevron naming twice LARWQCB the in resulted and letter, LARWQCB
2015 24, June attached the in documented well are site the at releases hydrocarbon The
site. the at releases documented the to connection apparent no
with property, the of owner the being merely by requirements Board Regional
5
1996. May dated Guidebook Cleanup and Assessment Site
Interim LARWQCB's the was assessment baselining 1997 the of time the at
soil in concentrations TPHd for levels screening establishing for reference The
86-18. WQ and 89-8
WQ Orders Board Water State as well as 2012, September Manual, Guidance
Tank Fuel Underground Leaking Board Control Resources Water Water
State the in established is Thrifty for status RP Secondary for precedent The
to: referred are that transcripts hearing or documents to citations
including petition, the in raised issues legal any for authorities and points of statement A 7.
Ltd.].). Park, [Vallco 86-18 WQ and al] et Spitzer [Arthur 89-8
WQ Orders Board Water (State discharge the to contribute or initiate not did
party responsible the things, other among where, appropriate status liability
secondary found have orders Board Water State responsible. secondary
are who those and responsible primarily are who parties between distinguish
agencies local many site, UST a at exist parties responsible more or one
Where RP. Secondary a as Thrifty name to possible, not is this if and site, the
for RP a as Thrifty remove Board Water State the that requests petitioner The
take: to Board Water State the requests petitioner the action The 6.
to. contribute or cause not did they that release a of actions
corrective for costs substantial incur unnecessarily to forced be will petitioner Further,
record. the in evidence by unsupported finding unfair and arbitrary an of provisions to
subjected be will they because actions LARWQCB's the by aggrieved been has Petitioner
Aggrieved: is Petitioner the How 5.
chain. hydrocarbon the in overlap the on based
TPHg be fact in may level) actionable an at not (although investigation 1997 the during
detected soil in TPHd alleged the discussed, previously As release. documented prior
Chevron's of rediscovery the and/or operations ARCO's during release(s) new indicating
2012, in operations ARCO of end the and 1997 in operations Thrifty of end the between
concentrations constituent hydrocarbon in increases significant show clearly results The
MTBE
TBA
39
NA
59
1,100
TPHg
TPHd
1,500
NA
74
770
21,000
Benzene
190.000
Results 2012
Results 1997
ug/1) (in Results Sample Water
6
letter. a such receiving be would it that notice advance no had it because
letter, LARWQCB the to objections raise not could Thrifty unexpected. completely
was co-RP a as Thrifty naming letter 2015 24, June LARWQCB the of issuance The
board. regional the before objections those
raise not could petitioner the why of explanation an or acted, board regional the before
board regional the to presented were petition the in raised issues the that statement A 9.
94583 CA Ramon, San
Road Canyon Bollinger 6101
Unit Business Marketing
Company Management Environmental Chevron
Lathrop Shelby Ms.
90623-1066 CA Palma, La
LPR-4-221 200, Suite Drive, Centerpointe 4
Company Richfield Atlantic
Christie Kyle Mr.
90013 CA Angeles,
200 Ste. Street, 4th West
Board Control Quality Water Regional Angeles
Unger Sam
Los
320
Los
Mr.
parties: following the to sent been has petition The
petitioner. the from different if discharger, the
to and Board Water Regional the to sent been have petition the of copies that statement A 8.
7
1997 22, December dated Report, Investigation Subsurface Baselining
characterization site perform to RP
a as Co. Oil Thrifty naming 2015, 24, June dated
letter LARWQCB
B: Attachment
A:
Attachment
Attachments:
File
Co. Oil Thrifty President, Vice Executive Berkett, Barry Mr.
Company Management Environmental Chevron Lathrop, Shelby Ms.
Company Richfield Atlantic Christie, Kyle Mr.
Board Control Quality Water Regional Angeles Los Unger, Sam Mr.
cc:
Affairs Environmental
Manager General
Panaitescu Chris
OF
Services Technical
Director
P.E. Suryakusuma, Jeff
,
a.
6s-9.\AIGIA/
G
Professional
California
Manager Project
P.G Higinbotham, Larry
q
\0NAL
311. Ext at Suryakusuma Jeff or 390, Ext. at Panaitescu
Chris 325, Ext. 921-3581, (562) at Higinbotham Larry either contact please information,
additional require or transmittal this regarding comments or questions any have should you If
V
INIIIIH3VIIV
www.waterOoarcit7.4a.gwiosanyolev
WE
90073 CA An0c49t7. Los 200. Sutte St.. 4th Wes[ 320
13!40EY,. SAMUEL.
i
GHAII
63213. No. Station Tesoro operating began and Thrifty
from Site the leased Tesoro 2012, June In 2012. June and 1997 June between 9615 No. Station
ARCO operated and Thrifty from Site the leased ARCO 1997. June and 1990 August between
Site the at operated was 213 No. Station Thrifty (Thrifty). Company Oil Thrifty to Chevron by
sold was property the time which at 1990, August until 6-1400 No. Station Chevron as operated
was Site The years. 40 least at for station service fuel a as operated been has Site The
Background Site
Site. the for
files case previous the in contained information and ARCO by provide information the reviewed
have We 2013. 13, June dated Information" Site "Additional titled report the in information
specific site available provided (ARCO) Company Richfield Atlantic The (Site). California
Malibu, Road, Heathercliff 29145 at located 9615 No. Station ARCO former the to regards
information specific site of submittal the required (enclosed) 2013 10, April dated letter Our
in
Panaitescu: Mr. and Molla, Ms. Christie, Mr. Dear
110000004593 NO. GLOBAL I-00626B; NO. CASE
CALIFORNIA MALIBU, ROAD, HEATHERCLIFF 29145
6-1400) NO. STATION CHEVRON FORMER AND 213 NO. STATION THRIFY (FORMER
9615 NO. STATION ARCO FORMER
2727 2720 SECTIONS REGULATIONS, OF CODE CALIFORNIA 16, CHAPTER
23, TITLE AND 25296.10 SECTION CODE SAFETY AND HEALTH TO PURSUANT
RELEASE TANK STORAGE UNDERGROUND UNAUTHORIZED TO RESPONSE IN ACTION
CORRECTIVE TAKE TO DIRECTIVE
PROGRAM TANK STORAGE UNDERGROUND
-
-
90623-1066 CA Palma, La
LPR-4-221 200, Suite Drive, Centerpointe 4
Company Richfield Atlantic
Christie Kyle Mr.
7049 6294 0000 1640 7012 NO.: CLAIM
REQUESTED RECEIPT RETURN
MAIL CERTIFIED
92822-2292 CA Brea,
2292 Box P.O.
Company Management Environmental Chevron
Molla Natasha Ms.
7056 6294 0000 1640 7012 NO.: CLAIM
REQUESTED RECEIPT RETURN
MAIL CERTIFIED
90670 CA Springs, Fe Santa
Highway Imperial 13116
Company Oil Thrifty
Panaitescu Chris Mr.
7063 6294 0000 1640 7012 NO.: CLAIM
REQUESTED RECEIPT RETURN
MAIL CERTIFIED
/3 52:09
ENVIRONMENTAL
2015
26
2015 24, June
JUN
Board Control Quality Water Regional Angeles Los
RECEIVED
Boards Water
C
.-084414200e
www.wais-ruoar<ls.ca.poviir,sancyiLos
I
01,013
,)FFICE,R SL:ECLiTivL :i1HE,13111 SAMUEL.
!
An,rles Los 20U, :3!Li1.3
,
4114
Wow 32C
CHAVI SL!Lttl!:.W:,
respectively. pg/L, 39 and pg/L, 8.0 pg/L, 2.9 pg/L, 12 pg/L, 74 pg/L, 1,500
of concentrations at detected were MTBE and BTEX, TPHg, showed results analytical
and MW-7 well on-site from collected was sample groundwater a 1997, July In respectively.
mg/kg, 1.9 and mg/kg, 17 /kg, mg 2.3 mg/kg, 6.1 mg/kg, 1.5 mg/kg, 81 mg/kg, 150 were
samples soil in (MTBE) ether butyl tertiary methyl and BTEX, (TPHd), diesel as hydrocarbons
petroleum total TPHg, of concentrations Maximum ARCO. for Site the at investigation
subsurface baseline a conducted Inc. Group, Environmental Pacific 1997, July and June In
abandoned. not were wells monitoring groundwater on-site three
the and 1996 September in case the closed Board Regional The respectively. pg/L, 1,100 and
pg/L, 530 pg/L, 1,100 pg/L, 3,000 pg/L, 16,100 of concentrations at were groundwater in BTEX
and TPHg of detections maximum 1996, April In 1996. April and 1994 June between events
monitoring groundwater periodic conducted Chevron respectively. pg/L, 1,600 and pg/L, 310
pg/L, 2,400 pg/L, 1,200 (pg/L), liter per micrograms 9,500 of concentrations at BTEX and TPHg
of detections maximum had 1993 November in collected samples Groundwater respectively.
mg/kg, 210 and mg/kg, 34 mg/kg, 180 mg/kg, 34 mg/kg, 2,100 were samples soil in BTEX
and TPHg of concentrations Maximum MW-7. and MW-5, MW-4, wells monitoring groundwater
as completed were borings the of three and Site the at advanced were borings soil nine 1993, In
mg/kg,
USTs.
respectively. mg/kg, 886.74 and mg/kg, 167.66 mg/kg, 459.93 mg/kg, 54.87
6,306.67 were samples soil in BTEX and TPHg of concentrations Maximum
former the of area the in collected were samples soil six 1991, In
party. responsible the as Chevron named
and Site the for 1-00626) number (case case a opened Board) (Regional Board Control Quality
Water Regional Angeles Los the 1987, April In respectively. mg/kg, 2,100 and mg/kg, 430
mg/kg, 350 mg/kg, 110 (mg/kg), kilogram per milligrams 2,200 were 1987 and 1986 in collected
samples soil in (BTEX) xylenes total and ethylbenzene, toluene, benzene, (TPHg), gasoline
as hydrocarbons petroleum total of concentrations maximum The islands. dispenser the
of southeast well monitoring one installed and borings soil six advanced ITC 1987, and 1986 In
line. product regular the
on detector leak and turbine the between occurring Site, the at released were gasoline regular
of gallons 1,000 approximately that suggested 1986 March in conducted audit tank a of Results
1985. October in ended that time of period unknown an over islands dispenser two the between
located piping from lost were gasoline unleaded of gallons 2,600 approximately reported that
report incident leak a submitted (ITC) Corporation Technology International 1986, February In
History Investigation Site
sumps. containment under-dispenser
and dispensers, new piping, fiberglass double-contained new with replaced and removed were
piping product fiberglass double-contained and dispensers onsite the 2003, In 1991. in activities
reconfiguration during Site the at installed were piping associated and gasoline unleaded
supreme and unleaded, regular, and diesel contained historically that USTs fiberglass walled
double- new Four Site. the from removed were gasoline unleaded supreme and unleaded,
regular, contained that USTs steel single-walled 10,000-gallon three 1991, March In Site. the
from removed was (UST) tank storage underground oil waste 280-gallon one 1990, August In
2
Page
Thrifty Panaitescu, Chris Mr.
Chevron Molla, Natasha Ms.
ARCO Christie, Kyle Mr.
2015 24, June
wwv...wolor0oara,ca.c10%210sange.,
OFFICER i,:.XECliTivE.
I
90013
Lb/6E0. SAM001.
I
47-0/.1,1
20Q, S;nte
St, 01, Wes. 320
Srrom:,)Ek.
2012. and 1986 between investigations subsurface
during Site the at collected samples 2) (Table groundwater and 1) (Table soil in TBA and MTBE,
BTEX, TPHd, TPHg, of concentrations detected maximum the summarize tables following The
respectively.
TBA, and MTBE, BTEX, TPHd, TPHg, for pg/L 1,100 and pg/L, 59 pg/L, 14,000 pg/L, 2,300
pg/L, 30,000 pg/L, 21,000 pg/L, 770 pg/L, 190,000 of concentrations analytical maximum
had investigation the during collected samples groundwater Grab respectively. TBA, and MTBE,
BTEX, TPHd, TPHg, for mg/kg 2.7 and mg/kg, 3.9 mg/kg, 110 mg/kg, 17 mg/kg, 55 mg/kg, 9.1
mg/kg, 23 mg/kg, 1,400 of concentrations maximum reported and borings soil the from
samples soil split analyzed ARCO respectively. mg/kg, 3.7 and mg/kg, 12 mg/kg, 240 mg/kg, 44
mg/kg, 130 mg/kg, 22 mg/kg, 1,600 mg/kg, 2,700 were Tesoro by reported samples soil
in TBA and MTBE, BTEX, TPHd, TPHg, for concentrations analytical Maximum Tesoro. for Site
the at investigation subsurface baseline a conducted ERI Cardno 2012, November and July In
2009. November in Site the at wells monitoring groundwater three the abandoned
Chevron and 2009 July in case the closed Board Regional The TPHd. for analyzed not
were 2009 and 2006 between collected samples Groundwater 2009. June in collected samples
groundwater in limit reporting analytical the above detected not was MTBE respectively.
pg/L, 23 and pg/L, 18 pg/L, 6 pg/L, 17 pg/L, 26 pg/L, 790 were samples groundwater
in detected TBA and BTEX, TPHg, of concentrations maximum 2009, June In 2006.
June in collected samples groundwater in limit reporting the above detected not was MTBE and
pg/L 550 of concentration maximum a at detected was (TBA) alcohol butyl Tertiary respectively.
pg/L, 740 and pg/L, 260 pg/L, 510 pg/L, 990 pg/L, 8,900 of concentrations maximum at BTEX
and TPHg of detections had wells on-site from collected samples groundwater 2006, June In
activities. monitoring groundwater resume to Site the at wells monitoring groundwater
three existing the used Chevron party. responsible the as Chevron named and I-00626A
number case under Site the for case the reopened Board Regional the 2003, October In
USTs. existing the near dispensers
gasoline/diesel the of one beneath located was detection soil TPHd maximum The samples.
soil all in limit reporting respective their above detected not were ethylbenzene and toluene,
Benzene, respectively. mg/kg, 2.2 and mg/kg, 0.0021 mg/kg, 0.0037 mg/kg, 530 mg/kg, 0.49
were samples soil in detected TBA and MTBE, xylenes, total TPHd, TPHg, of concentrations
maximum The total). in collected samples (five piping product the near and dispenser each
beneath collected were samples soil 2003, in activities upgrade piping and dispenser the During
respectively. pg/L, 42 and pg/L, 370 pg/L, 110 pg/L, 400 pg/L, 620
pg/L, 0.85 pg/L, 2,100 were MTBE and BTEX, TPHd, TPHg, of concentrations Maximum
MW-7. and MW-5, MW-4, wells on-site from collected were samples groundwater 1998, In
3 Page
Thrifty Pariaitescu, Chris Mr.
Chevron Molla, Natasha Ms.
ARCO Christie, Kyle Mr.
2015 24, June
wair,M0aras.ca.gov/I.sang9,:s www
or-FIcps
iticrc.i.r!!
90013
ULIC:EV, SAMUEL.
AnAele,. Los 200, Stott: St West.411, 320
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,
00;00 Sr!!,!001F-0, C0,01.1=!!!
by Plan) (Work Plan Work Installation Well Monitoring Groundwater a submit to required are
RPs the plumes, hydrocarbon phase dissolved and adsorbed the of extent the define to order In
2727. through 2720 sections 23, Title (CCR),
Regulations of Code California in forth set are requirements action Corrective environment. the
and safety health, human of protection ensure to Monitoring) Verification and Implementation,
Plan Action Corrective Investigation, Water and Soil Assessment, Site Preliminary (i.e. action
corrective take to required are RPs the 25296.10, Section Code Safety and Health to Pursuant
(RPs). parties responsible the as to referred be will
and requirements Board Regional with comply jointly must above listed addressees all made,
is determination a Until requirements. Board Regional with comply to responsibility legal bears
also Thrifty property, referenced the of owner the As plume. comingled a formed releases Those
groundwater. and soil in detected was TPHd and operations their during fuel diesel dispensed
and stored ARCO and Thrifty 1990. in Chevron from Site the purchasing after 1991 in property
the on UST diesel a installed Thrifty closed. were cases previous the when groundwater
and soil the in contamination residual had and operations its during releases had Chevron
plume. comingled the for parties responsible as above listed addressees the identified has
Board Regional the files, case previous the from information and provided information on Based
2725) § 16, Chapter 23, Title (CCR Characterization Site
detected not = ND
analyzed not = NA
MTBE
TBA
NA
NA
NA
NA
8
39
740
370
ND
42
NA
NA
6
18
ND
2,300
14,000
59
1,100
23
550
1,100
1,600
X
260
110
2.9
530
310
E
21,000
26
990
620
30,000
17
510
400
74
12
3,000
1,200
1,100
2,400
T
B
16,100
9,500
TPHg
NA
NA
TPHd
190,000
790
8,900
2,100
1,500
770
NA
NA
0.85
NA
2012
2009
2006
1998
1997
1996
1993
(pg/L) Groundwater in Concentrations TBA and MTBE, BTEX, TPH, Maximum of Summary
- 2
Table
detected not = ND
analyzed not = NA
MTBE
TBA
NA
NA
NA
NA
NA
NA
1.9
NA
0.0021
12
3.7
2.2
3.9
2.7
44
240
0.0037
17
110
17
ND
2.3
E
X
210
886.74
2,100
55
9.1
22
130
ND
ND
1.5
34
6.1
110
350
54.87
459.93
167.66
430
180
34
T
B
1,400
2,700
0.49
23
1,600
530
150
81
NA
NA
NA
TPHd
2,100
6,306.67
2,200
TPHg
(ARCO) 2012
(Tesoro) 2012
2003
1997
1993
1991
&1987 1986
(mg/kg) Soil in Concentrations TBA and MTBE, BTEX, TPH, Maximum of Summary
-
1
Table
4 Page
Thrifty Panaitescu, Chris Mr.
Chevron Molla, Natasha Ms.
ARCO Christie, Kyle Mr.
2015 24, June
www.s,thlaiwarcis.r.a.c10,/1,,sartc,31.s
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California Southern of District Replenishment Water Ly, Phuong
Division Program Environmental
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Fund Cleanup Tank Storage Underground
Board, Control Resources Water State Jundt, Kathy
2013 10, April Dated Letter Board Regional
cc:
Enclosure:
Officer Executive
P.E. Unger, Samuel
Sincerely,
iamesw.rvanwaterboards.ca.qov. at or -6711 576 (213)
at IV Ryan W. James Mr. contact please matter, this regarding questions any have you If
law. by authorized action enforcement further
any take to right its reserves Board Regional The 13386. and 13340, 13331, 13304, 13264,
13262, sections Code Water California to pursuant relief injunctive or liabilities civil judicial seek
General Attorney the that request also may Board Regional The 13328. through 13323 sections
Code Water to pursuant Board Regional the by administratively imposed or 25299(d)(2)
section to pursuant action civil by imposed be may penalty civil A violation. of day each for tank
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6
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Thrifty Panaitescu, Chris Mr.
Chevron Molla, Natasha Ms.
ARCO Christie, Kyle Mr.
2015 24, June
.
www,waierboards.ca.gov/losangelos
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90013 CA An0919s, Los 200, Suite
(MINCES EXECUTIVE UNGER. SAMUEL
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date); repair
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Report); Assessment Site of copy (e.g., information release Contaminant
address; mailing Facility
any; if address, email and number, phone name, person's contact Facility
4.
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2,
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we review, our facilitate To
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site.
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activities) monitoring and/or (assessment action corrective overseeing for agency regulatory
uses beneficial all 'for
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public the is Region, -Angeles Los Board, Control Quality Water Regional California The
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environment. the and safety, health, human of protection ensure
action Corrective
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to required is (ARCO)
and SOil Assessment, Site Preliminary (i.e., action corrective take
site. the at
Company Richfield Atlantic 25296.10, section Code Safety and Health to Pursuant
on Based Co. Oil Thrifty by submitted
contamination groundwater and soil there,is report, this
office This
2013, 1,. February dated Report," Baseline II "Phase entitled report the reviewed
Skance: Mr. Dear
I-00626B) (l.D.
