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AIAS Meeting Gruppo di Lavoro Tecnologie di Giunzione Vicenza, 27-28 Marzo 2008 Prof. Ing. Alessandro Pirondi Università di Parma, Dipartimento di Ingegneria Industriale OUTLINE • Adhesive bonding - Academic Research - Technology Transfer - Education and Symposia • Welding - Academic Research - Education • Ongoing research and perspectives eretta, Poli MI) • Application - Lightweight jib for long-distance concrete casting - Structural adhesive (3M 9323 A/B) + woven grafite-epoxy laminate • Flow-chart of the project [Goglio, Rossetto, Dragoni, AIAS ‘02, Parma] ADHESIVE BONDING: Research OUTLINE •Adhesives and environmental conditions considered - Structural adhesives (Multibond 330, Hysol 9514, Hysol 9466) - Adherends: construction steel or aluminum alloy - Lab air •Studies - Fracture toughness, Fatigue Crack Growth (FCG) (experimental) - Fatigue strength and fatigue life prediction (experimental) - Failure simulation with a Cohesive Zone Model (CZM) (numerical) WHY FRACTURE...? •Bonding technology faults, service conditions •Literature survey - About 100 papers collected spanning over the last 10 years - Applications in: residual strength of joints with defects fatigue life prediction durability ranking (fitness-for-purpose) FRACTURE AND FCG TESTS DCB (Double Cantilever Beam) P teflon (s=0.05mm) shims h t h a0 = 45 mm W = 120 mm h = 15 mm t = 0.3 mm b = 30 mm a0 P W b P Tensile loading (Mode I) Mixed Tensile-Shear loading (Mixed-Mode I/II) CTS (Compact Tension-Shear) FRACTURE AND FCG TESTS •Qualifying points of the research (non-conventional features) - Automated crack length evaluation from compliance measurement - Fracture toughness correction to account for elasticity of the adhesive layer - Mixed-Mode I/II conditions •Outcomes - 3 peer-reviewed papers on international journals + 1 submitted - several national and international conferences •Exploitation of the results - Testing procedures - Fatigue life prediction methodology FATIGUE TESTS •Clip-gages (compliance monitoring=crack length evolution) •Applied load •Single-lap joint FATIGUE TESTS: defect evolution 25 Crack length, a [mm] 20 a a 15 10 5 steady-state accelerating 0 0 20000 40000 60000 80000 Number of cycles 100000 120000 140000 FATIGUE TESTS: life prediction - Time (cycles) to nucleate a defect negligible - Time (cycles) to propagate to rupture (Nf): Nf ac da C G m L W ac 2 a0 ( possible ) initial crack a0 b rupture L da C G m dN G f Pmax Pmin ,a C,m adhesive properties from FCG tests FATIGUE TESTS: life prediction •Example: Hysol 9514 single-lap joint 6 Average Shear Stress [Mpa] 5 4 3 2 1 Pred. 60mm exp 60mm Pred. 80mm exp 40mm exp 80mm Pred. 40mm 0 1000 10000 100000 Cycles to failure, Nf 1000000 10000000 SIMULATION: cohesive zone model •Concept (from: Hutchinson, Evans, Acta Mater. 48, 2000, 125-135 ) Adherend contribution to peel strength Adhesive contribution to peel strength SIMULATION: cohesive zone model •Use - Calibration of parameters on (standard) fracture tests - Simulation of failure of different geometries •Advantages - Efficient way to model potentially failing interfaces, including adhesive joints - Model transferability (not to be tuned case-by-case) •Potential applications - Structural joints static and fatigue failure - Composites static and fatigue delamination - Impact delamination (shock absorbers, car bodies, ...) - Peeling of flexible laminates - ... CZM SIMULATION: example •T-peel test: CZM calibrated on DCB fracture test (Multibond 330)* 800 700 600 Load (N) 500 Experiment Simulation 400 300 200 100 0 0.00 0.50 1.00 1.50 Displacement (mm) Courtesy Prof. M. Rossetto, Politechnic of Turin, Italy 2.00 2.50 3.00 ADHESIVE BONDING: Technology Transfer Plate heat exchanger •Current solution •AISI 316L stainless steel •Brazing •Max pressure 15bar •Max temperature 70°C •Overall cost: 11.5€ •Cost of brazing: 4.25€ (37% tot.!) Adhesive bonding ? •Proposed solution •Bolt(s) to sustain loading •MS adhesive for sealing •Overall cost 25% lower ! Wall decoration preassembled patches •Current solution •2x2cm2 10x10cm2 tesseras •Patch: 45x90cm2 •Preassembly system: adhesive dots on the back •Current adhesive solution: plastisol (single-component) highly flexibile low cost cure time 15’ at 190°C •Wear of anti-sticking coating alternative ? •Energy (heating) costs •Proposed solution •Two-component, high-flexibility adhesive (developed specifically by Henkel) •Cure time 20’ at room temperature •Higher adhesive cost •No energy costs for heating •Compactness of the new process line (no oven) Wall decoration preassembled patches - Polimerization tower (20’ storage capacity) •Engineering - Two-component adhesive dispenser Component A injectors Component B injectors Railway track joint (RFI-Henkel) •Application - Sustained loading conditions - High average shear stress •Sustained loading testing Creep Composite joint design (project driven by S. Beretta, Poli MI) • Application - Lightweight jib for long-distance concrete casting - Structural adhesive (3M 9323 A/B) + woven grafite-epoxy laminate • Flow-chart of the project [Goglio, Rossetto, Dragoni, AIAS ‘02, Parma] ADHESIVE BONDING: education EDUCATION • Academic - Seminars - Viscoelastic behaviour (polymers in general, about 6h) • On-the-job and collective courses - “Simulazione ad elementi finiti di giunzioni incollate”. 8h, Dallara Automobili, Parma - “TECNOLOGIE DI GIUNZIONE NON TRADIZIONALI: INCOLLAGGIO E FRICTION STIR WELDING”. 4h, CISITA, Parma. - “GIUNZIONI/COLLEGAMENTI”. Corso di Alta Formazione “Materiali, Progettazione e Innovazione di Prodotto”, UNIVERSITA’ DI PARMA - “ESEMPI APPLICATIVI DEL METODO DEGLI ELEMENTI FINITI: CONTATTO, ASSEMBLAGGIO, GIUNZIONI”. Corso di Formazione “Gli Elementi Finiti nella Progettazione Meccanica”, CSPMI, Reggio E. • Symposia - Yearly Henkel-Loctite workshop, 2000, 2005 • Progetto 2007 2° posto in classe 3 • Progetto 2008 • Utilizzo di materiali compositi (fibra di carbonio-resina epossidica) • Utilizzo di incollaggi • Motore semiportante WELDING: research OUTLINE •Joints and environmental conditions considered - Friction Stir Welded joints - Materials: aluminum alloy, aluminum alloy matrix composite - Lab air •Studies - Fracture toughness, Fatigue Crack Growth (FCG) (experimental) - Fatigue strength and fatigue life prediction (experimental) - Residual strength prediction (numerical) FRACTURE AND FCG TESTS - Al/Al2O3 butt joints C* d dP a f (C * ) FRACTURE AND FCG TESTS •Qualifying points of the research (non-conventional features) - FSW applied to Al/Al2O3 particulate composites - Automated crack length evaluation from compliance measurement - Crack closure evaluation and analysis - Crack path evaluation •Outcomes - 2 peer-reviewed papers on international journals (under re-review) - several national and international conferences •Exploitation of the results - Testing procedures - Joining technique qualification FATIGUE TESTS - Al overlap joints FATIGUE TESTS: defect evolution and life prediction Experimental Nasgro model-threshold 2,7 MPa*m^0.5 Nasgro early mode II propagation: 200 microns Nasgro early mode II propagation: 100 microns 60 s MPa 50 40 30 20 10 1,00E+04 1,00E+05 1,00E+06 1,00E+07 Number of cycles (N) 1,00E+08 RESIDUAL STRENGTH PREDICTION Transferability Kahn tear test large M(T) panels Al-alloy FSW butt joint 1:50 scale (in-plane) CTOA F Keff COD Δa WELDING: education • Academic - Seminars - Overview of weldability and design (about 10h) • On-the-job and collective courses - “Simulazione ad elementi finiti di giunzioni saldate”. 8h, Dallara Automobili, Parma - “TECNOLOGIE DI GIUNZIONE NON TRADIZIONALI: INCOLLAGGIO E FRICTION STIR WELDING”. 4h, CISITA, Parma. - “GIUNZIONI/COLLEGAMENTI”. 4h. Corso di Alta Formazione “Materiali, Progettazione e Innovazione di Prodotto”, UNIVERSITA’ DI PARMA - “ESEMPI APPLICATIVI DEL METODO DEGLI ELEMENTI FINITI: CONTATTO, ASSEMBLAGGIO, GIUNZIONI”. 8h. Corso di Formazione “Gli Elementi Finiti nella Progettazione Meccanica”, CSPMI, Reggio E. ONGOING RESEARCH AND PERSPECTIVES HYBRID JOINTS • Origin: PhD student stage at Henkel • Typologies of hybrid joints considered - Weldbonded (spot); Ultrasonic weldbonded (spot); rivetbonded; clinchbonded - Al/Al; Fe/Fe; Al/Fe (non weldbonded) + structural adhesive - Overlap joint • Program Literature research Market analysis Testing parameters (DoE from market analysis) Manufacturing Testing / FE simulation Influence of parameters Design guidelines HYBRID JOINTS -Ultrasonic weldbonding prel. results (joints manufactured at Poli MI) Strutturale Solo spotweld ultrasonico Ibrido con strutturale Ibrido con frenafiletti Ibrido con retainer Retainer HYBRID JOINTS Rivetbonding damage and failure simulation HYBRID JOINTS (da letteratura) Clinchbonding damage and failure simulation SELF-HEALING ? That’s all Folks! COLLABORATIONS - Prof. Gianni Nicoletto - Ing. David Fersini - Ing. Fabrizio Moroni - Ing. Matteo Vettori - Dr. Pierfranco Mauri - Dr. L.M. Volpone - Ing. C. Dalle Donne - ....