CALIFORNIA MALIBU, ROAD, HEATHERCLIFF 29145
#9615. STATION ARCO FORMER
Information Additional for. Request
2720-2727 Sections Regulations,
of Code California 23, Title and 25296.10 Section Code Safety and Health
to Pursuant Release Tank Storage Underground Unauthorized to. Response
- Program Tank Storage Underground
Corrective Take to Directive
in Action
94583 CA Ramon, San
1257 Box P.O.
Company Richfield Atlantic
Skance John Mr.
2013 10, April
Board Control Quality Water Regional Angeles Los
Boards Water
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EXEGUTIvE UNOEFL SAMUEL
CHAIR MEHRANIAN, MARIA
status, well monitoring product, free to depth elevation, (i.e., information groundwater
with together data) survey elevation and longitude, latitude, (i.e., wells monitoring
groundwater all for data locational submit to required also are you regulations,
same the Per
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periodic activities, assessment site removal, system tank storage underground
for completed sampling any include would This 2001. 1, September after obtained
samples groundwater and/or soil any databasefOr GeoTracker SWRCB's the to Format
Deliverable Electronic the in Internet over.the data laboratory all submit to required are
you regulations, above the with accordance http://oeotrackerwaterboards.ca.dovin at
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California of 23 Title of 3 Division 30, Chapter in regulations revise to resolution the
adopted (SWRCB) Board Control Resources Water State the 2004, 30, September On
Database. Internet Geotracker
State the to Data Laboratory of Submission Electronic for Requirement Regulatory
11.
2013. 15, June than later no Board, Regional this to due is information
requested above The aboye. stated requirement the with comply shall owner new
The changes. owner(s) property the if information contact new provide to responsible
also are You site. the from. contamination by impacted owner(s) property other any to
and site the of owner property the to directly sent be also shall reports technical future of
Copies form.pdf). http://www.waterboards.ca.qov/losangeles/htMl/proqrams/ust/AB681
each
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of record county of copy a with together site, subject the from releases by impacted
property(ies) offsite any and site subject the for holders title fee record any for number
phone and address, mailing name, the Board Regional this to provide to required
are you Therefore, owners. property offsite notify to required also are we property, offsite
impacted have systems tank storage underground the from release(s) that indicate
site the from data action corrective If closure. case or cleanup and action corrective
considering to prior tanks storage underground from releases by impacted sites
or site subject the for holders title fee current all notify to required is Board Regional
the 681, AB under Act Control Quality Water Cologne Porter the of 7 Division and
25299.37.2) (Section 6.75 Chapter Code Safety and Health California the to Pursuant
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Information Owner Property
any; if report(s), remediation and/or assessment site previous all of Copies
documentation; disposal Tank
- 2 -
2013 10, April
5.
Company Richfield Atlantic
Skance John Mr:
wwwmalerboards.co.govilostingeles
I
50013 CA Angeles, Los 200, Suite St.. Ath West 320
OFFICER EXEOUTIVE UNGER. SAMUEL
F
oimin MEHNANIAN, MARIA
Co. ThriftyOil Panaitescu, Chris
Services Health of Department Angeles, Los of County Lavin, Richard
California Southern of District Replenishment Water Ly, Phuong
Division
Program Environmental Works, Public of Department County Angeles Los Smith, Tim
Fund Cleanup
.
Tank Storage Underground
Board, Control Resources Water .State Jundt, Kathy
cc:
681) Bill (Assembly Requirements Notification Holder
Title Fee with Compliance for Declaration Certification Program UST Leaking Enclosure:
Coastal Section/LA Tank Underground
Geologist Engineering Associate
.G. C. P.G., Huang, C. ay
Sincerely,
waterboards.ca.gov. ihuang at email an me
send or 576-6711 (213) at me contact please matter, this regarding questions any have you If
Ofor%20G7/020Users.pdf.
http://www.waterboards.ca.gov/losangeles/resources/Paperless/Paperless%200ffice/02
following
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e-QMRGuideline6-04.pdf. 0621 http://www.waterboards.ca.gov/losangeles/html/programs/ust/04
guidelines
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while Tracker, Geo to submitted be also must 2005, 1, January since reports monitoring
and clean-up all of copy complete A 2002. 1, January commencing map site a and etc.)
Company Richfield Atlantic
Skance John Mr.
- 3 -
2013 10, April
Et
JN1It?H3 Vii V
351-4822 (626) FAX
351-4814 (626)
91107 California Pasadena, 204, Suite Villa, Madre Sierra 650
to relinquished were samples groundwater 2 and samples soil 52 of total A California. Irvine,
in located laboratory, Services-certified Health of Department California a Analytical, Mar
Del to submitted were activities field during collected samples groundwater and samples Soil
report.
this to attached sampling groundwater for procedures operating standard the in summarized
procedures using well the from collected were samples Groundwater (TDD-4). well installed
newly the from samples groundwater collect to site the to returned PACIFIC 1997, 25, July On
information'. boring-specific for logs construction well '
and boring soil attached the See depths. drilling and locations boring soil for figure attached
the See well. monitoring groundwater a to converted was borings soil the of One attached.
are wells monitoring groundwater developing and installing, sampling, soil for procedures
operating standard the of copy A wells. monitoring groundwater installing and borings soil
drilling included which islands dispenser the and tanks storage underground the of areas the in
activities investigation site conducted PACIFIC 1997, 21, July and 1997, 26, June On present.
was containment underdispenser since collected samples,were soil No dispenser. each beneath
samples soil collect to site the visited PACIFIC 1997, 27, May On 1997. 22, May on location
borihg soil proposed each clear to site the visited E.S.I.), (Spectrum company geophysical
a USA, to addition In drilling. the of notified was (USA) Alert Service Undergrotind
locations. boring soil proposed the mark to site the visited PACIFIC 1997, 8, May On
Work of Scope
attachments. enclosed
the in and below paragraphs the in summarized are investigation subsurface the of Results
CA. Malibu, Road, Heathercliff 29145 at conditions subsurface related environmentally
baseline to was investigation the of purpose The site. subject the at investigation subsurface
baselining a conduct to contracted was (PACIFIC) Inc. Group, Environmental Pacific
Thrifty: Dear
732-038.1A No. Project PACIFIC
California Malibu,
Road Heathercliff 29145
213 No. Station Service Thrifty
Report Investigation Subsurface Baselining.
Subject:
90670 California Springs, Fe Santa
Road Foster East 13539
Company Oil Thrifty
1997 22, December
INC. GROUP
ENVIRONMENTAL
PACIFIC
Manager Project
stana, P P. Gary
DOC \PROJECT\732\REPORTS\9615-213.
Luka Kateri cc:
Geologist Staff Sr.
Rohlfing Chris
INC. GROUP, ENVIRONMENTAL PACIFIC
Sincerely,'
351-4814. (626) at undersigned the of either call please questions, any have should you If
intended. or implied is warranty
no this, than Other location'. and time this at practices engineering and hydrogeologic accepted
currently with accordance in at arrived are and information available currently on based are
opinions These opinions. professional our represents report this in contained information The
Comments Closing
(bgs). surface ground below
feet 84 approximately of depth a at encountered was Groundwater investigation. the of depth
total the to surface ground from sand silty and sand of predominantly consisted investigation
site the during, encountered types Soil 1961). (DWR, depth unknown an to Formation
Monterey Miocene the of consists lithology the deposits age Quaternary the Beneath deposits.
marine and colluvial Quaternary by underlain is site The 1950). (USGS, foot per foot 0.033
approximately at southeast the to slopes topography Local (ust). level sea mean above feet
206 approximately of elevation an at Malibu of City the in located is 213 No. Station Thrifty
Geology Site
report. this to attached destruction well for procedures operating standard the in summarized
method grout pressure the using abandoned was TDD-4 well Monitoring Groundwater
activities. abandonment well conduct to site the to returned PACIFIC 1997, 15, September On
attached. are reports analytical certified the of Copies respectively. 2, arid 1 Tables
in summarized are analyses sample groundwater and sample soil of Results metals. 22 title and
compounds, organic volatile hydrocarbons, petroleum recoverable total ether, tert-butyl methyl
xylenes, ethylbenzene, toluene, benzene, diesel, and gasoline as hydrocarbons petroleum
total for analyzed were samples groundwater 2 and samples soil 15 of total A laboratory. the
,
2 Page
732-038.1A No. Project PACIFIC
California Malibu,
213 No. Station Service Thrifty
Report Investigation Subsurface BaselininR
GAPROJECT\732\REPORTS\9615-213.60C
Method Grotit Pressure - Wells Extraction Vapor Soil and
Monitoring Groundwater of Destruction Well for Procedure Operating Standard
Techniques Sampling Groundwater for Procedures Operating Standard
Wells Monitoring Groundwater Developing for Procedures Operating Standard
Wells Monitoring Groundwater Installing for Procedures Operating Standard
Techniques Sampling Soil for Procedures Operating Standard
Technique Decontamination Equipment
Documentation Chain-of-Custody and Report Laboratory
Logs Construction 'Soil:Boring/Well
Samples Groundwater - Summary Analytical 2: Table
Samples Soil - Summary Analytical 1: Table
Map Site Geophysical
Locations Boring Soil Showing Plan Site Attachments:
.
3 Page
732-038.1A No. Project PACIFIC
California Malibu,
213 No. Station Service Thrifty
Report Investigation Subsurface lining Base
GAPIWJECT\732\REPORTS\9615-213.DOC
1994. and .1981 photoreyised topographic,
minute 7.5 Quadrangle, Dume Point 1950, (USGS), Survey Geological States United
County. Angeles Los of Plain Coastal the of Basins Water Ground
the of UtilizatiOn Planned 104, No. Bulletin 1961 (DWR), Resources Water of Department
References
4 Page
732-038.1A No. Project PACIFIC
California Malibu,
213 No. Station Service Thrifty
Report Investigation Subsurface lining Base
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APPLICANT
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APPL OF DISPOSITION
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application this Chief, Section by signed When
DATE
DATE
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condition or reason report conditions, with approved or denied if
CONDITIONS WITH APPROVED
DENIED IN
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Services.
Health Preventive/Public County such by necessary
deemed data other any and casing, In perforations all well,
of depth drilled, date giving well, the of log complete a
with Services Health Preventive/Public County the furnish
will I thereafter, days ten within and well of completion
Upon destruction. and reconstruction construction, well
to pertaining California of State the of and Angeles Los of
County the of laws and ordinances all with and Services
Health Preventive/Public County the of regulations
all with respect every in comply to agree hereby I
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RENOVATION OR RECONSTRUCTION El
CONSTRUCTION WELL NEW
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(CHECK) PERMIT OF TYPE
SERVICES HEALTH OF DEPARTMENT ANGELES LOS OF
91754 Ca Park, Monterey
DATE
- SG 1
(01-
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COUNT
Place Corporate 2525 HEALTH ENVIRONMENTAL
PERMIT WELL FOR APPLICATION
COPY SENIOR PINK:
COPY APPLICANT CANARY:
COPY CHIEF WHITE:
1/96 3/91) (Rev. H2124 76S979
materials. ree7cled
STAMP DEPARTMENT
PH411614211
0
OFFICE CONTACT
Application) Renovation or Construction System Disposal Sewage Private for above line (Complete
Bedrooms No.
No. Lot
No. Tract
No. Check Plan Engineer Co.
No. Phone
C/i
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Po-Welis
VA Madre
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FEES. ACCEPT CANNOT PERSONNEL FIELD
91754 Ca Park, Monterey
Place Corporate 2525
Health Environmental
Programs Health Public
Services Health of Department
Angeles Los of County
NOTE:
year. fiscal current for
of Schedule to Refer *
Fees
to:
indicated. forms the
with check or order money application, completed the deliver or information required the Complete
information. or requirements for below stamped Office Contact with Check
3.
2.
Agriculture of Department
U.S. by required as CERTIFICATION AND TEST SUPPLY WATER
FHAJVA by
required as SYSTEM SEWAGE PRIVATE EXISTING OF INSPECTION
Service Forest States United
the by required as SITE CABIN MOUNTAIN OF INSPECTION
RENOVATION/EXPANSION SYSTEM DISPOSAL SEWAGE PRIVATE
PERMIT CONSTRUCTION SYSTEM DISPOSAL SEWAGE PRIVATE
Application Permit Well a attach and Complete
>PERMITTW.JCfibEST( OR RENOVATION CONSTRUCTION, WELL
.
Gr6
CONSTRUCTION/DESTRUCTION WELL MONITORING
SERVICE OF TYPE
133
REQUIRED* FEE
nontransferable. is application This CASH. SEND
NOT DO TREASURER, COUNTY ANGELES LOS to payable check or order money Make tion.
applica- the to fee non-refundable required the attach and requested SERVICE OF TYPE the Check
1.
INSTRUCTIONS
APPLICATION REQUEST SERVICE
HEALTH ENVIRONMENTAL - PROGRAMS HEALTH PUBLIC
SERVICES HEALTH OF DEPARTMENT - ANGELES LOS OF COUNTY
COLLECTION FEE AND APPLICATION SERVICE
2/5
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1997
1997
1997
1997
1997
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Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
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#1197) (ELAP ANALYTICAL MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel Volatile
Benzene
Toluene
mg/Kg
(ppm)
mg/Kg
(ppm)
mg/Kg
0.12
0.14
0.0084
0.063
0.30
0.33
0.029
0.19
0.0050
0.0050
0.015
(PPm)
Benzene
Ethyl
Xylenes
Total
mg/Kg
0.0050
(PPrn)
Limit: Reporting
1.0
1.5
N.D.
(ppm)
mg/Kg
Hydrocarbons
Fuel Volatile
GF05861
TDD-1-15
GF05862
TDD-1-25
Soil
Description
Sample
Number
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
11, Jul
8, Jul
8, Jul
27, Jun
26, Jun
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
GF05861 #: Sample First
O'Connell Erin :.Attention:
8015/8020 Mod. DHS 5030/CA EPA Method: Analysis
91107 CA Pasadena,
Malibu 213,
204
Ste. Villa, Madre Sierra 650
Group Environmental Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
92606
261-1022 (714)
92324 CA Colton, A, Suite Dc, Cooley
370-4667 (909)
91406 CA Nuys,
779-1844 (818)
85281 AZ Tempe,
968-8272 (602)
I, Suite St., 12th W.
2465
Analytical Mar Del
Van C-11, Suite Way, Sherman 16525
E. 1014
CA Irvine, Ave., Alton 2852
:
(
6> of <2 GF05861.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
ohnson Nancy
#1197) (ELAP ANALYTICAL MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C40. to C8 from range method this by detected Hydrocarbons standard. fuel diesel a against quantitated are Hydrocarbons Extractable
Limit: Reporting
5.0
N.D.
N.A.
N.D.
N.A.
GF05861
TDD-1-15
GF05862
TDD-1-25
(PPm)
mg/Kg
Type
Hydrocarbons
Hydrocarbon Extractable
Soil
Description
Sample
Number
Laboratory
8015) EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
1997i 11, Jul
1997i 8, Jul
7, Jul
1997 27, Jun
1997:i.!::
iii
1997g 26, Jun
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
779-1844 (818)
85281 AZ Tempe,
1,
GF05861
#: Sample First
O'Connell Erin Attention:
8015 Mod. DHS 3550/CA EPA Method: Analysis
91107 CA Pasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra 650
#9615-97-01 Auth. Work Thrifty ID: Project Client
92324 CA Colton, A. Suite Dr., Cooley
370-4667 (909)
MarAnalytical Del
E. 1014
(
Group Environmental Pacific 1'
Suite St., 12th W. 2465
91406 CA Nuys, Van C-11. Suite Way, Sherman 16525
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
6> of <3 GF05861.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
on hn
Nancy
#1197) (ELAP ANALYTICAL MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
Ether tert-Butyl Methyl = MTBE
Limit: Reporting
1.0
GF05861
TDD-1-15
N.D.
GF05862
TDD-1-25
N.D.
(PPm)
Description
Sample
Result
Sample
Soil
mg/Kg
Number
Laboratory
MODIFIED) 8020 (EPA MTBE
1997.1::. 11, Jul
199'.0 8, Jul
1 1997 8, Jul
1997.]:]:: 27, Jun
1997:i: 26, Jun
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-1338 (602) FAX 968-8272 (602)
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
779-1844 (818)
370-4667 (909)
261-1022 1714)
85281 AZ Tempe,
91406 CA Nuys,
I.
GF05861 #: Sample First
O'Connell Erin Attention:
5030/8020 EPA Method: Analysis
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
Suite St., 12th W. 2465
Analytical Mar Del
Van C-11, Suite Way. Sherman 16525
CA Irvine, Ave., Alton 2852
92606
CA Colton, A, Suite Dr., Cooley E. 1014
92324
(
6> of <4 GF05861.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Johnson Nancy
en)
#1197) (ELAP ANALYTICAL MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are
Hydrocarbons Fuel Volatile
Benzene
Toluene
Benzene
Ethyl
Xylenes
Total
(ppm)
mg/Kg
(ppm)
mg/Kg
(ppm)
mg/Kg
(ppm)
mg/Kg
N.D.
N.D.
N.D.
0.0050
0.0050
0.015
N.D.
N.D.
1.0
0.0050
Limit: Reporting
Blank Method
(ppm)
mg/Kg
Hydrocarbons
Fuel Volatile
Description
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
Soil
1997 11, Jul
1997 8, Jul
1997 8, Jul
Matrix:
Reported:
Analyzed:
Extracted:
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
CA Irvine, Ave., Alton 2852
92606
-1022 261 (714)
FAX
261-1228 (714)
CA Colton, A, Suite Dr., Cooley E. 1014
92324
-4667 370 (909)
FAX
370-1046 (909)
CA Nuys, Van C-11. Suite Way, Sherman 16525
91406
-1844 779 (818)
FAX
779-1843 (818)
85281 AZ Tempe,
-8272 968 (602)
FAX
968-1338 (602)
I. Suite St., 12th W.
2465
MarAnalytical Del
(
6> of <5 GF05861.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
on John Nancy
,
#1197) (ELAP ANALYTICAL MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C40. to C8 from range method this by detected Hydrocarbons standard. fuel diesel
a
against quantitated are Hydrocarbons Extractable
Limit: Reporting
5.0
N.A.
Blank Method
N.D.
(ppm)
mg/Kg
Type
Hydrocarbon
Hydrocarbons
Extractable
Description
Laboratory
8015) EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
Soil
1997 11, Jul
1997 8, Jul
1997 7, Jul
Matrix:
Reported:
Analyzed:
Extracted:
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
FAX
261-1228 (714)
92324 CA Colton, A, Suite Dr., Cooley
370-4667 (909)
FAX
370-1046 (909)
91406 CA Nuys, Van C-11, Suite Way, Sherman 16525
-1844 (818)779
779-1843 (818) FAX
968-8272 (602)
968-1338 (602)
FAX
85281 AZ Tempe,
I.
Suite St., 12th W. 2465
E.
MarAnalytical Del
1014
IC
6> of <6 GF05861.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Johnson Nancy
#1197) (FLAP ANALYTICAL MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
Ether tert-Butyl Methyl = MTBE
Limit: Reporting
1.0
N.D.
Blank Method
(PPrn)
mg/Kg
Result
Sample
Description
Laboratory
MODIFIED) 8020 (EPA MTBE
Soil
1997 11, Jul
1997 8, Jul
1997 8, Jul
968-1338 (602)
FAX
Matrix:
Reported:
Analyzed:
Extracted:
-8272 968 (602)
779-1843 (818) FAX -1844 779 (818)
FAX
261-1228 (714)
FAX
370-1046 (909)
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe, I, Suite St., 12th
91406
W.
2465
CA Nuys, Van C-11, Suite Way, Sherman 16525
92606
-1022 261 (714)
92324 CA Colton, A, Suite
-4667 370 (909)
Dr., Cooley E. 1014
Analytical Mar Del
CA Irvine, Ave., Alton 2852
(
RPD
PR
MEAN
53%
74%
Analytical Mar Del
R1
Analysis Sample of Result
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
Terms: of Definition
120%
I
28%
PR1
PR2
0/0
cyo
I
110
ppm
MSD
64
I
50
I
ppm
ppm
50
Hydrocarbons
ppm
Sp
MS
R1
Analyte
GG00683
7/7/97
FAX
779-1844 (818)
261-1022 (714)
#: SAMPLE
85281 AZ Tempe. 1. Suite St., 12th W. 2465
91406
779-1843 (818)
FAX
DATE:
Matrix:
METHOD: EPA
Soil
extraction by 8015
968-1338 (602) FAX 968-8272 (602)
92324 CA Colton, A. Suite Dr, Cooley
370-1046 (909) FAX 370-4667 (909)
261-1228 (714)
92606
MarAnalytical Del
CA Nuys, Van C-11, Suite Way, Sherman 16525
E. 1014
CA Irvine, Ave., Alton 2852
(
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
968-8272 (602)
779-1844 (818)
370-4667 (909)
-1022 261 (714)
Analytical Mar Del
St
Concentration Standard
R1
Result Standard
PR
of Recovery Percent
100 X St) / (R1 R1;
Terms: of Definition
R1
PR
ppm
0/0
38
76%
50
Hydrocarbons
ppm
St
Analyte
7/7/97
DATE:
extraction by 8015 METHOD: EPA
85281 AZ Tempe,
91406
92324
1,
Suite St., 12th W. 2465
Analytical Mar Del
CA Nuys, Van C-11, Suite Way, Sherman 16525
CA Colton, A, Suite Dr., Cooley
E.
1014
92606 CA Irvine, Ave., Alton 2852
(
Analytical Mar Del
R1
Analysis Sample of Result
Sp
sample to added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X ((MS-R1)/SP) MS; of Recovery Percent
PR2
100 X ((MSD-R1)/SP) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2) Difference; Percent Relative
PR Mean
Recovery Percent Mean
Limits Acceptance
Charts Control in-house by Determined
Terms of Definition
validation. batch for LCS to Refer *
*
*
RPD
PR Mean
30 5
129 - 81
0.61
91
25 <
115 - 83
2.6
80
25
115 - 80
..25
-115 83
25 <
-118 85
Limits Acceptance
*
84
82
74
5.2
5.4
13
PR Mean
RPD
81
80
78
91
69
PR2
0.25
86
0.26
0.30
0.10
0.093
0.093
90
0.10
0.084
0.081
81
0.085
0.080
85
80
0.10
ppm
ppm
ppm
1.1
0.95
0.84
-
MSD
PR1
Soil
MS
Ethylbenzene
0
Xylenes
0.0013
0.0029
0.0022
0.078
Toluene
Benzene
TPH
ppm
R1
Analyte
Date:
07/08/97
#: Sample
GF05499
#: Batch
GG08151S
Matrix:
8015/8020 Method EPA
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
91406 CA Nuys, Van C-11, Suite Way, Sherman 16525
779-1844 (818)
85281 AZ Tempe,
968-8272 (602)
370-4667 (909)
261-1022 (714)
1,
Suite St., 12th W. 2465
92324 CA Colton, A, Suite
MarAnalytical Del
Dr., Cooley E. 1014
92606 CA Irvine, Ave., Alton 2852
(
Analytical Mar Del
ACP
Recovery Percent for Limits Acceptance
TPH
Hydrocarbons Petroleum Total
LCS
Sample Control Laboratory
Conc Spike
Analysis Sample of Result
Result
Analysis Sample Control Laboratory of Result
%Recovery
100 X Conc.) Spike / Conc.) Spike - ((Result LCS; of Recovery Percent
Terms of Definition
100
85
102
% 115 - 85
-
% 115
-
% 115
-
% 115
-
% 115
85
85
85
ACP
Result
Recovery %
1.1
1.2
107
Benzene
0.10
0.098
98
Xylenes
Ethylbenzene
Toluene
0.10
0.093
93
0.10
0.10
0.30
0.31
Soil
TPH
Conc. Spike
Analyte
Date:
07/08/97
#: Sample
BLANK
#: Batch
GG08151S
Matrix:
8015/8020 Method EPA
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
92324
370-4667 (909)
91406
779-1844 (818)
85281 AZ Tempe, I. Suite St., 12th
968-8272 (602)
261-1022 (714)
W.
2465
CA Nuys, Van C-11, Suite Way, Sherman 16525
CA Colton, A, Suite Dr, Cooley
E
Analytical Mar Del
1014
92606 CA Irvine, Ave., Alton 2852
(
E.
3704667
I. Van Nuys. CA 91406
c.'%
Sample
Description
Vis-- 3S1-L13,iti
Pe'
ii
10
:
4
-d By:
.
,
('
.
3.
/
t(
11
1/
if
261-1228
19091370.1046
7
II
,4
/6S
to /Time:
D- e /Ti e:
Date /Time
/1
0
.)
)'
24-44s5
L t rJeL
V
C-,1
-
0'
/
/
(
/
i
4:.C11
)" -(..
ci,
(
-fittt
ti
n.,
r,
.
G.,'
s-7:'
q.44../._
If
-?%5(,
Sampling
Date/Time
G zki -.11
(
I
O
0
ed
-
.it
1-
Filt6..
....
,)
E
9,.
\---
'5
r.,
V)
r)
,
')(
'I
''.--7
/Time:
ime:
co.
-?...
y.
Z
+
42
U
4
ate /Time:
-
,
Date
jo.tL Dat
00
_C
ffX 7\ X
"r-r/fillii
'
in Lab by:
'
by
, 1e-
Re
I/
k
//
it
Ec---..
Preservatives kici
It "7 '7._. - 03% ,
s11-10\-A-:.--)
1---1
#of
Cont
e
C.....\....:,
Sampler:
V1
C
____.-
intact
:)
days
on is
(Check)
normal
5
\--V
Special Instructions
(LosN....\-t4
72 hours
(check)
-"X
....
_IntegXr2ity:
Sample
48 hours
24 hours
same day
0
'-
Q
TM6G-
qGis-cri-0/
X--v,
Turnaround Time:
Analysis Required
6 ira
(7,-
CHAIN OF CUSTODY FORM
1\;,5,-1
4
1,,,,,t,,.cl.k Pc"
968 1338
Project/PO Number:
klr113
FAX (607)
Sample Container
Matrix
Type
16021968 8772
..--C---t:-
_
FAX
FAX 1714)
03181779 1844 FAX 18181779.1843
Note: Sample(s) will be disposed of after 30 days.
I
ReIrnu
'
By:
rRelinquished
l
..41
e !Wished
Air
1r i
L1411*-17471'
,'7 1-6)1) - 1- D. 0
.
ou --1--
lvvT,, -,.4, '"
/
t-- _
V
Project Manager/Phone Number:
s_,-frx
c-0 iv....\1
( t-- - / -sTo
er
C I
L_. .Y.,0,-,4\ i"--g-
-,1c:( 0:l
Client Name/Address:
lo.....-,-.
.
2465 W 121119 Suite I, Tempe. AZ 85281
19091
Cowl. CA 92324
.
Cooley Dr Suite A.
16525 Sherman Way. Suite
1014
(7141261 1021
2852 Alton Aye.. Irvine. CA 92714
Del Mar Analytical
1997i:
38> of <1 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Linsel Ann Mary
#1865) (ELAP NUYS VAN ANALYTICAL, MAR DEL
6. of factor a by raised been have sample this for limits Reporting dilution. required
sample the factors, other and/or effects matrix to Due limit. reporting the above or at present not were N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel Volatile
Toluene
Benzene
Ethyl
Xylenes
Total
mg/Kg
mg/Kg
mg/Kg
(PPrn)
(PPrn)
(PM')
0.89
0.084
0.58
1.6
0.12
0.76
0.030
0.030
0.090
(PPrn)
(ppm)
mg/Kg
7.1
0.44
8.2
0.85
6.0
0.030
Benzene
Limit: Reporting
V7071262
TDD-1-40
V7071263
TDD-1-50
Description
Hydrocarbons
Fuel Volatile
Soil
mg/Kg
Sample
Number
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION DROCARBONS/I3TEX HY FUEL VOLATILE
1,
Aug
1997:::::: 30, Jul
1997:i:i: 30, Jul
1997 24, Jul
1997i:ii 21, Jul
Reported:
Analyzed:
Extracted:
Received:
Sampled:
:ii:Pacific
FAX
779-1843 (818)
FAX
968-1338 (602)
V7071262 #: Sample
First
O'Connell
Erin Attention:
8015/8020 Mod. DHS 5030/CA EPA Method: Analysis
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra
Group Environmental
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
91406
779-1844 (818)
85281 AZ Tempe.
968-8272 (602)
1,
Suite St., 12th W. 2465
MarAnalytical Del
CA Nuys, Van C-11, Suite Way. Sherman 16525
92606
261-1228 (714) FAX 261-1022 (714)
92324 CA Colton, A, Suite Or., Cooley
370-1046 (909) FAX 370-4667 (909)
E. 1014
CA Irvine, Ave., Alton 2852
i
(
38> of <2 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lin Ann Mary
I
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel Volatile
Benzene
Ethyl
Xylenes
Total
(ppm)
mg/Kg
(ppm)
mg/Kg
(ppm)
mg/Kg
0.14
0.13
0.025
0.16
0.0050
0.0050
0.0050
0.015
Toluene
(ppm)
mg/Kg
1.0
N.D.
Limit: Reporting
TDD-2-25
V7071264
(PPm)
mg/Kg
Benzene
Hydrocarbons
Fuel Volatile
Soil
Description
Sample
Number
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
19971 1, Aug
19971:: 29, Jul
1997F 29, Jul
1997 24, Jul
1997:::: 21, Jul
Reported:
Analyzed:
Extracted:
Received:
Sampled:
V7071264 #:
Sample
First
O'Connell
Erin Attention:
8015/8020 Mod. DHS 5030/CA EPA Method: Analysis
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra ii!:!650
Group Environmental Pacific
Malibu 213,
91406
779-1843 (818) FAX 779-1844 (818)
85281 AZ Tempe,
968-1338 (602)
FAX
FAX
968-8272 (602)
#9615-97-01 Auth. Work Thrifty ID: Project Client
92324 CA Colton, A, Suite Dr., Cooley
370-1046 (909) FAX 370-4667 (909)
261-1228 (714)
261-1022 (714)
I,
Suite St., 12th W. 2465
Analytical Mar Del
CA Nuys, Van C-11, Suite Way. Sherman 16525
E. 1014
0(
92606 CA Irvine, Ave., Alton 2852
38> of <3 PEG V7071262.
Analytical. Mar Del from permission written without full, In except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lintel Ann Mary
c,
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
50. of factor a by raised been have sample this for limits Reporting dilution. required
sample the factors, other and/or effects matrix to Due limit. reporting the above or at present not were N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel Volatile
Benzene
Ethyl
Xylenes
Total
mg/Kg
mg/Kg
(PPm)
(PPm)
2.3
17
0.25
0.75
0.25
Description
Sample
Hydrocarbons
Fuel Volatile
Benzene
Soil
mg/Kg
mg/Kg
mg/Kg
(PPm)
(PPm)
(PPm)
150
0.61
5.3
50
0.25
Toluene
Limit: Reporting
TDD-2-30
V7071265
Number
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
::ii 1997
1, Aug
1997;i:i:i 29, Jul
1997 29, Jul
ii,' 1997
24, Jul
1997 21, Jul
:::
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
.,.
V7071265 #: Sample First
O'Connell Erin :::::Attention:
,.,
8015/8020 Mod. DHS 5030/CA EPA Method:
Analysis
91107 CA Pasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra iiiii650
Group Environmental Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe,
1.
:1:.
Suite St., 12th W. 2465
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
92324 CA Colton,
370-4667 (909)
91406 CA Nuys, Van C-11, Suite Way, Sherman 16525
779-1844 (818)
Analytical Mar Del
A, Suite Dr, Cooley E. 1014
1997
1997
1997
1997
1997
38> of <4 PEG V7071262.
Analytical.Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lin Ann Mary
#1856) (ELAP NUYS VAN ANALYTICAL, MAR DEL
60. of factor a by raised been have sample this for limits Reporting dilution. required
sample the factors, other and/or effects matrix to Due limit. reporting the above or at present not were
N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against
quantitated are Hydrocarbons Fuel Volatile
Benzene
Ethyl
Xylenes
Total
mg/Kg
(PPrn)
1.1
8.3
0.30
0.90
Description
Sample
Hydrocarbons
Fuel Volatile
Benzene
Soil
mg/Kg
Toluene
mg/Kg
mg/Kg
mg/Kg
(PPm)
(PPrn)
(PPrn)
(PPrn)
95
1.5
6.1
0.30
0.30
60
TDD-3-25
Limit: Reporting
V7071266
Number
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
1, Aug
Jul
Jul
Jul
Jul
29,
29,
24,
21,
968-1338 (602)
FAX
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
V7071266 #: Sample First
O'Connell Erin :!Attention:
8015/8020 Mod. DHS
5030/CA
EPA
Method:
Analysis
91107 CA Pasadena,
Malibu 213,
204
Ste. Villa, Madre Sierra 650
Group Environmental Pacific $
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe,
1,
Suite St., 12th W. 2465
CA Irvine, Ave., Alton 2852
92606
CA Colton, A, Suite Dr., Cooley E. 1014
92324
370-4667 (909)
91406
779-1843 (818) FAX 779-1844 (818)
FAX
261-1228 (714)
FAX
370-1046 (909)
261-1022 (714)
CA Nuys, Van C-1I, Suite Way, Sherman 16525
MarAnalytical Del
(
38> of <5 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lin Ann Mary
I
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
4. of factor a by raised been have sample this for limits Reporting dilution. required
sample the factors, other and/or effects matrix to Due limit. reporting the above or at present not were N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel Volatile
Toluene
Benzene
Ethyl
Xylenes
Total
(ppm)
mg/Kg
(ppm)
mg/Kg
(ppm)
mg/Kg
0.50
4.6
0.020
0.060
Description
Sample
Hydrocarbons
Fuel Volatile
Soil
(ppm)
mg/Kg
(ppm)
mg/Kg
29
0.53
1.7
0.020
0.020
4.0
Benzene
Limit: Reporting
TDD-3-40
V7071267
Number
Laboratory
:::::*:::::::::::::::::::::::::::::::::::::::::
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
1997::: 1, Aug
1997:::::: 29, Jul
1997:::: 29, Jul
1997:: 24, Jul
21, Jul
1997::::::
Reported:
Analyzed:
Extracted:
Received:
Sampled:
V7071267 #: Sample First
O'Connell Erin ':;Attention:
8015/8020 Mod. DHS 5030/CA EPA
Method:
Analysis
91107 CA Pasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra 1650
Group Environmental Pacific gi
:::
#9615-97-01 Auth. Work Thrifty ID: Project Client
iiiiiiiiiiiiiiiiiiiiiiiiiiiiiii*iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii0iiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiiii:
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
968-8272 (602)
779-1844 (818)
370-4667 (909)
261-1022 (714)
Kiiiiiiiiiiiiii
85281 AZ Tempe. I, Suite St., 12th W. 2465
91406
Analytical Mar Del
CA Nuys, Van C-II, Suite Way, Sherman 16525
92324 CA Colton,
92606
A, Suite Dr., Cooley E. 1014
CA Irvine. Ave., Alton 2852
(
38> of <6 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Linsel Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel Volatile
Description
Sample
Hydrocarbons
Fuel Volatile
Soil
(ppm)
mg/Kg
(ppm)
mg/Kg
V7071268
TDD-4-35
N.D.
N.D..
N.D.
V7071269
TDD-4-50
N.D.
N.D.
N.D.
V7071270
TDD-4-85
N.D.
N.D.
N.D.
N.D.
V7071271
TDD-5-25
N.D.
N.D.
N.D.
N.D.
N.D.
V7071272
TDD-5-40
N.D.
N.D.
N.D.
N.D.
N.D.
1.0
0.0050
0.0050
0.0050
0.015
Toluene
Benzene
Ethyl
Xylenes
Total
(ppm)
mg/Kg
(ppm)
mg/Kg
(ppm)
mg/Kg
N.D.
N.D.
N.D.
N.D.
N.D.
Benzene
Limit: Reporting
Number
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
1997;i:::: 1, Aug
1997:::i:i 28-31, Jul
1997 28-31, Jul
1997 24, Jul
iiiiii
iiiiii
19971 22, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
...
..
...
V7071268 #:
Sample
First
O'Connell
Erin :::::Attention:
8015/8020 Mod. DHS 5030/CA EPA Method:
Analysis
91107 CA Pasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra :::i650
Group Environmental :::Pacific
<:
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe,
I,
Suite
92324 CA Colton,
370-4667 (909)
91406 CA Nuys, Van
779-1844 (818)
261-1022 (714)
C-11,
,
St 12th W. 2465
MarAnalytical Del
Suite Way, Sherman 16525
Dr, Cooley
A. Suite
E. 1014
92606 CA Irvine, Ave., Alton 2852
(
38> of <7 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Linsel Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel Volatile
Benzene
Ethyl
Xylenes
Total
(PPrn)
(ppm)
mg/Kg
mg/Kg
0.0057
0.034
0.052
0.015
(PPm)
Description
Hydrocarbons
Fuel Volatile
Benzene
Soil
mg/Kg
mg/Kg
(PPrn)
(PPIn)
V7071273
TDD-6-30
N.D.
0.023
0.045
V7071274
TDD-6-40
N.D.
0.057
0.10
0.010
1.0
0.0050
0.0050
0.0050
mg/Kg
Toluene
Sample
Limit: Reporting
Number
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
1997 1, Aug
1997 29, Jul
1997 29, Jul
1997 24, Jul
19971 23, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
779-1844 (818)
V7071273 #: Sample First
O'Connell Erin i!.Attention:
8015/8020 Mod. DHS 5030/CA EPA Method: Analysis
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra .650
Group Environmental Pacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe, I, Suite St., 12th
91406 CA Nuys,
W.
2465
Analytical Mar Del
Van C-11, Suite Way, Sherman 16525
92606 CA Irvine, Ave.. Alton 2852
261-1022 (714)
92324 CA Colton, A, Suite
370-4667 (909)
Dr., Cooley E. 1014
38> of <8 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lins Ann Mary
I
aA.
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
Ether tert-Butyl Methyl = MTBE
0.050
Limit: Reporting
V7071262
TDD-1-40
N.D.
V7071263
TDD-1-50
N.D.
V7071264
TDD-2-25
1.9
(PPrn)
Description
Sample
Result
Sample
Soil
mg/Kg
Number
Laboratory
MODIFIED) 8020 (EPA MTBE
1997:ii 1, Aug
29, Jul
1997::::::,.
1997:::: 29, Jul
199T::: 24, Jul
1997:::: 21, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
91406
779-1844 (818)
85281 AZ Tempe,
968-8272 (602)
370-4667 (909)
261-1022 (714)
I,
V7071262 #:
Sample
First
O'Connell
Erin :::Attention:
5030/8020 EPA Method: Analysis
91107 CA Pasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra :::650
Group Environmental Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
Suite St., 12th W. 2465
CA Nuys, Van C-11, Suite Way, Sherman 16525
92324 CA Colton, A. Suite
Dr.. Cooley E. 1014
Analytical Mar Del
92606 CA Irvine, Ave., Alton 2852
38> of <9 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Libel Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
50. of factor a by raised been have sample this for limits Reporting dilution. required
sample the factors, other and/or effects matrix to Due limit. reporting the above or at present not were N.D. as reported Analytes
Ether tert-Butyl Methyl = MTBE
2.5
Limit: Reporting
Soil
(ppm)
mg/Kg
TDD-2-30
N.D.
Result
Sample
Description
Sample
V7071265
Number
Laboratory
MODIFIED) 8020 (EPA MTBE
1997:::: 1, Aug
1997 29, Jul
1997 29, Jul
19971 24, Jul
19971 21, Jul
Reported:
Analyzed:
Extracted:
Received:
Sampled:
V7071265 #: Sample First
O'Connell Erin :iAttention:
5030/8020 EPA Method: Analysis
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
92606 CA Irvine. Ave., Alton 2852
261-1022 (714)
FAX
261-1228 (714)
92324 CA Colton, A, Suite Dr., Cooley
370-4667 (909)
FAX
370-1046 (909)
91406
779-1844 (818)
FAX
779-1843 (818)
85281 AZ Tempe, I. Suite St., 12th
968-8272 (602)
FAX
968-1338 (602)
W.
2465
CA Nuys, Van C-11, Suite Way. Sherman 16525
MarAnalytical Del
E. 1014
1997::::::
38> of <10 V7071262.PEG
Analytical. Mar Del from permission written without full, In except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lin Ann Mary
#1855) (E,,4AP NUYS VAN ANALYTICAL, MAR DEL
60. of factor a by raised been have sample this for limits Reporting dilution. required
sample the factors, other and/or effects matrix to Due limit. reporting the above or at present not were N.D. as reported Analytes
Ether tert-Butyl Methyl
3.0
= MTBE
Limit: Reporting
Description
Sample
Result
Sample
Soil
(ppm)
mg/Kg
TDD-3-25
N.D.
V7071266
Number
Laboratory
MODIFIED) 8020 (EPA MTBE
1, Aug
Jul
Jul
1997 29,
1997:g 29,
1997:111 24,
21,
1997:1::!
Jul
Jul
Reported:
Analyzed:
Extracted:
Received:
Sampled:
92606
261-1022 (714)
FAX
261-1228 (714)
92324
370-4667 (909)
FAX
370-1046 (909)
91406 CA Nuys,
779-1844 (818)
FAX
779-1843 (818)
968-8272 (602)
FAX
968-1338 (602)
V7071266 #: Sample First
O'Connell
Erin ::Attention:
5030/8020 EPA Method: Analysis
91107 CA Pasadena, ik
204 Ste. Villa, Madre Sierra 1650
Group Environmental Pacific
Malibu 213,
(
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe, 1, Suite St., 12th W. 2465
MarAnalytical Del
Van C-11, Suite Way, Sherman 16525
CA Colton, A, Suite Dr., Cooley E. 1014
CA Irvine, Ave., Alton 2852
ii
38> of <11 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
el Li Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
4. of factor a by raised been have sample this for limits Reporting dilution. required
sample the factors, other and/or effects matrix to Due limit. reporting the above or at present not were N.D. as reported Analytes
Ether tert-Butyl Methyl = MTBE
0.20
Limit: Reporting
Description
Sample
Result
Sample
Soil
(ppm)
mg/Kg
TDD-3-40
0.65
V7071267
Number
Laboratory
MODIFIED) 8020 (EPA MTBE
1 1997 1, Aug
1997iiiii 29, Jul
1997P 29, Jul
1997 24, Jul
19971 21, Jul
Reported:
Analyzed:
Extracted:
Received:
Sampled:
...
V7071267 #: Sample First
O'Connell Erin Attention:
5030/8020 EPA Method: Analysis
91107 CA Pasadena, '>
Malibu 213,
204 Ste. Villa, Madre Sierra ::::650
::::i
(
#9615-97-01 Auth. Work Thrifty ID: Project Client
Group Environmental Pacific
::::::::::*::::;:::::::::::::::::x:ix::::ix:::::::::::::::::::::::::::::::;xiv
968-1338 (602) FAX 968-8272 (602)
85281 AZ Tempe, I. Suite St.. 12th
W.
92606 CA Irvine, Ave.. Alton 2852
261-1022 (714)
FAX
261-1228 (714)
92324 CA Colton, A, Suite Dr, Cooley
370-4667 (909)
FAX
370-1046 (909)
FAX
779-1843 (818)
779-1844 (818)
91406
2465
CA Nuys, Van C-11, Suite Way. Sherman 15525
E. 1014
Analytical Mar Del
i::
38> of <12 PEG V7071262.
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
el Lin Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
Ether tert-Butyl Methyl = MTBE
0.050
Limit: Reporting
Description
Sample
Result
Sample
Soil
(ppm)
mg/Kg
V7071268
TDD-4-35
N.D.
V7071269
TDD-4-50
N.D.
V7071270
TDD-4-85
N.D.
W071271
TDD-5-25
N.D.
W071272
TDD-5-40
N.D.
Number
Laboratory
MODIFIED) 8020 (EPA MTBE
1997:: 1, Aug
1997 28-31, Jul
1997 28-31, Jul
1997:: 24, Jul
22, Jul
1991
968-1338 (602)
FAX
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
779-1843 (818) FAX 779-1844 (818)
85281 AZ Tempe,
91406 CA Nuys,
V7071268 #: Sample First
O'Connell Erin Attention:
5030/8020 EPA Method: Analysis
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
I, Suite St., 12th W.
2465
MarAnalytical Del
Van C-II, Suite Way, Sherman 16525
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
FAX
261-1228 (714)
92324 CA Colton, A. Suite
370-4667 (909)
FAX
-1046(9091370
Dr., Cooley E. 1014
(
1997E
38> of <13 V7071262,PEG
Analytical. Mar Del from permission written without full, In except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
I
Manager Project
Lin Ann Mary
tAkA..1)
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
Ether tert-Butyl Methyl = MTBE
0.050
Limit: Reporting
V7071273
TDD-6-30
N.D.
W071274
TDD-6-40
N.D.
(PPrn)
Description
Sample
Result
Sample
Soil
mg/Kg
Number
Laboratory
MODIFIED) 8020 (EPA MTBE
1,
1997 29,
1997:i:i 29,
19971: 24,
't997 23,
Aug
Jul
Jul
Jul
Jul
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-1338 (602) FAX 968-8272 (602)
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
85281 AZ Tempe,
I,
V7071273 #: Sample First
O'Connell Erin !Attention:
5030/8020 EPA Method: Analysis
91107 CA Pasadena,
Malibu 213,
204
Ste. Villa, Madre Sierra 1650
Group Environmental Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
Suite St., 12th W. 2465
CA Irvine, Ave., Alton 2852
92606
261-1022 (714)
CA Colton, A, Suite Dr., Cooley E. 1014
92324
370-4667 (909)
91406 CA Nuys. Van C-11, Suite Way, Sherman 16525
779-1844 (818)
Analytical Mar Del
(
38> of <14 PEG V7071262.
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lin Ann Mary
#1855)
P
(E NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C40. to C8 from range method this by detected Hydrocarbons standard. fuel diesel a against quantitated are Hydrocarbons Extractable
5.0
Limit: Reporting
V7071262
TDD-1-40
V7071263
TDD-1-50
5.7
V7071264
TDD-2-25
N.D.
N.A.
V7071265
TDD-2-30
81
C8-C32
V7071266
TDD-3-25
26
C8-C32
V7071267
TDD-3-40
46
C8-C32
N.D.
N.A.
C8-C32
(PPrn)
mg/Kg
Type
Hydrocarbons
Hydrocarbon Extractable
Soil
Description
Sample
Number
Laboratory
8015) EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
1997:;::: 1, Aug
Jul
Jul
Jul
Jul
1997!1ii 28,
1997 25,
1997:i; 24,
1997 21,
iii
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
V7071262 #: Sample First
O'Connell Erin Attention: ii
8015 Mod. DHS 3550/CA EPA Method: Analysis
91107 CA Pasadena, i!i
Malibu 213,
204
Ste. Villa, Madre Sierra :i650
Group Environmental Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
92324 CA Colton, A, Suite
370-4667 (909)
91406 CA Nuys,
779-1844 (818)
85281 AZ Tempe, I, Suite St., 12th W 2465
968-8272 (602)
Mar-Analytical Del
Van C-11, Suite Way, Sherman 16525
Dr., Cooley E. 1014
38> of <15 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
sel L Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
C40. to C8 from range method this by detected Hydrocarbons standard. fuel diesel a against quantitated are Hydrocarbons Extractable
5.0
Limit: Reporting
Soil
(ppm)
mg/Kg
V7071268
TDD-4-35
N.D.
N.A.
V7071269
TDD-4-50
N.D.
N.A.
V7071271
TDD-5-25
N.D.
N.A.
V7071272
TDD-5-40
N.D.
N.A.
Type
Hydrocarbons
Hydrocarbon
Extractable
Description
Sample
Number
Laboratory
8015) EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
1997 1, Aug
1997 29-30, Jul
1997:0:: 28, Jul
1997:0:: 24, Jul
1997< 22, Jul
Reported:
Analyzed:
Extracted:
Received:
Sampled:
V7071268 #: Sample First
O'Connell
Erin ;Attention:
8015 Mod. DHS 3550/CA EPA Method: Analysis
91107 CA ::::Pasadena,
204 Ste. Villa, Madre Sierra $650
Group Environmental Pacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
FAX
261-1228 (714)
92324 CA Colton,
370-4667 (909)
FAX
370-1046 (909)
91406 CA Nuys,
779-1844 (818)
FAX
779-1843 (818)
85281 AZ Tempe,
968-8272 (602)
FAX
968-1338 (602)
I,
Suite St., 12th W. 2465
Analytical Mar Del
Van C-11, Suite Way, Sherman 16525
A. Suite Dr., Cooley E. 1014
38> of <16 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Linsel Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
2. of factor a by raised been have sample this for limits Reporting dilution. required
sample the factors, other and/or effects matrix to Due limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
C40. to 08 from range method this by detected Hydrocarbons standard. fuel diesel a against quantitated are Hydrocarbons Extractable
10
C8-C37
42
(ppm)
mg/Kg
Type
Hydrocarbons
Hydrocarbon Extractable
8015)
1997:ii1i 1, Aug
1997;:::: 29-30, Jul
19971 28, Jul
1997': 24, Jul
19971 22, Jul
968-1338 (602)
FAX
TDD-4-85
Limit: Reporting
V7071270
Soil
Number
Laboratory
V7071270 #: Sample First
O'Connell Erin Attention: :
8015 Mod. DHS 3550/CA EPA Method: Analysis
91107 CA Pasadena,
Malibu 213,
204
Ste. Villa, Madre Sierra i:::::650
Group Environmental Pacific fiii
',..:
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe, I, Suite St., 12th
W.
2465
92324
91406 CA Nuys, Van C-1I. Suite Way, Sherman 16525
779-1843 (818) FAX 779-1844 (818)
FAX
Description
Sample
EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
92606
261-1022 (714)
370-1046 (909) FAX 370-4667 (909)
261-1228 (714)
CA Colton, A, Suite Dr. Cooley
E
Analytical Mar Del
1014
CA Irvine, Ave., Alton 2852
(
iii 1997
38> of <17 PEG V7071262.
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lins Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C40. to C8 from range method this by detected Hydrocarbons standard. fuel diesel a against quantitated are Hydrocarbons Extractable
5.0
Limit: Reporting
V7071273
TDD-6-30
N.D.
N.A.
V7071274
TDD-6-40
N.D.
N.A.
(PPrn)
Type
Hydrocarbon
8015)
1,
Aug
1997iii:ii 28, Jul
1997::::::
25, Jul
1997;:;; 24, Jul
1997::! 23, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Description
Sample
Hydrocarbons
Extractable
Soil
mg/Kg
Number
Laboratory
EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
Reported:
Analyzed:
Extracted:
Received:
Sampled:
91406
779-1844 (818)
85281 AZ Tempe,
968-8272 (602)
370-4667 (909)
261-1022 (714)
92324
1,
V7071273 #: Sample First
O'Connell Erin :::Attention:
8015 Mod.
DHS
3550/CA
EPA
Method:
Analysis
91107 CA Pasadena,
Malibu 213,
204
Ste. Villa, Madre Sierra i:i650
Group Environmental Pacific <''
#9615-97-01 Auth. Work Thrifty ID: Project Client
Suite St.. 12th W. 2465
Analytical DelMar
CA Nuys, Van C-11, Suite Way, Sherman 16525
CA Colton, A, Suite
Dr, Cooley
E. 1014
92606 CA Irvine, Ave., Alton 2852
:::11
)7
D7
D7
97
97
38> of <18 V7071262.PEG
82%
98%
101%
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
(74-121) 4-Bromofluorobenzene
(81-117) Toluene-d8
(80-120) Dibromofluoromethane
Limits): (Accept. Recoveries Standard Surrogate
Manager 'roject
Lin Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported knalytes
#1197. ELAP
-
Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
Limit
Reporting
Result
Sample
pg/Kg
pg/Kg
pg/Kg
(PPb)
(PPb)
(PPb)
(PPb)
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
5.0
2.0
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
1,1,2-Trichloroethane
1,1,1-Trichloroethane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Toluene
Tetrachloroethene
1,1,2,2-Tetrachloroethane....
1,1,1,2-Tetrachloroethane....
Styrene
n-Propylbenzene
Naphthalene
chloride Methylene
p-Isopropyltoluene
lsopropylbenzene
Hexachlorobutadiene
Ethylbenzene
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
m,p-Xylenes
o-Xylene
chloride Vinyl
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2,3-Trichloropropane
Trichlorofluoromethane
5.0
2.0
2.0
2.0
5.0
5.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
20
2.0
2.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
2.0
2.0
5.0
2.0
2.0
10
Limit
Reporting
Result
Sample
pg/Kg
Analyte
Trans-1,3-Dichloropropene
:is-1,3-Dichloropropene
1,1-Dichloropropene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloroethane
1,1-Dichloroethane
)ichlorodifluoromethane
,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
)ibromomethane
Dibromoethane ,21,2-Dibromo-3-chloropropane
Jibromochloromethane
.-Chlorotoluene
2-Chlorotoluene
Chloromethane
Thloroform
Thloroethane
Chlorobenzene
tetrachloride carbon
art-Butylbenzene
sec-Butylbenzene
n-Butylbenzene
lromomethane
iromoform
Bromodichloromethane
Jromochloromethane
Iromobenzene
Renzene
,inalyte
8260) (EPA GC/MS by ORGANICS VOLATILE
1 1997 1, Aug
1997:::::: 29, Jul
1997 29, Jul
1997 24, Jul
1997 22, Jul
FAX
261-1228 (714)
1-1228
FAX
370-1046 (909)
1-1046
FAX
779-1843 1818)
1-1843
FAX
968-1338 (602)
1-1338
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
V7071268
Number:
Lab
O'Connell
Erin ,ttention:
TDD-4-35 Soil, Descript: Sample
91107 CA Thsadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental iacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe, I, Suite St.. 12th
779-1844 (818)
91406
W.
I
2465
Analytical Mar Del
CA Nuys, Van C-11, Suite Way, Sherman 16525
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
92324 CA Colton, A, Suite
370-4667 (909)
Dr., Cooley E. 1014
38> of <20 V7071262.PEG
*67%
86%
102%
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
(74-121) 4-Bromofluorobenzene
(81-117) Toluene-d8
Manager Project
Linsel Ann Mary
(80-120) Dibromofluoromethane
Limits): (Accept. Recoveries Standard Surrogate
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
confirmed. was which interference matrix to due was recovery *Low
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
2.0
2.0
5.0
2.0
2.0
10
5.0
2.0
2.0
2.0
5.0
5.0
2.0
Limit
Reporting
Result
Sample
pg/Kg
pg/Kg
(PPb)
(PPb)
2.0
2.0
5.0
2.0
2.0
5.0
20
2.0
2.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
m,p-Xylenes
o-Xylene
chloride Vinyl
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2,3-Trichloropropane
Trichlorofluoromethane
Trichloroethene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Toluene
Tetrachloroethene
1,1,2,2-Tetrachloroethane....
1,1,1,2-Tetrachloroethane....
Styrene
n-Propylbenzene
Naphthalene
chloride Methylene
p-lsopropyltoluene
lsopropylbenzene
Hexachlorobutadiene
Ethylbenzene
Analyte
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
5.0
2.0
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
Limit
Reporting
Result
Sample
pg/Kg
pg/Kg
(PPb)
(PPb)
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,1-Dichloropropene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloroethane
1,1-Dichloroethane
Dichlorodifluoromethane
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dibromomethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
4-Chlorotoluene
2-Chlorotoluene
Chloromethane
Chloroform
Chloroethane
Chlorobenzene
tetrachloride Carbon
tert-Butylbenzene
sec-Butylbenzene
n-Butylbenzene
Bromomethane
Bromoform
Bromodichloromethane
Bromochloromethane
Bromobenzene
Benzene
Analyte
8260) (EPA GC/MS by ORGANICS VOLATILE
1 1997 1, Aug
1997::::$
30, Jul
19971 30, Jul
199r:i: 24, Jul
1997 22, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
779-1844 (818)
370-4667 (909)
261-1022 (714)
V7071270
Number: Lab
O'Connell Erin ;:Attention:
TDD-4-85 Soil, Descript: Sample
91107 CA Pasadena, fill
204 Ste. Villa, Madre Sierra li:!650
Group Environmental Pacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe,
91406 CA Nuys,
I, Suite St., 12th W.
2465
Analytical Mar Del
Van C-11, Suite Way, Sherman 16525
92324 CA Colton,
A, Suite Dr, Cooley
E
1014
92606 CA Irvine, Ave., Alton 2852
(
38> of <21 V7071262.PEG
82%
95%
102%
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
(74-121) 4-Bromofluorobenzene
(81-117) Toluene-d8
Manager Project
Lin Ann Mary
el
(80-120) Dibromofluoromethane
Limits): (Accept. Recoveries Standard Surrogate
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
2.0
2.0
2.0
2.0
2.0
2.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
2.0
2.0
5.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
Limit
Reporting
Result
Sample
pg/Kg
pg/Kg
pg/Kg
(PPb)
(PPb)
(PPb)
(PPb)
5.0
2.0
5.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
2.0
5.0
5.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
20
2.0
2.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
10
5.0
2.0
2.0
Limit
Reporting
Result
Sample
pg/Kg
m,p-Xylenes
o-Xylene
chloride Vinyl
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2,3-Trichloropropane
Trichlorofluoromethane
Trichloroethene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Toluene
Tetrachloroethene
1,1,2,2-Tetrachloroethane
1,1,1,2-Tetrachloroethane
Styrene
n-Propylbenzene
Naphthalene
chloride Methylene
p-lsopropyltoluene
Isopropylbenzene
Hexachlorobutadiene
Ethylbenzene
Analyte
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D
N.D.
N.D.
5.0
2.0
5.0
5.0
5.0
5.0
5.0
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,1-Dichloropropene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloroethane
1,1-Dichloroethane
Dichlorodifluoromethane
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dibromomethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
4-Chlorotoluene
2-Chlorotoluene
Chloromethane
Chloroform
Chloroethane
Chlorobenzene
tetrachloride Carbon
tert-Butylbenzene
sec-Butylbenzene
n-Butylbenzene
Bromomethane
Bromoform
Bromodichloromethane
Bromochloromethane
Bromobenzene
Benzene
Analyte
8260) (EPA GC/MS by ORGANICS VOLATILE
1997 1, Aug
1997: 30, Jul
19971 30, Jul
1997 24, Jul
1997 22, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
V7071271
Lab
Number:
O'Connell
Erin :Attention:
TDD-5-25 Soil, Descript: Sample
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 11650
Group Environmental Pacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
CA Colton. A. Suite Dr., Cooley E. 1014
92324
CA Nuys, Van C-11, Suite Way, Sherman 16525
91406
-1844 779 (818)
85281 AZ Tempe,
8272 968- (602)
92606
-1022 261 (714)
-4667 370 (909)
I, Suite St.. 12th W.
2465
MarAnalytical Del
CA Irvine, Ave., Alton 2852
38> of <22 V7071262.PEG
79%
97%
103%
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
(74-121) 4-Bromofluorobenzene
(81-117) Toluene-d8
Manager Project
bl Lin Ann Mary
(80-120) Dibromofluoromethane
Limits): (Accept. Recoveries Standard Surrogate
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
2.0
2.0
5.0
2.0
2.0
Limit
Reporting
Result
Sample
pg/Kg
(PPb)
5.0
2.0
2.0
2.0
5.0
5.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
20
2.0
2.0
5.0
2.0
N.D.
N.D.
N.D.
2.5
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
10
m,p-Xylenes
o-Xylene
chloride Vinyl
,3,5-Trimethylbenzene 11
1,2,4-Trimethylbenzene
1,2,3-Trichloropropane
Trichlorofluoromethane
Trichloroethene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Toluene
Tetrachloroethene
1,1,2,2-Tetrachloroethane....
1,1,1,2-Tetrachloroethane....
Styrene
n-Propylbenzene
Naphthalene
chloride Methylene
p-Isopropyltoluene
lsopropylbenzene
Hexachlorobutadiene
Ethylbenzene
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
5.0
2.0
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
Limit
Reporting
Result
Sample
pg/Kg
pg/Kg
pg/Kg
(PPb)
(PPb)
Analyte
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,1-Dichloropropene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloroethane
1,1-Dichloroethane
Dichlorodifluoromethane
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dibromomethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
4-Chlorotoluene
2-Chlorotoluene
Chloromethane
Chloroform
Chloroethane
Chlorobenzene
tetrachloride Carbon
tert-Butylbenzene
sec-Butylbenzene
n-Butylbenzene
Bromomethane
Bromoform
Bromodichloromethane
Bromochloromethane
Bromobenzene
Benzene
(PPb)
Analyte
8260) (EPA GC/MS by ORGANICS VOLATILE
1997 1, Aug
1997g 29, Jul
1997g 29, Jul
19971 24, Jul
1997::::::
22, Jul
FAX
261-1228 (714)
FAX
-1046370 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
V7071272
Number: Lab
O'Connell Erin :::::Attention:
TDD-5-40
Soil,
Descript:
Sample
91107 CA iPasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra :i:i650
Group Environmental Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
92606 CA Irvine, Ave Alton 2852
261-1022 (714)
92324 CA Colton, A. Suite
370-4667 (909)
91406 CA Nuys, Van C-11, Suite Way. Sherman 16525
779-1844 (818)
85281 AZ Tempe, 1, Suite St.. 12th W. 2465
968-8272 (602)
Dr..
Cooley
MarAnalytical Del
E. 1014
.
38> of <23 PEG V7071262.
Analytical. Mar Del from permission written without full, in except reproduced,
be not shell report This laboratory. the in tested samples to only pertain Results
Manager Project
Lins Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
5.0
Limit: Reporting
Description
Sample
Hydrocarbons
Petroleum
Soil
(ppm)
mg/Kg
V7071268
TDD-4-35
27
V7071269
TDD-4-50
8.6
V7071270
TDD-4-85
22
V7071271
TDD-5-25
23
V7071272
TDD-5-40
21
Number
Laboratory
418.1) (EPA HYDROCARBONS PETROLEUM RECOVERABLE TOTAL
1997::'::::. 1, Aug
1997:*:: 30, Jul
1997::::.: 30, Jul
1997::: 24, Jul
1997::' 22, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
779-1844 (818)
370-4667 (909)
261-1022 (714)
V7071268 #: Sample First
O'Connell Erin :Attention:
clean-up) with (I.R. 418.1 EPA Method: Analysis
91107 CA Pasadena,
204 Ste, Villa, Madre Sierra 650 ii
Group Environmental Pacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe, 1, Suite St., 12th
91406 CA Nuys,
92324
92606
W.
2465
Analytical Mar 'Del
Van C-11, Suite Way. Sherman 16525
CA Colton, A, Suite Dr., Cooley E. 1014
CA Irvine, Ave., Alton 2852
(
38> of <24 W071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lin Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
110
1.0
1.0
10
1.0
EPA
STLC
TTLC
Reporting
Method
Sample
TTLC
Limit Max.
Limit Max.
Limit
Result
mg/L
mg/Kg
mg/Kg
mg/Kg
(PPrn)
(PPrn)
(PPrn)
(PPm)
15
2.0
D. N.
1.0
0.75
75
10000
500
500
10
N.D.
1.0
100
5.0
5.0
5000
2400
700
500
100
2000
3500
20
1000
2500
8000
2500
500
10
45
N.D.
1.8
N.D.
170
31
N.D.
N.D.
N.D.
120
N.D.
0.067
4.7
40
2.0
1.0
1.0
0.020
2.0
1.0
1.0
1.0
0.50
0.50
0.50
METALS
1997::::::
1997:i::::
1, Aug
28-30, Jul
1997:i::: 28, Jul
1997::i:: 24, Jul
1997i 22, Jul
250
24
7.0
5.0
1.0
20
350
0,20
5.0
25
80
100
5.0
6010
6010
6010
6010
6010
6010
6010
7471
6010
6010
6010
6010
7196
6010
6010
6010
6010
6010
Zinc
Vanadium
Thallium
Silver
Selenium
Nickel
Molybdenum
Mercury
Lead
Copper
Cobalt
total Chromium,
VI
Chromium,
Cadmium
Beryllium
Barium
Arsenic
Antimony
Analyte
22 TITLE REGULATIONS, OF CODE
CALIFORNIA
Reported:
Analyzed:
Extracted:
Received:
Sampled:
V7071268
Number Lab
O'Connell
Erin :Attention:
TDD-4-35 Soil, Descript: Sample
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
261-1022 (714)
FAX
261-1228 (714)
92324
370-4667 (909)
FAX
370-1046 (909)
91406
779-1844 (818)
FAX
779-1843 (818)
85281 AZ Tempe,
968-8272 (602)
FAX
968-1338 (602)
I.
Suite St., 12th W. 2465
CA Nuys, Van C-11, Suite Way. Sherman 16525
Analytical Mar Del
CA Colton, A, Suite Dr., Cooley E. 1014
92606 CA Irvine, Ave., Alton 2852
(
35> of <25 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
LAAIL.AZ
r
I
Lin Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
#1197. ELAP
110
52
N.D.
N.D.
N.D.
83
2.3
0.060
4.5
44
10
58
N.D.
1.7
N.D.
130
5.8
N.D.
(ppm)
/Kg mg
Result
Sample
TTLC
100
2.0
5000
2400
700
500
1.0
1.0
10
1.0
1.0
1.0
0.020
2.0
1.0
1.0
1.0
0.50
0.50
0.50
1.0
-
limit. reporting the above or at present not were N.D. as reported Analytes
Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
250
24
7.0
5.0
1.0
20
350
0.20
5.0
25
80
5.0
5.0
1.0
0.75
100
5.0
2000
3500
20
1000
2500
8000
2500
500
100
6010
6010
6010
6010
6010
6010
6010
Method
Limit Max.
mg/L
mg/Kg
mg/Kg
(PPrn)
(PPm)
(PPIn)
15
75
10000
500
500
2.0
10
Zinc
Vanadium
Thallium
Silver
Selenium
Nickel
Molybdenum
Mercury
7471
6010
6010
6010
6010
7196
6010
6010
6010
6010
6010
EPA
STLC
TTLC
Limit Max.
Limit
Reporting
Lead
Copper
Cobalt
total Chromium,
VI Chromium,
Cadmium
Beryllium
Barium
Arsenic
Antimony
Analyte
METALS 22 TITLE REGULATIONS, OF CODE CALIFORNIA
1997 1 Aug
11:
1997 28-30, Jul
0 1997 28, Jul
199711: 24, Jul
,
1997:::i: 22, Jul
968-1338 (602)
FAX
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
V7071269
Number: Lab
O'Connell Erin :::::Attention:
TDD-4-50 Soil, Descript: Sample
91107 CA Pasadena,
Malibu 213,
204
Ste. Villa, Madre Sierra ::650
Group Environmental Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe,
1,
Suite St., 12th W 2465
92324 CA Colton, A, Suite
370-1046 (909) FAX 370-4667 (909)
91406 CA Nuys. Van C-11, Suite Way, Sherman 16525
779-1843 (818) FAX 779-1844 (818)
261-1228 (714)
FAX
261-1022 (714)
MarAnalytical Del
Dr., Cooley E. 1014
92606 CA Irvine, Ave., Alton 2852
(
38> of <26 V7071262.PEG
Analytical.Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to Only pertain Results
Manager Project
Libel Ann Mary
#1855) (FLAP NUYS VAN ANALYTICAL, MAR DEL
#1197. ELAP
110
160
N.D.
N.D.
-
limit. reporting the above or at present not were N.D. as reported Analytes
Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
Method
Limit Max.
mg/L
mg/Kg
mg/Kg
mg/Kg
(Piom)
(Pim)
(PPITI)
(PPrn)
15
5000
2400
700
500
100
2000
3500
20
1000
2500
8000
2500
500
100
75
10000
500
500
10
N.D.
8.3
N.D.
140
4.4
N.D.
2.1
80
26
N.D.
3.1
46
5.0
68
1.0
1.0
10
1.0
2.0
1.0
1.0
0.020
2.0
1.0
1.0
1.0
0.50
0.50
0.50
1.0
2.0
250
24
7.0
5.0
1.0
20
350
0.20
5.0
25
80
5.0
5.0
1.0
0.75
100
5.0
6010
6010
6010
6010
6010
6010
6010
EPA
STLC
TTLC
Limit Max.
Limit
Reporting
Result
Sample
TTLC
7471
6010
6010
6010
6010
7196
6010
6010
6010
6010
6010
Zinc
Vanadium
Thallium
Silver
Selenium
Nickel
Molybdenum
Mercury
Lead
Copper
Cobalt
total Chromium,
VI Chromium,
Cadmium
Beryllium
Barium
Arsenic
Antimony
Analyte
METALS 22 TITLE REGULATIONS, OF CODE CALIFORNIA
::::: 1997
1, Aug
1997::: 28-30, Jul
1997:ii: 28, Jul
1997;;:: 24, Jul
1997;:`; 22, Jul
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
779-1844 (818)
370-1046 (909) FAX 370-4667 (909)
261-1228 (714)
FAX
261-1022 (714)
V7071270
Number: Lab
O'Connell Erin Attention:
TDD-4-85 Soil, Descript: Sample
91107 CA Pasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific $:
::
]:
:
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe,
91406
1,
Suite St., 12th W. 2465
MarAnalytical Del
CA Nuys, Van C-11, Suite Way, Sherman 16525
92324 CA Colton.
A, Suite Dr., Cooley E. 1014
f4(
92606 CA Irvine. Ave.. Alton 2852
i:iii
i:!
38> of <27 W071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lins Ann Mary
14.kih-40
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
#1197. ELAP
65
43
N.D.
N.D.
N.D.
43
2.4
0.040
1.0
1.0
10
1.0
2.0
1.0
1.0
0.020
2.0
-
5000
2400
700
500
100
2000
3500
20
1000
2500
8000
2500
500
limit. reporting the above or at present not were N.D. as reported Analytes
Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
250
24
7.0
5.0
1.0
20
350
0.20
6010
6010
6010
6010
6010
6010
6010
7471
STLC
TTLC
Limit Max.
Limit Max.
Limit
Reporting
Result
Sample
TTLC
mg/Kg
mg/Kg
mg/Kg
(PIDirl)
(PPrrl)
10
4.8
27
4.9
38
N.D.
2.3
N.D.
200
N.D.
N.D.
1.0
1.0
1.0
0.50
0.50
0.50
5.0
25
80
5.0
5.0
1.0
100
75
1.0
2.0
0.75
(PPrn)
(PPrn)
100
5.0
15
10000
500
500
6010
6010
6010
6010
7196
6010
6010
6010
6010
6010
Zinc
Vanadium
Thallium
Silver
Selenium
Nickel
Molybdenum
Mercury
Lead
Copper
Cobalt
total Chromium,
VI Chromium,
Cadmium
Beryllium
Barium
Arsenic
Antimony
mg/L
Method
Analyte
EPA
METALS 22 TITLE REGULATIONS, OF CODE CALIFORNIA
1997 1, Aug
1997 28-30, Jul
28, Jul
1997::::::
1997::: 24, Jul
1997:::: 22, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
V7071271
Number: Lab
O'Connell Erin ;Attention:
TDD-5-25 Soil, Descript:
Sample
91107 CA Pasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra iii:i650
Group Environmental :::'Pacific
i
#9615-97-01 Auth. Work Thrifty ID: Project Client
92324 CA Colton, A, Suite
370-4667 (909)
91406
779-1844 (818)
85281 AZ Tempe, I, Suite St., 12th W. 2465
968-8272 (602)
261-1022 (714)
MarAnalytical Del
CA Nuys, Van C-11, Suite Way. Sherman 16525
Dr., Cooley E. 1014
92606 CA Irvine, Ave., Alton 2852
(
38> of <28 PEG x7071262.
Analytical. Mar Del from permission written without full, in except reproduced,
be not shah report This laboratory. the in tested samples to only pertain Results
Manager Project
Linsel Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
#1197. ELAP
98
55
N.D.
N.D.
N.D.
66
1.0
1.0
10
1.0
2.0
0.020
2.0
0.054
3.3
1.0
1.0
1.3
38
-
5000
2400
700
500
100
1.0
1.0
1.0
4.7
61
limit. reporting the above or at present not were N.D. as reported Analytes
Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
250
24
7.0
5.0
1.0
20
350
0.20
5.0
25
80
5.0
5.0
1.0
0.75
100
5.0
2000
3500
20
1000
2500
8000
2500
Limit Max.
TTLC
Reporting
Limit
Result
Sample
TTLC
mg/Kg
mg/Kg
mg/Kg
(PPrn)
(PPTI)
(PM)
(PPn1)
15
75
10000
500
500
10
N.D.
2.4
N.D.
220
N.D.
N.D.
0.50
0.50
0.50
500
100
1.0
2.0
6010
6010
6010
6010
6010
6010
6010
7471
6010
6010
6010
6010
7196
6010
6010
6010
6010
6010
Zinc
Vanadium
Thallium
Silver
Selenium
Nickel
Molybdenum
Mercury
Lead
Copper
Cobalt
total Chromium,
VI Chromium,
Cadmium
Beryllium
Barium
Arsenic
Antimony
mg/L
EPA
STLC
Method
Limit Max.
Analyte
METALS 22 TITLE REGULATIONS, OF CODE CALIFORNIA
g 1997 1, Aug
1997 28-30, Jul
1997 28, Jul
::::::
iiii:i
:::
::,.
1997::: 24, Jul
1997::: 22, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-8272 (602)
779-1844 (818)
V7071272
Number
Lab
O'Connell
Erin iirs.Attention:::
TDD-5-40 Soil, Descript:
Sample
91107 CA Pasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra iiii650
Group Environmental ,:Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe. 1, Suite St., 12th
91406
W.
2465
MarAnalytical Del
CA Nuys, Van C-11, Suite Way, Sherman 16525
92606
261-1022 (714)
92324 CA Colton,
370-4667 (909)
A, Suite Or, Cooley E. 1014
CA Irvine. Ave.. Alton 2852
38> of <29 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain
Results
Manager Project
Lintel Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against
quantitated are Hydrocarbons Fuel Volatile
mg/Kg
mg/Kg
Benzene
Benzene
Ethyl
Xylenes
Total
(PPm)
(PPrn)
(ppm)
mg/Kg
mg/Kg
mg/Kg
(PM))
(PPrn)
N.D.
N.D.
N.D.
N.D.
N.D.
1.0
0.0050
0.0050
0.0050
0.015
Toluene
Hydrocarbons
Fuel Volatile
Limit: Reporting
Blank Method
Description
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
Soil
1997 1, Aug
1997 29, Jul
1997 29, Jul
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix:
Reported:
Analyzed:
Extracted:
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
92324 CA Colton, A, Suite
370-4667 (909)
406 I 9 CA Nuys, Van
779-1844 (818)
85281 AZ Tempe,
968-8272 (602)
261-1228 (714) FAX 261-1022 (714)
1.
Suite St., 12th W. 2465
C-11,
Suite Way, Sherman 16525
Mar-Analytical Del
Dr., Cooley E. 1014
92606 CA Irvine, Ave., Alton 2852
(
38> of <30 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
el Lin Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
-
#1197. ELAP Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel Volatile
Benzene
Ethyl
Xylenes
Total
(ppm)
mg/Kg
N.D.
N.D.
N.D.
0.0050
0.0050
0.015
0.0050
1.0
mg/Kg
Benzene
Toluene
mg/Kg
mg/Kg
(PPm)
(PPm)
(PPm)
(PPm)
N.D.
N.D.
Limit: Reporting
Blank Method
mg/Kg
Hydrocarbons
Fuel Volatile
Description
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
Soil
1997 1, Aug
1997 28-31, Jul
1997 28-31, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix:
Reported:
Analyzed:
Extracted:
968-8272 (602)
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe,
I,
Suite St., 12th W. 2465
92606
-1022 261 (714)
92324 CA Colton, A, Suite
370-4667 (909)
91406 CA Nuys,
779-1844 (818)
Analytical Mar Del
Van C-11. Suite Way, Sherman 16525
Dr., Cooley E. 1014
CA Irvine, Ave., Alton 2852
38> of <31 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lins Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
Ether tert-Butyl Methyl = MTBE
Limit: Reporting
1.0
N.D.
Blank Method
(PP')
mg/Kg
Result
Sample
Description
Laboratory
MODIFIED) 8020 (EPA MTBE
Soil
1997 1, Aug
1997 29, Jul
1997 29, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix
Reported:
Analyzed:
Extracted:
968-8272 (602)
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe, 1, Suite St., 12th
92606
261-1022 (714)
92324
370-4667 (909)
91406
779-1844 (818)
W.
2465
CA Nuys, Van C-11, Suite Way. Sherman 16525
CA Colton, A, Suite Dr, Cooley E. 1014
CA Irvine,
.
MarAnalytical Del
Ave Alton 2852
(
39> of <32 PEG W071262.
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tasted samples to only pertain Results
Manager Project
Lintel Ann Mary
LAAL-r
64.
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
Ether tert-Butyl Methyl = MTBE
1.0
N.D.
Limit: Reporting
Blank Method
(ppm)
mg/Kg
Result
Sample
Description
Laboratory
MODIFIED) 8020 (EPA MTBE
Soil
1997 1, Aug
1997 28-31, Jul
1997 28-31, Jul
Matrix
Reported:
Analyzed:
Extracted:
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
92606 CA Irvine, Ave.. Alton 2852
261-1022 (714)
FAX
261-1228 (714)
92324 CA Colton, A, Suite
370-4667 (909)
FAX
370-1046 (909)
91406 CA Nuys, Van C-11.
779-1844 (818)
FAX
779-1843 (818)
968-8272 (602)
FAX
968-1338 (602)
85281 AZ Tempe. 1, Suite St., 12th W 2465
Suite Way. Sherman 16525
Dr., Cooley E. 1014
Analytical Mar Del
t.
38> of <33 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the In tested samples to only pertain Results
Manager Project
Lins Ann Mary
.44-)--,0
ry 0A-4-
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C40. to C8 from range method this by detected Hydrocarbons standard. fuel diesel a against quantitated are Hydrocarbons Extractable
Limit: Reporting
5.0
N.A.
N.D.
Blank Method
(ppm)
mg/Kg
Type
Hydrocarbon
Hydrocarbons
Extractable
Description
Laboratory
8015) EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
Soil
1997 1 Aug
1997 28, Jul
1997 25, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix
Reported:
Analyzed:
Extracted:
968-8272 (602)
::
O'Connell Erin Attention
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe, I, Suite St., 12th W. 2465
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
92324 CA Colton, A, Suite Dr., Cooley
370-4667 (909)
91406 CA Nuys,
779-1844 (818)
Mar-Analytical Del
Van C-11, Suite Way, Sherman 16525
E. 1014
f
38> of <34 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Linse Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
C40. to C8 from range method this by detected Hydrocarbons standard. fuel diesel a against quantitated are Hydrocarbons Extractable
Limit: Reporting
5.0
N.A.
Blank Method
N.D.
(ppm)
mg/Kg
Type
Hydrocarbon
Hydrocarbons
Extractable
Description
Laboratory
8015) EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
Soil
1997 1, Aug
1997 29-30, Jul
1997 28, Jul
968-1338 (602)
FAX
Matrix
Reported:
Analyzed:
Extracted:
968-8272 (602)
92324
91406
779-1843 (818) FAX 779-1844 (818)
FAX
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
(
Group Environmental Pacific
85281 AZ Tempe, 1, Suite St., 12th
92606
261-1022 (714)
370-1046 (909) FAX 370-4667 (909)
261-1228 (714)
W.
2465
MarAnalytical Del
CA Nuys, Van C-11. Suite Way. Sherman 16525
CA Colton, A, Suite Dr., Cooley
CA Irvine, Ave.,
E. 1014
Alton 2852
38> of <35 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
84%
99%
99%
(74-121) 4-Bromofluorobenzene
(81-117) Toluene-d8
(80-120) Dibromofluoromethane
Limits): (Accept. Recoveries Standard Surrogate
Manager Project
Lin Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
2.0
2.0
5.0
2.0
2.0
Limit
Reporting
Result
Sample
pg/Kg
(PPb)
5.0
2.0
2.0
2.0
5.0
5.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
20
2.0
2.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
10
m,p-Xylenes
o-Xylene
chloride Vinyl
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2,3-Trichloropropane
Trichlorofluoromethane
Trichloroethene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Toluene
Tetrachloroethene
1,1,2,2-Tetrachloroethane
1,1,1,2-Tetrachloroethane
Styrene
n-Propylbenzene
Naphthalene
chloride Methylene
p-lsopropyltoluene
Isopropylbenzene
Hexachlorobutadiene
Ethylbenzene
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
2.0
5.0
2.0
2.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
2.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
5.0
2.0
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
5.0
2.0
Limit
Reporting
Result
Sample
pg/Kg
pg/Kg
pg/Kg
(PPb)
(PPb)
(PPb)
Analyte
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,1-Dichloropropene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloroethane
1,1-Dichloroethane
Dichlorodifluoromethane
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dibromomethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
4-Chlorotoluene
2-Chlorotoluene
Chloromethane
Chloroform
Chloroethane
Chlorobenzene
tetrachloride Carbon
tert-Butylbenzene
sec-Butylbenzene..
n-Butylbenzene
Bromomethane
Bromoform
Bromodichloromethane
Bromochloromethane
Bromobenzene
Benzene
Analyte
8260) (EPA GC/MS by ORGANICS VOLATILE
Soil
1997 1, Aug
1997 29, Jul
1997 29, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix
Reported:
Analyzed:
Extracted:
968-8272 (602)
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe,
1,
Suite St., 12th W. 2465
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
92324
370-4667 (909)
91406
779-1844 (818)
CA Nuys, Van C-11, Suite Way, Sherman 16525
MarAnalytical Del
CA Colton, A, Suite Dr., Cooley E. 1014
38> of <36 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
90%
101%
99%
(74-121) 4-Bromofluorobenzene
(81-117) Toluene-d8
(80-120) Dibromofluoromethane
Limits): (Accept. Recoveries Standard Surrogate
Manager Project
Lins Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
2.0
2.0
5.0
2.0
2.0
Limit
Reporting
Result
Sample
pg/Kg
pg/Kg
(PPb)
(PPb)
5.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
20
2.0
2.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
10
5.0
2.0
2.0
2.0
5.0
m,p-Xylenes
o-Xylene
chloride Vinyl
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2,3-Trichloropropane
Trichlorofluoromethane
Trichloroethene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
1,2,4-Trichlorobenzene
1,2,3-Trichlorobenzene
Toluene
Tetrachloroethene
1,1,2,2-Tetrachloroethane
1,1,1,2-Tetrachloroethane
Styrene
n-Propylbenzene
Naphthalene
chloride Methylene
p-Isopropyltoluene
lsopropylbenzene
Hexachlorobutadiene
Ethylbenzene
(PPb)
(PPb)
2.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
5.0
5.0
5.0
2.0
5.0
2.0
5.0
5.0
5.0
5.0
5.0
5.0
2.0
5.0
5.0
2.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D,
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
pg/Kg
Analyte
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,1-Dichloropropene
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloroethane
1,1-Dichloroethane
Dichlorodifluoromethane
1,4-Dichlorobenzene
1,3-Dichlorobenzene
1,2-Dichlorobenzene
Dibromomethane
1,2-Dibromoethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
4-Chlorotoluene
2-Chlorotoluene
Chloromethane
Chloroform
Chloroethane
Chlorobenzene
tetrachloride Carbon
tert-Butylbenzene
sec-Butylbenzene
n-Butylbenzene
Bromomethane
Bromoform
Bromodichloromethane
Bromochloromethane
Bromobenzene
Benzene
pg/Kg
Result
Sample
Limit
Reporting
Analyte
8260) (EPA GC/MS by ORGANICS VOLATILE
Soil
1997 1, Aug
1997 30, Jul
1997 30, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix
Reported:
Analyzed:
Extracted:
968-8272 (602)
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe, I, Suite St., 12th
W.
2465
92324 CA Colton, A, Suite Dr. Cooley
370-4667 (909)
91406 CA Nuys, Van C-11, Suite Way, Sherman 16525
779-1844 (818)
261-1022 (714)
92606
Mar-Analytical Del
E. 1014
CA Irvine, Ave., Alton 2852
f,
38> of <37 V7071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Lintel Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
#1197.
RAP -
limit. reporting the above or at present not were N.D. as reported Analytes
Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
5.0
Limit: Reporting
N.D.
Blank Method
(PPrn)
mg/Kg
Hydrocarbons
Petroleum
Description
Laboratory
418.1) (EPA HYDROCARBONS PETROLEUM RECOVERABLE TOTAL
Soil
1997 1, Aug
1997 30, Jul
1997 30, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix:
Reported:
Analyzed:
Extracted:
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
91406
779-1844 (818)
85281 AZ Tempe, 1, Suite St., 12th
968-8272 (602)
W.
2465
CA Nuys, Van C-11, Suite Way, Sherman 16525
92606
261-1022 (714)
92324 CA Colton, A, Suite
370-4667 (909)
Dr., Cooley E. 1014
Analytical Mar Del
CA Irvine, Ave., Alton 2852
(
38> of <38 W071262.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
nsel Ann Mary
#1855) (ELAP NUYS VAN ANALYTICAL, MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
#1197. ELAP - Irvine Analytical, Mar Del by performed and to subcontracted was analysis This
EPA
STLC
TTLC
Method
Limit Max.
Limit Max.
mg/L
mg/Kg
mg/Kg
(PPITI)
(Plorn)
(PPrn)
(PPril)
15
0.75
100
5.0
75
10000
500
500
10
1.0
100
20
350
0.20
5.0
25
80
5.0
5.0
2000
3500
20
1000
2500
8000
2500
500
1.0
100
2.0
250
24
7.0
5.0
5000
2400
700
500
1.0
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
1.0
1.0
10
1.0
1.0
0.020
2.0
1.0
1.0
1.0
0.50
0.50
0.50
1.0
2.0
Limit
Reporting
Result
Sample
TTLC
mg/Kg
6010
6010
6010
6010
6010
6010
6010
7471
6010
6010
6010
6010
7196
6010
6010
6010
6010
6010
Zinc
Vanadium
Thallium
Silver
Selenium
Nickel
Molybdenum
Mercury
Lead
Copper
Cobalt
total Chromium,
VI Chromium,
Cadmium
Beryllium
Barium
Arsenic
Antimony
Analyte
METALS 22 TITLE REGULATIONS, OF CODE CALIFORNIA
Soil
1997 1, Aug
1997 28-30, Jul
1997 28, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix
Reported:
Analyzed:
Extracted:
968-8272 (602)
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe, 1, Suite
St.,
12th W. 2465
92606
261-1022 (714)
CA Colton, A. Suite Dr., Cooley E. 1014
92324
370-4667 (909)
CA Nuys, Van C-11, Suite Way. Sherman 16525
91406
779-1844 (818)
MarAnalytical Del
4(
CA Irvine, Ave.. Alton 2852
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
103%
1
PR
MEAN
Analytical Mar Del
R1
Analysis Sample of Result
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
Terms: of Definition
MSD
PR1
ppm
PPm
%
ok
200
210
100%
4.9%
I
RPD
105%
1
PR2
1
I
MS
200
I
ppm
0
Hydrocarbons
ppm
Sp
R1
Analyte
V7071262
7/28/97
Soil
85281 AZ Tempe. 1, Suite St., 12th W. 2465
968-8272 (602)
C-11,
92324 CA Colton, A, Suite
#: SAMPLE
DATE:
Matrix:
METHOD: EPA
Diesel 8015
91406 CA Nuys, Van
779-1844 (818)
370-4667 (909)
ica MarAnal Del
Suite Way, Sherman 16525
Dr., Cooley E. 1014
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
(
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
100 X SP) / ((MS-R1) MS; of Recovery Percent
Result Duplicate Spike Matrix
Result Spike Matrix
Sample to Added Concentration Spike
Analysis Sample of Result
0.90%
1.2%
0.42%
666
600
480
MS
MSD
PR1
PR2
ppb
ppb
Ok
OA
0/0
92%
99%
96%
72%
93%
87%
100%
96%
97%
96%
98%
94%
101%
68%
103%
96%
91%
98%
96%
84%
92%
86%
100%
95%
96%
95%
98%
94%
101%
79%
102%
96%
30%
1.1%
0.77%
1.4%
1.2%
1.1%
1.0%
0.94%
1.1%
0.20%
13%
0.76%
1.4%
RPD
PR
91%
97%
96%
96%
92%
86%
99%
94%
96%
95%
97%
93%
101%
91%
102%
95%
672
607
482
179
463
522
502
566
547
503
535
471
507
849
526
497
241
458
518
495
559
541
498
530
466
506
966
522
490
R1
SP
ppb
ppb
15
500
500
500
250
500
500
500
500
500
500
500
500
500
500
500
500
212
114
0
0
0
88
0
88
62
25
44
0
0
511
12
MEAN
RPD
PR2
PR1
MSD
MS
Sp
R1
Zinc
Vanadium
Thallium
Silver
Selenium
Nickel
Molybdenum
Lead
Copper
Cobalt
Chromium
Cadmium
Beryllium
Barium
Arsenic
Antimony
Analyte
GG04812
Instrument:
METHOD:
Metals
Matrix:
SOIL
ICP
91406
779-1844 (818)
85281 AZ Tempe.
968-8272 (602)
370-4667 (909)
261-1022 (714)
I,
7/30/97
#: Sample
Date:
(
Suite St., 12th W. 2465
cal Anal Mar Del
CA Nuys, Van C-11, Suite Way. Sherman 16525
92324 CA Colton,
92606
A. Suite Dr.. Cooley
1014
E
CA Irvine, Ave_ Alton 2852
90%
PR
MEAN
Analytical Mar Del
R1
Analysis Sample of Result
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
Terms: of Definition
Sp
MS
MSD
PR1
ppb
ppb
ppb
%
OA
90%
0.0%
I
RPD
90%
I
PR2
I
8.1
I
8.1
I
8.0
I
0.89
Mercury
ppb
R1
lyte Ana
GG04193
7/28/97
Soil
7471
92324 CA Colton, A, Suite
370-4667 (909)
FAX
370-1046 (909)
91406 CA Nuys, Van C-11, Suite Way, Sherman 16525
779-1844 (818)
FAX
779-1843 (818)
85281 AZ Tempe,
968-8272 (602)
FAX
968-1338 (602)
1,
#: SAMPLE
DATE:
Matrix:
METHOD: EPA
261-1022 (714)
FAX
261-1228 (714)
Suite St.. 12th W. 2465
Analytical Mar Del
Dr., Cooley E. 1014
92606 CA Irvine, Ave., Alton 2852
(
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Analytical Mar Del
R1
Analysis Sample of Result
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
Terms: of Definition
PR2
RPD
PR
MEAN
107%
3.2%
105%
I
I
103%
0.32
MSD
PR1
PPm
%
I
0.31
I
PPm
PPm
PPm
0
0.30
I
Sp
MS
R1
(VI) Chromium
Analyte
GG04190
7/28/97
Soil
3060/7196
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
92324 CA Colton,
370-4667 (909)
406 I 9 CA Nuys, Van
779-1844 (818)
85281 AZ Tempe, I, Suite St., 12th
968-8272 (602)
C-11,
W.
#: SAMPLE
DATE:
Matrix:
METHOD: EPA
2465
MarAnalytical Del
Suite Way, Sherman 16525
A, Suite Dr, Cooley E. 1014
C
FAX
779-1843 (818)
FAX
968-1338 (602)
FAX
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
0/0
0/0
3.8%
94%
I
Analytical Mar Del
R1
Analysis Sample of Result
Terms: of Definition
RPD
PR
MEAN
I
92%
I
97%
I
77
80
ppm
OA
PR2
PR1
MSD
I
ppm
MS
R1
Sp
ppm
ppm
22
60
I
Hydrocarbon
Analyte
GG04388
7/30/97
Soil
418.1
968-8272 (602)
779-1844 (818)
370-1046 (909) FAX 370-4667 (909)
261-1228 (714)
261-1022 (714)
85281 AZ Tempe,
91406
I,
#: SAMPLE
DATE:
Matrix:
METHOD: EPA
Suite St., 12th W. 2465
CA Nuys, Van C-11, Suite Way, Sherman 16525
92324 CA Colton, A, Suite Dr., Cooley E.
MarAnalytical Del
1014
92606 CA Irvine, Ave., Alton 2852
(
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
5.7%
67%
I
Analytical Mar Del
R1
Analysis Sample of Result
Terms: of Definition
RPD
PR
MEAN
_I
65%
I
PR2
69%
I
PR1
34
1
36
MS
MSD
ppm
ppm
I
50
I
ppm
1.7
Hydrocarbons
ppm
Sp
R1
Analyte
GG04020
7/28/97
Soil
91406 CA Nuys,
779-1844 (818)
85281 AZ Tempe,
968-8272 (602)
92606
I.
#: SAMPLE
DATE:
Matrix:
METHOD: EPA
extraction by 8015
92324 CA Colton,
370-4667 (909)
261-1022 (714)
Suite St., 12th W. 2465
Analytical Mar Del
Van C-11, Suite Way, Sherman 16525
A, Suite Dr., Cooley E. 1014
CA Irvine, Ave.,
Alton 2852
(
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
968-8272 (602)
Analytical Mar Del
R1
Analysis Sample of Result
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
Terms: of Definition
OA
OA
6.7%
103%
PR
MEAN
1
RPD
0/0
OA
106%
99%
I
PR2
I
1.1
1
ppm
MSD
PR1
ppm
ppm
1.1
1.2
1
Sp
MS
0.00241
1,
92324
370-4667 (909)
406 9 CA Nuys, Van
779-1844 (818)
Dr, Cooley
Analyte
# SAMPLE
Analytical Mar Del
Suite Way. Sherman 16525
CA Colton, A. Suite
DATE:
matrix:
METHOD: EPA
Suite St., 12th W. 2465
C-11,
I
TPH
ppm
R1
GG04033
7/28/97
soil
8015/8020
85281 AZ Tempe,
92606
261.1022 (714)
E. 1014
CA Irvine, Ave., Alton 2852
(
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
99%
95%
94%
97%
Analytical Mar Del
R1
Analysis Sample of Result
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
Terms: of Definition
4.3%
4.1%
3.9%
3.6%
96%
93%
93%
95%
0.093
0.093
0.095
97%
96%
99%
0.29
101%
ppm
OA
PR
MEAN
RPD
PR2
PR1
MSD
0.30
0.097
0.097
0.099
ppm
MS
0.30
0.10
0.10
0.10
ppm
0
0
0.00054
0
soil
R1
85281 AZ Tempe, 1, Suite St., 12th W. 2465
91406
Analyte
# SAMPLE
DATE:
Analytical Mar Del
CA Nuys, Van C-11. Suite Way. Sherman 16525
92324 CA Colton, A, Suite
92606
Xylenes
Ethylbenzene
Toluene
Benzene
ppm
Sp
GG04033
7/28/97
matrix:
METHOD: EPA
8015/8020
968-8272 (602)
779-1844 (818)
370-4667 (909)
261-1022 (714)
Dr., Cooley E. 1014
CA Irvine, Ave.. Alton 2852
C
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Analytical Mar Del
R1
Analysis Sample of Result
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
Terms: of Definition
PR2
RPD
PR
MEAN
115%
3.5%
113%
112%
5.5%
109%
116%
3.5%
114%
0.0%
104%
110%
1.8%
109%
108%
1.9%
107%
5.7%
105%
3.8%
102%
3.8%
104%
3.9%
154%
157%
106%
104%
108%
104%
53
102%
79
151%
100%
102%
106%
53
54
54
52
104%
55
108%
56
106%
58
112%
111%
PR1
58
76
51
50
50
0.30
0
0
50
51
1.0
50
51
53
54
52
56
50
50
50
50
0.20
0
0
0
0.50
50
56
0
50
53
MS
MSD
ppb
ppb
R1
Sp
ppb
ppb
Chloride Vinyl
Trichloroethene
Toluene
Tetrachloroethene
Chloroform
1,1-Dichloroethene
1,2-Dichloroethane
1,1-Dichloroethane
Chlorobenzene
Benzene
Analyte
GG04386
7/29/97
#: SAMPLE
DATE:
Soil Matrix:
8260 METHOD: EPA
968-8272 (602)
779-1844 (818)
-4667 370 (9091
261-1022 (714)
85281 AZ Tempe. 1, Suite St., 12th W. 2465
91406
92324
92606
Anal Mar Del
CA Nuys. Van C-11, Suite Way. Sherman 16525
CA
Colton, A, Suite Dr., Cooley
CA Irvine, Ave.,
E. 1014
Alton 2852
(
Analytical Mar Del
St
Concentration Standard
111
Result Standard
PR
100 x St) / (R1 R1; of Recovery Percent
Terms: of Definitions
106%
98%
PR
1063
979
1000
1000
St
R1
ppb
ppb
Silver
Barium
Analyte
7/30/97
Soil
6010
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
FAX
261-1228 (714)
92324 CA Colton,
370-4667 (909)
FAX
370-1046 (909)
406 I 9 CA Nuys, Van C-11, Suite Way, Sherman 16525
779-1844 (818)
FAX
779-1843 (818)
85281 AZ Tempe.
968-8272 (602)
FAX
968-1338 (602)
1,
DATE:
Matrix:
METHOD
Suite St., 12th W. 2465
MarAnalytical Del
A, Suite Dr., Cooley E. 1014
(
Sp
sample to added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X ((MS-R1)/SP) MS; of Recovery Percent
PR2
100 X ((MSD-R1)/SP) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2) Difference; Percent Relative
PR Mean
Recovery Percent Mean
Limits Acceptance
Charts Control in-house by Determined
102
...10
85
100
516
-118 85
104
:5_25
85
-122
104
...19
-120 85
-124
Analytical Mar Del
R1
Analysis Sample of Result
Terms of Definition
104
...30
85
-120
PR Mean
100
104
98
102
3.6
102
106
4.4
106
5.0
3.7
5.5
RPD
Limits Acceptance
RPD
107
PR2
101
101
0.32
0.11
0.10
PR1
Toluene
0.0011
Ethylbenzene
0.10 0.00036
0.10
Xylenes
0.0027
0.31
0.30
ppm
ppm
0.033
1.0
1.0
1.1
0.00021
0.10
0.10
0.10
0.10
0.099
ppm
0/0
PR Mean
MSD
Soil
Benzene
TPH
ppm
Date:
07/29/97
#: Sample
V7071289
#: Batch
GG29G21S
Analyte
R1
MS
Matrix:
8015/8020 Method EPA
92606 CA Irvine, Ave., Alton 2852
261-1228 (714) FAX 261-1022 (714)
92324 CA Colton, A, Suite
370-4667 (909)
FAX
370-1046 (909)
91406 CA Nuys, Van C-1I, Suite Way, Sherman 16525
779-1844 (818)
FAX
779-1843 (818)
85281 AZ Tempe,
968-8272 (602)
FAX
968-1338 (602)
1,
Suite St., 12th W. 2465
ical MarAnal Del
Dr., Cooley E. 1014
R1
Result Standard
PR
100 x St) / (R1 R1; of Recovery Percent
92324
91406
779-1843 (818) FAX 779-1844 (818)
85281 AZ Tempe,
968-1338 (602) FAX 968-8272 (602)
FAX
Analytical Mar Del
St
sample to added standard of nanograms Total
Terms: of Definitions
104%
104%
100%
106%
108%
96%
108%
104%
114%
160%
PR
52
52
50
53
54
48
54
52
57
80
50
50
50
50
50
50
50
50
50
50
St
R1
ng
ng
Ethylbenzene
Tetrachloroethene
Toluene
Trichioroethene
1,2-Dichloropropane
1,2-Dichloroethane
Benzene
Chloroform
1,1-Dichloroethene
Chloride Vinyl
Analyte
7/29/97
Soil
8260
92606
261-1022 (714)
370-1046 (909) FAX 370-4667 (909)
261-1228 (714)
1,
DATE:
Matrix:
METHOD
Suite St., 12th W. 2465
Analytical Mar Del
CA Nuys, Van C-11. Suite Way, Sherman 16525
CA Colton, A, Suite Or, Cooley E. 1014
CA Irvine, Ave., Alton 2852
7-17
91406 CA Nuys,
FAX
779-1843 (818)
FAX
968-1338 (602)
FAX
1--
Date:
Manager: Laboratory
reported. were results the and validated was
batch analytical the limits, acceptance within was (LCS) Sample Control Laboratory
on
was
the Since
results.
acceptable
with
7/30/97
calibrated
GC/MS
The
Action: Corrective
calibration. needed and time over unstable became detector The
Problem: the of Cause the of Determination
limits. acceptance the of outside were (MS/MSD)
Duplicate Spike Spike/Matrix Matrix the in chloride vinyl of recoveries The
Problem: of Definition and Identification
Soil
7/29/97
Matrix:
Date:
8260 EPA
GC/MS
Method:
Department:
REPORT ACTION CORRECTIVE
92324 CA Colton,
370-1046 (909) FAX 370-4667 (909)
261-1228 (714)
968-8272 (602)
779-1844 8) (8
I
261-1022 (714)
85281 AZ Tempe, I. Suite St.. 12th W 2465
92606
Analytical Mar Del
Van C-11, Suite Way. Sherman 16525
A, Suite Dr, Cooley E. 1014
CA Irvine, Ave., Alton 2852
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1. Tempe. AZ
1-.4,;(-tv, OON
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Client Name/Address:
W. 12th
(6021
(818) 779.1844 FAX 18181779-1843
2465
85281
16525 Sherman Way. Suite C-11. Van Nuys. CA 91406
261-1228
1909) 370-4667 FAX M091370.1046
FAX (7141
17141261-1022
92324
2852 AXon Ave.. Irvine.
92714
E.
CA
1014
Co Ney Or.. Suite A. Colton. CA
Del Mar Analytical
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Date/Time
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(check)
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Project/PO Number:
(602) 968 1338
ate /Time:
Note- Sample(s) will be disposed of after 30 days
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72 FAX
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inquished By:
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Sample
Description
35-
'TOD - .5-
r:.\1-,-
?c.:,- c.--1
(602) 968 82
(8181 779.1844 FAX (818)
Sample Container
Matrix
Type
Tenn*. AZ 85281
\--):).....-..e.,
Project Manager/Phone Number:
Cr .%r, 01Cocm,c\
A
-I\ ,(-1,S\-)
,
2465 W 12th St.. Suite
7791843
370.1046
FAX (9o91
State 4. Cotton. CA 92324
(9091370.4667
1714/ 261.1022 FAX 1714) 261-1228
2852 Mtan Ave.. Irvine. CA 92714
Cooley Dr
6525 Sherman Way. Suite C.11. Van Nuys. CA 91406
1014
Del Mar Analytical
Client Name/Address:
(
::::
10> of <1 GG04596.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Johnson Nancy
#1197) (ELAP ANALYTICAL MAR DEL
factors. other and effects matrix to due are factors Dilution limit. reporting the above or at present not were N.D. as reported Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel Volatile
pg/L
pg/L
(PPb)
(PPb)
2.9
8.0
1.5
3.0
N.D.
N.D.
0.30
0.60
Xylenes
Total
0.30
Limit: Reporting
N.D.
N.D.
50
0.30
1:1
Dilution
pg/L
pg/L
(PPb)
(PPb)
(PPb)
/L Jg
GG04596
MW-7
1,500
74
12
1:5 Dilution
Limit: Reporting
250
GG04597
TDD-4
N.D.
1.5
Benzene
Ethyl
Toluene
1.5
Benzene
Hydrocarbons
Fuel Volatile
Water
Description
Sample
Number
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
1997;: 1, Aug
1997:::'::: 30-31, Jul
1997 30-31, Jul
1997::-::':
25, Jul
1997::::. 25, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
GG04596 #: Sample First
8015/8020 Mod. DHS 5030/CA EPA Method: Analysis
Malibu 213,
y
#9615-97-0.1. Auth. Work Thrift ID: Project Client
Sampled:
92324 CA Colton, A, Suite
370-4667 (909)
91406 CA Nuys, Van C-11, Suite Way, Sherman 16525
(8181779-1844
85281 AZ Tempe,
968-8272 (602)
1,
O'Connell Erin ::::Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra '1650
Analytical Mar Del
Dr., Cooley E. 1014
(
Group Environmental :Pacific
Suite St., 12th W. 2465
92606
261-1022 (714)
CA Irvine, Ave., Alton 2852
1997::::::
10> of <2 GG04596.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Johnson Nancy
CiAtliT)
#1197) (ELAP ANALYTICAL MAR DEL
factors. other and effects matrix to due are factors Dilution limit. reporting the above or at present not were N.D. as reported Analytes
Ether tert-Butyl Methyl = MTBE
pg/L
Result
Sample
Limit
Reporting
(PPb)
(PPb)
GG04596
MW-7
39
10
1
GG04597
TDD-4
N.D.
10
1
pg/L
Factor
Dilution
Water
Description
Sample
Number
Laboratory
MODIFIED) 8020 (EPA MTBE
1,
1997 30,
1997 30,
iii:199T
25,
25,
1997:::::
Aug
Jul
Jul
Jul
Jul
Reported:
Analyzed:
Extracted:
Received:
Sampled:
GG04596 #: Sample First
O'Connell Erin ::::Attention:
5030(8020 EPA Method: Analysis
91107 CA Pasadena,
Malibu 213,
204 Ste. Villa, Madre Sierra 650
91406
FAX
779-1843 (818)
FAX
968-1338 (602)
FAX
968-8272 (602)
#9615-97-01 Auth. Work Thrifty ID: Project Client
92324 CA Colton, A, Suite
370-1046 (909) FAX 370-4667 (909)
261-1228 (714)
779-1844 (818)
261-1022 (714)
85281 AZ Tempe,
I,
Dr., Cooley E. 1014
(
Group Environmental Pacific
Suite St., 12th W. 2465
CA Nuys, Van C-11, Suite Way, Sherman 16525
MarAnalytical Del
92606 CA Irvine, Ave., Alton 2852
1997::::
10> of <3 GG04596.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Johnson Nancy
#1197) (ELAP ANALYTICAL MAR DEL
factors. other and effects matrix to due are factors Dilution limit. reporting the above or at present not were N.D. as reported Analytes
C40. to C8 from range method this by detected Hydrocarbons standard. fuel diesel a against quantitated are Hydrocarbons Extractable
1
N.A.
1
N.A.
Description
Sample
Result
Sample
Limit
Reporting
Water
(ppm)
mg/L
(PPm)
GG04596
MW-7
N.D.
0.50
GG04597
TDD-4
N.D.
0.50
mg/L
Type
Hydrocarbon
Factor
Dilution
Number
Laboratory
8015) EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
1,
1997::'h 31,
30,
25,
1997 25,
1997:iii::
Aug
Jul
Jul
Jul
Jul
Reported:
Analyzed:
Extracted:
Received:
Sampled:
GG04596 #: Sample First
O'Connell Erin Attention:
8015 Mod. DHS 3510/CA EPA Method: Analysis
91107 CA Pasadena,
Malibu 213,
204
Ste. Villa, Madre Sierra 1650
Group Environmental Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
92606
-1022 I 26 (714)
92324
370-1046 (909) FAX 370-4667 (909)
91406
779-1844 (818)
85281 AZ Tempe, 1, Suite St., 12th
968-8272 (602)
FAX
779-1843 (818)
FAX
968-1338 (602)
261-1228 (714)
FAX
W.
2465
CA Nuys, Van C-11, Suite Way. Sherman 16525
CA Colton, A, Suite Dr., Cooley E. 1014
MarAnalytical Del
CA Irvine, Ave., Alton 2852
(
10> of <4 GG04596.PEG
Analytical.Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Johnson Nancy
#1197) (ELAP ANALYTICAL MAR DEL
factors. other and effects matrix to due are factors Dilution limit. reporting the above or at present not were N.D. as reported Analytes
1
Factor
Dilution
TDD-4
Description
Sample
Result
Sample
Limit
Reporting
Water
mg/L
(PPrn)
(PPril)
mg/L
N.D.
1.0
GG04597
Number
Laboratory
418.1) (EPA HYDROCARBONS PETROLEUM RECOVERABLE TOTAL
1997:iii 1, Aug
1997 31, Jul
1997 31, Jul
25, Jul
25, Jul
199T1::::
1997iii:;i
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Reported:
Analyzed:
Extracted:
Received:
Sampled:
GG04597 #: Sample First
O'Connell Erin :::::Attention:
clean-up) with (I.R. 418.1 EPA Method: Analysis
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Malibu 213,
#9615-97-01 Auth. Work Thrifty ID: Project Client
92606 CA Irvine, Ave.. Alton 2852
261-1022 (714)
92324
370-4667 (909)
91406 CA Nuys, Van C-11. Suite Way. Sherman 16525
779-1844 (818)
85281 AZ Tempe, 1, Suite St.. 12th
968-8272 (602)
W.
Group Environmental Pacific
2465
MarAnalytical Del
CA Colton, A. Suite Dr.. Cooley E. 1014
4(
10> of <5 GG04596.PEG
98%
102%
103%
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
(86-115) 4-Bromofluorobenzene
(88-110) Toluene-d8
Manager Project
Johnson Nancy
(76-114) 1,2-Dichloroethane-d4
Limits): (Accept. Recoveries Standard Surrogate
#1197) (ELAP ANALYTICAL MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
pg/L
pg/L
(PPb)
(PPb)
10
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
Result Sample
1997 1, Aug
1997i::: 29, Jul
iii:
1997 29, Jul
1997g 25, Jul
1997;i:::.
25, Jul
FAX
779-1844 (818)
2.0
5.0
5.0
5.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
5.0
20
Xylenes Total
chloride Vinyl
acetate Vinyl
Trichlorofluoromethane
Trichloroethene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
Toluene
Tetrachloroethene
1,1,2,2-Tetrachloroethane
Styrene
4-Methyl-2-pentanone
chloride Methylene
2-Hexanone
Ethylbenzene
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,2-Dichloropropane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloroethane
1,1-Dichloroethane
Chloromethane
Chloroform
ether vinyl 2-Chloroethyl
Chloroethane
Chlorodibromomethane
Chlorobenzene
tetrachloride Carbon
disulfide Carbon
2-Butanone
Bromomethane
Bromoform
Bromodichloromethane
Benzene
Acetone
10
2.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
2.0
10
5.0
2.0
2.0
5.0
5.0
10
5.0
5.0
2.0
2.0
Limit Reporting
8240) (EPA GC/MS by ORGANICS VOLATILE
Reported:
Analyzed:
Extracted:
Received:
Sampled:
968-1338 (602) FAX 968-8272 (602)
779-1843 (818)
Analyte
GG04597
Number: Lab
O'Connell Erin ::.Attention:
TDD-4 Water, Descript: Sample
91107 CA Pasadena,
Malibu 213,
204
Ste. Villa, Madre Sierra ii650
Group Environmental Pacific
#9615-97-01 Auth. Work Thrifty ID: Project Client
85281 AZ Tempe,
I.
91406 CA Nuys, Van
Suite St., 12th W. 2465
C-11,
92324 CA Colton, A, Suite Dr., Cooley
370-1046 (909) FAX 370-4667 (909)
CA Irvine, Ave.,
Analytical Mar Del
Suite Way, Sherman 16525
92606
261-1228 (714) FAX 261-1022 (714)
E. 1014
Alton 2852
(
10> of <6 GG04596.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Johnson Nancy
#1197) (ELAP ANALYTICAL MAR DEL
factors. other and effects matrix to due are
or
factors
Dilution
limit.
reporting
the
were
as
above
at
present
not
N.D.
reported
Analytes
C12. to C6 from range method this by detected Hydrocarbons standard. gasoline a against quantitated are Hydrocarbons Fuel
Volatile
Toluene
Benzene
Ethyl
Xylenes
Total
(ppb)
pg/L
(ppb)
pg/L
N.D.
N.D.
0.30
0.60
Hydrocarbons
Fuel Volatile
Benzene
(ppb)
pg/L
(ppb)
pg/L
(ppb)
pg/L
N.D.
N.D.
N.D.
50
0.30
0.30
Limit: Reporting
1:1
Dilution
Blank Method
Description
Laboratory
8015/8020) EPA Mod. DHS (CA DISTINCTION HYDROCARBONS/BTEX FUEL VOLATILE
Water
1997 1, Aug
1997 30-31, Jul
1997 30-31, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix:
Reported:
Analyzed:
Extracted:
968-8272 (602)
779-1844 (818)
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe,
91406 CA Nuys,
I,
Suite St., 12th W. 2465
Van C-11, Suite Way, Sherman 16525
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
92324 CA Colton, A, Suite Dr., Cooley
370-4667 (909)
MarAnalytical Del
E. 1014
I(
10> of <8 PEG GG04596.
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
Johnson Nancy
#1197) (ELAP ANALYTICAL MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
C40. to C8 from range method this by detected Hydrocarbons standard. fuel diesel a against quantitated are Hydrocarbons Extractable
N.A.
Type
Hydrocarbon
1
Factor
Dilution
Result
Sample
Limit
Reporting
(ppm)
mg/L
mg/L
(PPrn)
N.D.
0.50
Blank Method
Description
Sample
8015) EPA Mod. DHS (CA HYDROCARBONS FUEL EXTRACTABLE
Water
1997 1, Aug
1997 31, Jul
1997 30, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix:
Reported:
Analyzed:
Extracted:
968-8272 (602)
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe,
I. Suite St., 12th W.
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
92324 CA Colton,
370-4667 (909)
91406 CA Nuys, Van
779-1844 (818)
C-11,
2465
Suite Way, Sherman 16525
A. Suite Dr.. Cooley E. 1014
Analytical Mar Del
(
10> of <9 GG04596.PEG
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested samples to only pertain Results
Manager Project
son Joh Nancy
(fiter9tbt,17t1
#1197) (ELAP ANALYTICAL MAR DEL
factors. other and effects matrix to due are factors Dilution limit. reporting the above or at present not were N.D. as reported Analytes
1
Factor
Dilution
418.1)
Water
1997 1, Aug
1997 31, Jul
1997 31, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
(EPA
Result
Sample
Limit
Reporting
(ppm)
mg/L
(ppm)
mg/L
N.D.
1.0
Blank Method
Description
Sample
HYDROCARBONS PETROLEUM RECOVERABLE TOTAL
Matrix:
Reported:
Analyzed:
Extracted:
968-8272 (602)
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
85281 AZ Tempe,
I,
Suite St., 12th W. 2465
CA
92606
CA Colton, A, Suite Dr. Cooley E. 1014
92324
370-4667 (909)
CA Nuys, Van C-11, Suite Way, Sherman 16525
91406
779-1844 (818)
261-1022 (714)
MarAnalytical Del
Irvine, Ave., Alton 2852
(
10> of <10 GG04596.PEG
96%
104%
Analytical. Mar Del from permission written without full, in except reproduced,
be not shall report This laboratory. the in tested
samples to only pertain Results
(86-115) 4-Bromofluorobenzene
(88-110) Toluene-d8
105%
(76-114) 1,2-Dichloroethane-d4
Limits): (Accept. Recoveries Standard Surrogate
Manager Project
JtShnson Nancy
Qe/ifro*t'
#1197) (ELAP ANALYTICAL MAR DEL
limit. reporting the above or at present not were N.D. as reported Analytes
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
N.D.
2.0
5.0
5.0
5.0
2.0
2.0
2.0
2.0
2.0
2.0
2.0
5.0
20
Xylenes Total
chloride Vinyl
acetate Vinyl
Trichlorofluoromethane
Trichloroethene
1,1,2-Trichloroethane
1,1,1-Trichloroethane
Toluene
Tetrachloroethene
1,1,2,2-Tetrachloroethane
Styrene
pentanone-2- Methyl 4chloride Methylene
2-Hexanone
Ethylbenzene
trans-1,3-Dichloropropene
cis-1,3-Dichloropropene
1,2-Dichloropropane
trans-1,2-Dichloroethene
cis-1,2-Dichloroethene
1,1-Dichloroethene
1,2-Dichloroethane
1,1-Dichloroethane
Chloromethane
Chloroform
ether vinyl 2-Chloroethyl
Chloroethane
Chlorodibromomethane
Chlorobenzene
tetrachloride Carbon
disulfide Carbon
2-Butanone
Bromomethane
Bromoform
Bromodichloromethane
Benzene
Acetone
10
2.0
2.0
2.0
2.0
2.0
2.0
5.0
2.0
2.0
5.0
2.0
10
5.0
2.0
2.0
5.0
5.0
10
5.0
5.0
2.0
2.0
10
(ppb)
(ppb)
pg/L
pg/L
Result Sample
Limit Reporting
Analyte
8240) (EPA GC/MS by ORGANICS VOLATILE
Water
1997 1, Aug
1997 29, Jul
1997 29, Jul
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
Matrix:
Reported:
Analyzed:
Extracted:
O'Connell Erin Attention:
91107 CA Pasadena,
204 Ste. Villa, Madre Sierra 650
Group Environmental Pacific
91406 CA Nuys,
779-1844 (818)
85281 AZ Tempe, I, Suite St.. 12th
968-8272 (602)
W.
2465
Van C-11, Suite Way, Sherman 16525
92606 CA Irvine, Ave Alton 2852
261-1022 (714)
92324 CA Colton, A, Suite
370-4667 (909)
MarAnalytical Del
Dr.. Cooley E. 1014
(
968-1338 (602)
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PRI
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
102%
1.9%
103%
3.8%
104%
10%
97%
5.2%
115%
98%
90%
7.8%
8.5%
94%
102%
96%
4.1%
98%
100%
3.1%
2.0%
101%
10%
116%
96%
RPD
Analytical Mar Del
Rl
Analysis Sample of Result
Terms: of Definition
OA
OA
PR
110%
100%
48
100%
50
102%
129
92%
55
122%
59
112%
45
98%
49
106%
51
104%
51
106%
102%
102%
118%
92%
PR2
46
61
125
51
50
53
49
56
51
53
52
MS
MSD
PRI
ppb
ppb
0/0
50
50
50
50
50
50
50
50
50
50
0
79
0
0
0.20
0
0
0
0
0
R1
Sp
ppb
ppb
Chloride Vinyl
Trichloroethene
Toluene
Tetrachloroethene
Chloroform
1,1-Dichloroethene
1,2-Dichlororethane
1,1-Dichloroethane
Chlorobenzene
Benzene
Analyte
MEAN
GG04038
7/29/97
#: SAMPLE
DATE:
Water Matrix:
624 METHOD: EPA
REPORT DATA MS/MSD
FAX
968-8272 (602)
85281 AZ Tempe.
1,
Suite
St 12th W. 2465
92324
370-1046 (909) FAX 370-4667 (909)
91406 CA Nuys, Van C-11. Suite Way. Sherman 16525
779-1843 (818) FAX 779-1844 (818)
261-1228 (714)
FAX
261-1022 (714)
MarAnalytical Del
CA Colton, A, Suite Dr., Cooley E. 1014
92606 CA Irvine. Ave., Alton 2852
(
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / ((MS-R1) MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
4.6
94%
I
4.3%
RPD
Analytical Mar Del
R1
Analysis Sample of Result
Terms: of Definition
ppm
Ok
PR
MEAN
92%
I
96%
PR1
PR2
I
4.8
I
ppm
MSD
ppm
ppm
0
5.0
Sp
MS
R1
Hydrocarbons
Analyte
Blank
7/31/97
Water
FAX
370-1046 (909)
91406
779-1844 (818)
FAX
779-1843 (818)
85281 AZ Tempe. I, Suite St., 12th W. 2465
968-8272 (602)
FAX
968-1338 (602)
92324 CA Colton, A, Suite Dr.. Cooley
370-4667 (909)
#: SAMPLE
C:
MarAnalyt-ical Del
CA Nuys. Van C-11, Suite Way. Sherman 16525
92606 CA Irvine, Ave., Alton 2852
261-1022 (714)
DATE:
Matrix:
METHOD: EPA
418.1
FAX
261-1228 (714)
E. 1014
Analytical Mar Del
R1
Analysis Sample of Result
Sp
sample to added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X ((MS-R1)/SP) MS; of Recovery Percent
PR2
100 X ((MSD-R1)/SP) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2) Difference; Percent Relative
PR Mean
Recovery Percent Mean
Limits Acceptance
Charts Control in-house by Determined
Terms of Definition
validation. batch for LCS to Refer *
*
:5.10
115 - 81
*
*
'10
82
115
5_10
115 - 81
-
115 83
119 - 81
PR Mean
89
...18
4.2
87
'10
5.1
80
5.6
79
6.9
80
6.9
83
85
89
16
16
78
82
16
77
50
77
81
85
92
RPD
Limits Acceptance
RPD
PR2
PR1
0
20
Ethylbenzene
0
20
15
Xylenes
0
60
46
212
198
17
18
ppb
PR Mean
MSD
Water
,
20
220
ppb
,
ppb
MS
0
10
Toluene
Benzene
TPH
ppb
Ss.
R1
Analyte
Date:
07/30/97
#: Sample
GG04449
#: Batch
GG30191W
Matrix:
8015/8020 Method EPA
92606
261-1022 (714)
FAX
261-1228 (714)
92324 CA Colton. A. Suite
370-4667 (909)
FAX
370-1046 (909)
779-1844 (818)
779-1843 (818) FAX
968-8272 (602)
968-1338 (602)
FAX
85281 AZ Tempe,
I,
Suite St., 12th W. 2465
91406 CA Nuys, Van
C-11,
Suite Way. Sherman 16525
Analytical Mar Del
Dr.. Cooley E. 1014
CA Irvine, Ave., Alton 2852
Analytical Mar Del
ACP
Recovery Percent for Limits Acceptance
TPH
Hydrocarbons Petroleum Total
100 X Conc.) Spike / Conc.) Spike - ((Result LCS; of Recovery Percent
%Recovery
LCS
Sample Control Laboratory
Conc Spike
Analysis Sample of Result
Result
Analysis Sample Control Laboratory of Result
Terms of Definition
% 115 - 85
% 115 - 85
% 115 - 85
% 115 - 85
% 115
-
85
ACP
19
95
20
20
18
90
18
92.
60
56
93
104
Recovery %
230
Result
Xylenes
Ethylbenzene
TPH
220
Toluene
Benzene
20
Conc. Spike
Analyte
Date:
07/30/97
#: Sample
BLANK
#: Batch
GG30191W
Water Matrix:
8015/8020 Method EPA
968-1338 (602) FAX 968-8272 (602)
FAX
261-1228 (714)
FAX
370-1046 (909)
FAX
779-1843 (818)
(
85281 AZ Tempe, 1, Suite St., 12th W. 2465
92324 CA Colton, A, Suite
370-4667 (909)
91406 CA Nuys, Van C-11,
779-1844 (818)
261-1022 (714)
Suite Way, Sherman 16525
Dr.,
Cooley
Analytical Mar Del
E. 1014
92606 CA Irvine, Ave., Alton 2852
FAX
261-1228 (714)
FAX
370-1046 (909)
779-1843 (818)
968-1338 (602)
Date:
Manager: Laboratory
limits. acceptance within were samples
QC of batch subsequent The future. the in closely more pressure concentrator the
monitoring about technicians the all to spoke Leader Group Organic The reported.
were results sample the limits, acceptance within were samples water the all
for recoveries surrogate the Since setting. pressure the corrected and concentrated
were samples water the before pressure incorrect the noticed technician The
Action: Corrective
concentrated. was solvent the of most problem, the noticed technician
extraction the time the By samples. QC the for concentration solvent the during
pressure wrong the at set was concentrator the procedure, extraction the During
Problem: the of Cause the of Determination
limits. acceptance the below was (LCS) Sample Control
Laboratory
the
and
(MS)
Spike
Matrix
the
for
TPH
extractable of recovery The
Problem: of Definition and Identification
Water
7/31/97
Matrix:
Date:
extractable 8015 mod. EPA
GC
Method:
Department:
REPORT ACTION CORRECTIVE
92606
261-1022 (714)
92324
370-4667 (909)
91406
779-1844 (818)
FAX
85281 AZ Tempe,
968-8272 (602)
FAX
I.
Suite St., 12th W. 2465
CA Nuys, Van C-11, Suite Way. Sherman 16525
CA Colton, A, Suite Dr, Cooley E. 1014
MarAnalytical Del
CA Irvine, Ave., Alton 2852
Sp
Sample to Added Concentration Spike
MS
Result Spike Matrix
MSD
Result Duplicate Spike Matrix
PR1
100 X SP) / -R1) ((MS MS; of Recovery Percent
PR2
100 X SP) / ((MSD-R1) MSD; of Recovery Percent
RPD
100 X ((MS-MSD)/(MS+MSD)/2)) Difference; Percent Relative
0/0
0/0
0/0
OA
56%
72%
25%
64%
I
Analytical Mar Del
R1
Analysis Sample of Result
Terms: of Definition
PR2
RPD
PR
MEAN
I
I
I
1.8
I
ppm
1.4
I
ppm
MSD
PR1
2.5
I
ppm
0
Hydrocarbons
ppm
Sp
MS
R1
Analyte
Blank
#: SAMPLE
7/31/97
Water
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
92606
261-1022 (714)
92324 CA Colton, A, Suite
370-4667 (909)
91406 CA Nuys, Van C-11, Suite Way, Sherman 16525
779-1844 (818)
85281 AZ Tempe, I, Suite St.. 12th
968-8272 (602)
CA Irvine, Ave.,
DATE:
Matrix
METHOD: EPA
extraction by 8015
FAX
261-1228 (714)
W.
2465
MarAnalytical Del
Dr.. Cooley E. 1014
Alton 2852
(
56%
PR
Analytical Mar Del
St
Concentration Standard
R1
Result Standard
PR
100 X St) I (R1 R1; of Recovery Percent
Terms: of Definition
1.4
Hydrocarbons
2.5
St
R1
ppm
ppm
Analyte
7/31/97
DATE:
extraction by 8015 METHOD: EPA
92606
261-1022 (714)
FAX
261-1228 (714)
92324 CA Colton, A, Suite Dr, Cooley
370-4667 (909)
FAX
370-1046 (909)
FAX
779-1843 (818)
FAX
968-1338 (602)
91406
779-1844 (818)
85281 AZ Tempe, I, Suite St., 12th
968-8272 (602)
W.
2465
Analytical Mar Del
CA Nuys, Van C-11, Suite Way, Sherman 16525
E. 1014
CA Irvine, Ave., Alton 2852
(
121/1
St. Suite
1. Tempe. AZ
85281
vJ
--1
Sample
Description
B
Relinqui 4'e
:
%....
_
Oil
7_,(1_,v,,1
a
13
Date /Time:
Date /Time
nodia.
Li Mc.
3
ftql
ocr64 it_i
6 VZAA.
D614-1
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do
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Sampling
Date/Time
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#of
Cont
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Z13
KIDNis-
Preservatives
pstibu I Oft sil
Sampler: peu.X,
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0
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Sample Container
Matrix
Type
14.0 Att.,
CVO
I
1
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17
t"
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.
/Time:
ate /T'
:
II
I
rili
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late /Ti 4"-
,
v
'..k
Rd
NE
(Th
CHAIN OF CUSTODY FORM
Project/PO Numbeechtz4
...-q
h5021968 8172 FAX (607) 968 1338
Note: Sample(s) will be disposed of after 30 days.
Relinuished By:
ii/
B
Vv
Relinquished
111
1
1-121) Li
115,D- 1--/
Vvx
.
two,/ 0 C bi.,mrc11.,
vez..c.ct, tvm cri20.19/4"
WO 36-1- 4 v-A4
Project ManagerfP,hone Nurntier:
5
d3 04: -0 ofi
(_
1
(818) 779 1844 FAX (818) 779.1843
Name/Addreset'etcA edckt Or b>
2465 W
FAX
pos) 370I046
(9091370.4667
(714) 2611022 FAX [7 41261.1228
2852 Alton Ave.. Inane. CA 92 714
Codey Or.. Suite A. Colton. CA 92324
10000 14=-11.62,von, gta
-
Client
E.
16575 Sherman Way. Suite C.11. Van Nuys, CA 91406
1014
Del Mar Analytical
/
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1
-go
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.
--#.7....s--.-ep
..h
4ry
--1\ e
ity-)is
,
u,
intact
Sampl Int
o
(Check)
ce
nor al
days
5
X
V/
1
structions
00
so
4.: 1
(check)
72 hours
24 hours
ray:
0
Z-
Special
y\}
No
&Jowl ilDot
P
48 hours
same day
Turnaround Time:
-c
,§-
Re
I
3.3
#1. bucket
of detergent) and water (tap contents the with equipment the Rinse brush.
with scrub and #1 bucket into washed be to equipment of piece the Place
3.4
#2. bucket
of water) (tap contents the with equipment the Rinse brush. with scrub
and #2 bucket in place and #1 bucket from equipment of piece the Remove
3.5
#3. bucket of
water) (distilled contents the with equipment the Rinse brush. the with scrub
and #3 bucket in place and #2 bucket from equipment of, piece Remove
water. Distilled #3: Bucket
water.
Tap
#2: Bucket
manufacturer).
the by specified as (mix detergent /CitranoxOwater Tap #1: Bucket
c)
b)
a)
3.1
use. to prior
water, distilled then and water tap with tub) wash (or bucket each Rinse
3.2
accordingly: fill and bucket each in brush one Place
Procedures
pair
gloves. Neoprene
3
brushes. Scrub
3.0
1
needed As
water. Tap
needed As
water. Distilled
gallon
detergent. CitranoxO
capacity).
minimum (5-gallon buckets or tubs Wash
1
3
Description
Quantity
Supplies and Equipment
2.0
project. this with
involved tasks the of performance the in personnel PACIFIC Inc. Group, Environmental
Pacific by performed were that techniques field describes section
following
The
Application and Scope
1.0
Technique Decontamination Equipment
conditions. site-specific on dependent is replaced be should contents
the which at frequency The bucket. each of contents the replace Periodically Note:
3.6
dry. air to surface prepared
or clean on place and #3 bucket from equipment of piece the Remove
3.7
decontamination. requires
which equipment field of piece each for 3.6 through 3.3 Steps Repeat
in soil the placing by screened field was soil The (FID). detector -ionizationflame a with
screening later for used was sampler the in soil Remaining laboratory. the to transport
for cooler chilled a in stored and custody, of chain the on identified labeled, then was
sample Each caps. plastic and sheets TeflonTM with covered were sleeve brass the of ends
The analysis. chemical for retained was sample soil intact lower-most The logs. boring
soil onto interval sample each at recorded was inches 18 sampler the advance to required,
counts blow of number The collection. sample for sampler the in placed were liners
brass 6-inch Three inches. 30 falling weight 140-pound a by feet vertical 5 every soil the
into driven is sampler California-type a procedure this Using 1586-84. Method Materials
and Testing for Society American with accordance in performed was sampling Soil
sampling. auger hand
during samples between contamination cross for potential the reduce to event sampling
each between water purified and tap with rinsed double and solution soap in washed
were augers Hand samples. between contamination cross for 'potential the reduce to event
sampling each between purified and tap with rinsed double and solution soap in washed
was sampler split-harrel The contamination. cross of chances the reduce to boring
each between and use to prior steam-cleaned was equipment drilling down-hole All
augers. stem hollow
with equipped rig drill truck-mounted a using drilled were borings soil The geologist.
or engineer PACIFIC a of direction the under performed was sampling soil and Drilling
Protocol Sampling Soil and Boring Soil
2.0
utilities. unmarked other and lines vent and/or distribution fuel underground
with contact avoid to feet 5 of depth minimum a to digger post-hole and auger hand
a using manually advanced was boring each drilling, to Prior utilities. underground their
of locations the mark owners utility the have to site the of vicinity the in utilities various
the of owners the contacted USA 1-800-422-4133). number phone free toll California
Southern - (USA Alert Service Underground of assistance the with utilities underground
all of location the researched PACIFIC site, on work of commencement the to Prior
Utilities Underground Locating
1.0
project. this with
involved tasks the of performance the in personnel PACIFIC Inc. Group, Environmental
Pacific by performed were that techniques field describes section following The
Techniques Sampling Soil
for
Procedure Operating Standard
8020A
and 8020
(MtBE) ether butyl
tertiary methyl and (BTEX) xylenes
ethylbenzene, toluene, Benzene,
8015 Mod.
(TPHg) gasoline as
hydrocarbons petroleum Total
8020
8015 Mod.
samples
soil other All
(BTEX) xylenes
ethylbenzene, toluene, Benzene,
(TPHd) diesel as
Hydrocarbons Petroleum Total
7471
Method(s)
Location Sample
Parameters Analytical
EPA
clarifiers or tanks, septic
diesel, waste-oil, Near
Metals 22 Title
Compounds Organic Volatile
(TRPH) hydrocarbons
petroleum recoverable Total
6010/7196/
624/8240
418.1
methods: test (EPA) Agency
Protection Environmental following the by analyzed were samples soil Select
Analyses Sample Soil
2.2
manager. project
regional the of discretion the at analyzed were and observations field on based selected
were analyzed samples soil additional Any result. screening field highest the with sample
the and boring per sample soil deepest the including analysis chemical for laboratory
the to submitted were boring soil each from samples soil two minimum, a At
Procedure Selection Analytical Sample Soil
2.1
System. Classification Soil United the by description and classification lithologic
for used was sample soil the of portion Another log. boring the onto recorded then was
reading stable observed highest The FID. calibrated a with screened field were bags the
in vapors Headspace temperature. ambient reach to allowed and bags plastic resealable
with compatible be to sized be should pack filter the in sand The interval.
casing slotted the of top the above feet 2 approximately of height a to
casing slotted the around placed be will pack filter The (Sand): Pack Filter
pre-cleaned. be must borehole the into introduced materials
All surface. the to well the extends which casing blank the with threaded
flush is casing slotted The table. water the below feet ten situated be
should well the of bottom The sand. pack filter of foot one approximately
on placed be will cap end an with casing well slotted of feet Twenty
casing. well factory-slotted and blank (PVC) chloride polyvinyl 40 schedule
diameter 2-inch of constructed is well The Screen: and Casing Well
below. presented are well monitoring groundwater
a of specifications and components well standard The well. the of
installation the begin will contractor drilling the borehole, the of completion
Following rig. drilling auger hollow-stem a using table water the below feet
approximately of depth a to boring soil a drill will contractor drilling The
11
Procedures
well per
plug well Locking
well per
box Well Rated Traffic
3.0
1
1
needed As
slotted). and (blank casing PVC 2-inch
needed, As
#3). Monterey (typically sand pack Filter
needed As
pellets. Bentonite
needed As
bentonite). and cement of (mixture Grout
Description
Quantity
driller) by (supplied Supplies and Equipment Required
2.0
Board. Control Quality Water Regional
the of requirements the meet to order in guidelines installation establish to is SOP this
of objective The well. monitoring groundwater a installing for (SOP) Procedure Operating
Standard following the developed has PACIFIC Inc. Group, Environmental Pacific
Application and Scope
1.0
Wells Monitoring Groundwater Installing
for
Procedure Operating Standard
well. the entering from fluids surface prevent to maintained
be will wellhead the at seal sanitary A grade. below feet 2 least at of depth
a to concrete in set be will box well The well. the of top the around installed
be will box well securable flush-mounted, traffic-rated, A Box: Well
casing. well
the on placed is plug well locking water-tight, expandable, An Plug: Well
bentonite. typically is grout This seal, bentonite the
above immediately space annular the in placed be will Grout Seal: Annular
feet. 3 of thickness approximate
an have will seal This pack. filter the above immediately
space annular the in placed be will pellets Bentonite Seal: Bentonite
bridging. for potential the minimize to casing
the around sand the introducing when taken be must Care #3. Monterey
is used typically sand The selected. size slot and size grain formation the
parameters. three the of stabilization
and water purge of volumes well-casing five to three of Removal (1)
met:
are conditions following two the of one until well the developing Continue
Sheet. Data Development Well PACIFIC a on
parameters stabilization the Record meter. triple a using water purge the of
conductivity specific and pH, temperature, the measure intervals, regular At
process. decontamination the during washer high-pressure a uses typically
contractor drilling The well. the entering equipment any decontaminating
is contractor drilling the that assure must personnel PACIFIC uses, between
and to Prior bailing. and surging both involves well the of Development
below). noted exceptions the (with well the develop will contractor drilling
the well, monitoring groundwater a of installation the completing Upon
Procedures
needed As
contractor). drilling by (provided block Surge
needed As
contractor). drilling by (provided bailer Purge
needed As
approved). (DOT drums 55-gallon
needed As
plugs. unlock'well to key appropriate
Also set). socket standard a (typically cover box well remove to required Tools
conductivity). specific and pH, temperature, measuring of (capable meter Triple
Description
3.0
1
Quantity
Supplies and Equipment Required
2.0
installation. well the of completion the following
immediately conducted usually is development Well well. monitoring groundwater the
in and formation the in groundwater between connection optimal the facilitate to is SOP this
of objective The well. monitoring groundwater a develop to (SOP) Procedure Operating
Standard following the developed has PACIFIC Inc. Consultants, Environmental PACIFIC
Application and Scope
1.0
Wells Monitoring Groundwater Developing
for
Procedure Operating Standard
be will drums The
disposal. pending site on stored temporarily
drums. 55-gallon approved (DOT) Transportation
of Department in water decontamination and purge the Contain
lid. box well the secure and well the on lock and plug well a Install
process.
purging the sustain to sufficient not is well the of Recharge (2)
1
laboratory).
the by prepared and (supplied blank Trip
needed As
set). socket standard a (typically
cover box well remove to required Tools
needed As
water. distilled water, tap
brushes, scrub equivalent), (or soap Citri-Nox
buckets, gallon 5 supplies: Decontamination
ice"). "blue (no ice dry or ice with chest Ice
sample per
bag. plastic Re-sealable
needed As
forms. Chain-of-custody
pen. marking Waterproof
performed.
be to analyses the on dependent is container(s)
of size and number The vials). VOA milliliter
40- (usually containers sample Lab-provided
Twine.
conductivity). specific and pH, temperature,
measuring of (capable meter Triple
(disposable). bailer Polyethylene
1
1
well per
3
needed As
1
well per
1
indicator. level water Electronic
1
(reusable) bailer PVC diameter 2-inch
Description
1
Quantity
Supplies and Equipment Required
2.0
project. this with
involved tasks the of performance the in personnel PACIFIC Inc. Group, Environmental
Pacific by performed were that techniques field describes section following The
Application and Scope
1.0
Technique Sampling Groundwater
for
Procedures Operating Standard
collection. of hours 24 within analysis for laboratory
the to relinquished were samples all event, sampling the of completion Upon
laboratory. the to transportation
during samples the accompanied blank trip laboratory-prepared One
-
analysis. chemical for laboratory the to transport for chest cooled
ice an in stored and bags plastic re-sealable in placed were sample(s) The
chain-of-custody. a on identified properly was sample Each
VOA.
labeled properly and laboratory-provided a to transferred was sample The
Sheet. Information Sampling PACIFIC
a on noted was appearance sample and time sampling
The well(s).
selected the from collected was sample groundwater a bailer), disposable
and gloves, sampling (twine, materials and equipment dedicated Using
first. came,
ever which hours, two or volume original its of 80% at-least to recharged
well the in groundwater of column the when collected were samples
Groundwater sampling. to prior measured again was groundwater to Depth
value(s). previous the of 10% within to stabilized parameters groundwater
the and groundwater of volumes casing three least at until continued
Bailing measured. were temperature and conductivity electrical pH,
of parameters groundwater the process, purging the Throughout well. the
from groundwater of volume calculated the purge to used was bailer PVC A
calculated. w'as purged be to
groundwater of volume appropriate the diameter, well the and measurements
the on Based measured. was well the of depth total The present). were
hydrocarbons phase liquid where used was probe (interface probe interface
or indicator level water a using measured was groundwater to Depth
water. deionized was bucket third the
and water tap clean was bucket second the solution, detergent non-phosphate
a of comprised was bucket first The wash. bucket three a
using equipment
of piece each decontaminate equipment, downhole any using to Prior
,
Procedures
3.0
disposal. pending site
on stored and labeled appropriately were
drums These drums. steel gallon,
55- Transportation-approved, of Department in contained were activities